Measurement Operation - JEOL JSPM-5200 Instructions Manual

Scanning probe microscope
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MEASUREMENT OPERATION

5.1
BASIC USAGE OF WinSPM............................................................................. 5-1
5.1.1
Before use................................................................................................... 5-1
5.1.2
Glossary...................................................................................................... 5-1
5.1.3
Setting the User Name................................................................................ 5-4
5.2
STARTING THE SCAN (MEASUREMENT ) MODE ..................................... 5-7
5.2.1
Selecting SPM Operation Mode................................................................. 5-7
5.2.2
5.2.3
Shortcut Icons........................................................................................... 5-11
5.2.4
Software Oscilloscope.............................................................................. 5-12
5.2.5
Lock-In Amplifier .................................................................................... 5-13
5.2.6
Specimen Temperature Controller (for JSPM-5200)................................ 5-18
5.2.7
CCD Camera ............................................................................................ 5-18
5.2.8
Digital Control MFM unit ........................................................................ 5-19
5.3
PREPARING FOR MEASUREMENT ............................................................ 5-20
5.3.1
Starting the System in Measurement Mode.............................................. 5-20
5.3.2
Resetting the Controller............................................................................ 5-21
5.3.3
Confirming Settings of the Device Setup Dialog Box ............................. 5-21
5.3.4
Opening the SPM (Measurement) Parameters Window........................... 5-21
5.3.5
Checking the Stage Position ..................................................................... 5-22
5.3.6
Setting an Optional Oscilloscope ............................................................. 5-23
5.4
AC AFM MODE .............................................................................................. 5-25
5.4.1
AC Mode Tab ........................................................................................... 5-25
5.4.2
MFM Tab.................................................................................................. 5-36
5.4.3
VE-AFM Tab ............................................................................................ 5-41
5.4.4
SKPM Tab ................................................................................................ 5-45
5.4.5
Advanced Tab ........................................................................................... 5-54
5.5
CONTACT AFM MODE ................................................................................. 5-80
5.5.1
Contact Mode Tab .................................................................................... 5-80
5.5.2
Viscoelasticity Tab.................................................................................... 5-91
5.5.3
Lateral Modulation FFM Tab ................................................................... 5-95
5.5.4
Electrostatic Force Tab ............................................................................. 5-99
5.5.5
Advanced Tab ......................................................................................... 5-102
TMPM5200-2
5

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