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JNM-ECX Series
User Manuals: JEOL JNM-ECX Series FT NMR
Manuals and User Guides for JEOL JNM-ECX Series FT NMR. We have
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JEOL JNM-ECX Series FT NMR manual available for free PDF download: User Manual
JEOL JNM-ECX Series User Manual (71 pages)
Solid Measurement
Brand:
JEOL
| Category:
Laboratory Equipment
| Size: 1 MB
Table of Contents
Table of Contents
7
Safety Precautions
9
Precautions for Use
11
Outline of Solid-State Nmr Measurement
12
Solid-State Nmr System
13
Difference between Solid-State Nmr and Solution Nmr
14
Fundamentals of Solid-State Nmr Measurement
15
Interactions Influencing Solid-State Nmr Spectrum
16
Magic Angle Spinning
17
CW (Continuous Wave) Decoupling
18
High Power Decoupling
18
TPPM (Two Pulse Phase Modulation) Decoupling
18
Single Pulse Measurement
19
Cross Polarization
20
Principle of Cross Polarization
20
Notes of Cross Polarization
21
Setting of Instrument Conditions
22
Precaution for Operation
23
Adjustment of Magic Angle
25
Setting of Irradiation Frequency
26
Setting Pulse Width
27
Adjustment of Resolution
29
External Reference Setting
30
Reference Setting
30
Reference Setting by Using Z0 Shim
31
Adjustment of Cross-Polarization Condition under Low-Speed Spinning
32
Adjustment of Cross-Polarization Conditions
32
Adjustment of CP Condition under High Speed Spinning
33
Adjustment of VACP Conditions
33
Selecting a Method for Cross Polarization
34
Adjustment of Decoupling Conditions
35
Setting of CW (Continuous Wave) Decoupling Conditions
35
Setting of TPPM Decoupling Conditions
35
Setting of SPINAL64 Decoupling Conditions
36
Setting of XIX Decoupling Conditions
36
Setting of CM Decoupling Conditions
37
Setting of Swf-TPPM Decoupling Conditions
37
Adjustment of Measurement Conditions and Processing Conditions
38
Setting Pulse Width in Single Pulse Measurement
39
Setting Waiting Time in Single Pulse Measurement
40
Setting Contact Time in Cp Method
41
Setting Waiting Time in Cp Method
42
How to Use Forward Linear Prediction
44
How to Use Backward Linear Prediction
45
Multinuclear Measurement
46
Outline of Multinuclear Measurement
47
Method of Measuring 1 H/ 19 F
48
Method of Measuring Rare Spin Nucleus of Spin 1/2
48
Method of Measuring Nucleus of Half-Integer Spin
49
Method of Measuring Nucleus of Spin 1
49
Measurement of Relaxation Time
50
Outline of Relaxation-Time Measurement
51
Method
52
Relaxation Time Measurement by Direct Measurement
52
Relaxation Time Measurement of
52
In the Rotating Frame)
55
Measurement of T
55
RELAXATION TIME MEASUREMENT of 1 Ρ
56
Mqmas Method
57
Outline of Mqmas Method
58
Principle
60
Adjustment
62
Adjustment of Power
62
Adjustment of Parameters
63
Measurement
65
Processing
66
Appendix
69
Shearing Process
69
Scaling Processing
70
Index
71
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