Thermo Scientific Dionex UltiMate 3000 Series Manuals

Manuals and User Guides for Thermo Scientific Dionex UltiMate 3000 Series. We have 9 Thermo Scientific Dionex UltiMate 3000 Series manuals available for free PDF download: Operating Instructions Manual, Standard Applications Manual

Thermo Scientific Dionex UltiMate 3000 Series Operating Instructions Manual (270 pages)

Nano/Cap System. Nano/Cap Pump

Brand: Thermo Scientific | Category: Laboratory Equipment | Size: 5 MB

Table of Contents
3
1 Introduction

9
- How to Use this Manual
  9
- Safety Information
  11
- Intended Use
  22
- Federal Communications Commission (FCC) Note
  23
2 Overview

25
- Unit Description
  25
- Module Configurations
  27
  - Overview
    27
  - Combinations of Ultimate 3000 Pumps and Solvent Racks
    28
- Operating Principle
  29
- Front Panel Elements
  30
- Rear Panel
  32
  - Power Switch
    33
  - Fuse Cartridge
    33
  - USB Port
    33
  - Digital I/O
    33
  - Solvent Rack
    33
- Interior Components
  34
- Fluid Connections
  35
- Pump Module
  37
  - Rear Seal Wash System
    37
  - Flow Meter
    38
  - Leak Sensor
    40
  - Purge Valve
    40
  - Inline Filter (Loading Pump)
    41
- Column Compartment
  42
- Operation from Chromeleon
  43
- System Wellness, Predictive Performance, and Diagnostics
  44
3 Installation

45
4 Preparation for Operation (Startup)

63
- Overview
  63
- Capillaries and Capillary Routing
  65
  - Connecting and Handling Capillaries
    65
  - Routing Capillaries
    68
- Solvent Reservoirs
  70
  - General Notes
    70
  - Connecting the Solvent Reservoirs
    71
- Connecting Drain Tubing
  73
- Pump Module
  75
  - Setting up the Rear Seal Wash System
    75
  - Flow Meter Settings
    77
  - Purging the Pumps
    80
- Column Compartment
  86
- Equilibrating the System
  91
5 Operation and Maintenance

93
- Power-Up
  93
- Status Screen
  94
  - Pump Module
    94
  - Column Compartment
    95
- Operation from Chromeleon
  96
  - Connecting to Chromeleon
    96
  - Direct Control
    97
  - Automated Control
    100
- Function Keys and Menus on the Display
  102
  - Showing the Function Keys
    102
  - Menu
    104
- Information for Operating the Pump
  115
- Information for Operating the Column Compartment
  135
- Special Functions in Chromeleon
  140
- Recommendations for Optimally Running Systems (Best Practice)
  146
- Shutting down the Module
  148
- Maintenance, and Maintenance and Calibration Intervals
  150
  - General Information
    150
  - Maintenance Intervals
    151
  - Calibration Intervals
    152
6 Troubleshooting

153
7 Service

183
8 Module-Specific Information

227
- NC Pump
  228
  - Interior Components (Detailed View)
    228
  - Flow Path
    229
  - Operating Principle
    230
- Loading Pump (Micro Pump)
  234
  - Interior Components (Detailed View)
    234
  - Flow Path
    235
  - Operating Principle
    236
- Column Compartment
  237
  - Interior Components
    237
  - Operating Principle
    238
9 Proflow Flow Meter Upgrade

239
- Modifying the Module with a Proflow Flow Meter
  239
- Guidelines on Operating the Proflow Flow Meter
  242
10 Technical Information

243
11 Accessories, Consumables, and Spare Parts

247
- Standard Accessories
  247
- Optional Accessories
  250
- Consumables and Spare Parts
  251
12 Reference Information

255
- Chemical Resistance of PEEK
  255
- Solvent Miscibility
  258
- Properties of Common Solvents
  259
- Safety Information about Flammable Solvents
  260
13 Appendix

263
- Digital I/O (Pin Assignment)
  263
- Solvent Rack (Pin Assignment)
  264
14 Index

265

Thermo Scientific Dionex UltiMate 3000 Series Operating Instructions Manual (166 pages)

Brand: Thermo Scientific | Category: Water Pump | Size: 2 MB

Table of Contents
5
Introduction
9
How to Use this Manual
9
Safety
11
Symbols on the Pump and in the Manual
11
Safety Precautions
12
Consignes de Sécurité
16
Intended Use
20
Federal Communications Commission (FCC) Note
21
Overview
23
Unit Description
23
Operating Principle
24
Functional Schematic
25
Front Panel Elements
26
Rear Panel
27
Power Switch
28
Fuse Cartridge
28
USB Port
28
Digital I/O
28
Interior Components
29
Flow Path
30
Fluid Connections
31
Rear Seal Wash System
32
Pump Head (Liquid Displacement Assembly)
33
Mixing System
34
Purge Unit
35
Proportioning Valve
35
Leak Sensor
36
Vacuum Degasser
36
Operation with Chromeleon
37
Wellness and Predictive Performance
38
Installation
39
Facility Requirements
39
Unpacking
40
Positioning the Pump in the Ultimate 3000 System
41
Connecting the Pump
44
General Information
44
Connecting the USB Cable
44
Connecting the Power Cord
45
Connecting the Digital I/O
45
Setting up the Pump in Chromeleon
53
Initial Installation
53
Installing the Pump in Chromeleon
55
Configuring the Pump in Chromeleon
56
Setting up the Pump in Dcmslink
60
When a Corona or Coulochem III Detector Is Connected
61
Preparation for Operation (Startup)
63
Overview of Actions
63
General Precautions for Connecting and Handling Capillaries
65
Solvent Reservoirs
66
General Notes
67
Connecting the Solvent Reservoirs
68
Connecting Drain Tubing
70
Setting up the Rear Seal Wash System
70
Purging the Pump
72
Equilibrating the System
74
Operation and Maintenance
75
Power-Up
75
Status Screen
76
Operation with Chromeleon
77
Connecting to Chromeleon
77
Direct Control
78
Automated Control
80
Information for Operating the Pump
82
Choosing the Solvents
82
Using Pump Stroke Synchronization with the Autosampler
84
Setting the Flow Rate, Flow Acceleration, and Flow Deceleration
89
Setting the Pressure Limits
90
Recording the Pump Pressure
90
Rear Seal Wash System
91
Purging the Pump
92
Detecting Liquid Leaks in the Pump
92
Adjusting the Screen Brightness or Contrast
92
Vacuum Degasser
93
Special Chromeleon Functions
94
Predictive Performance
94
Monitoring the Digital Inputs (Digital I/O)
95
Operational Qualification and Performance Qualification
95
Shutting down the Pump
96
Routine and Preventive Maintenance
98
Troubleshooting
101
Overview
101
Error Codes on the Pump Display
102
Operating Problems
105
Service
111
General Notes and Safety Precautions
111
Eliminating Leakage
113
Pump Head, Pistons and Piston Seals
114
Visually Inspecting the Pump for Piston Seal Leakage
117
Pump Head and Pistons
118
Replacing the Piston Seals
126
Replacing the Check Valve Cartridge
132
Replacing the Purge Unit
133
Replacing the Proportioning Valve
134
Cleaning the Pump Head Components
135
Cleaning the Pistons
135
Cleaning the Check Valve Cartridges
136
Testing the Pump for Leakage
137
Vacuum Degasser (Rinsing the Degassing Channels)
139
Replacing the Main Power Fuses
140
Updating the Pump Firmware
141
Technical Information
143
Accessories, Consumables, and Spare Parts
145
Standard Accessories
145
Optional Accessories
147
Consumables and Spare Parts
148
Reference Information
151
Chemical Resistance of PEEK
151
Solvent Miscibility
154
Properties of Common Solvents
155
Safety Information about Flammable Solvents
156
Appendix ─ Digital I/O (Pin Assignment)
159
Index
163

Thermo Scientific Dionex UltiMate 3000 Series Operating Instructions Manual (160 pages)

Variable Wavelength Detectors

Brand: Thermo Scientific | Category: Security Sensors | Size: 1 MB

Table of Contents

5
- 1 Introduction
  
  9
  - How to Use this Manual
    9
  - Safety
    11
    
    Symbols on the Instrument and in the Manual
    11
    
    Safety Precautions
    13
    
    Consignes de Sécurité
    17
  - Intended Use
    21
  - Federal Communications Commission (FCC) Note
    23
- 2 Overview
  
  25
  - Unit Description
    25
  - Operating Principle
    26
  - Configurations
    28
  - Interior Components
    30
  - Front Panel Elements
    31
  - Rear Panel
    32
    
    Power Switch
    32
    
    Fuse Cartridge
    33
    
    USB Port
    33
    
    Digital I/O
    33
    
    Analog Outputs (Optional)
    33
    
    Ph and Conductivity Monitor (Optional)
    34
  - Fluid Connections
    35
  - Flow Cells
    36
  - Lamps
    37
  - Leak Sensor
    38
  - Detector Control
    38
  - System Wellness, Predictive Performance, and Diagnostics
    40
- 3 Installation
  
  41
- 4 Preparation for Operation (Startup)
  
  57
- 5 Operation and Maintenance
  
  63
  - Power-Up
    64
  - Status Screens
    65
  - Detector Control
    66
    
    Operation from the Front Panel Display
    66
    
    Chromeleon Software
    66
  - Display Screens (Function Keys and Menus)
    72
    
    Showing the Function Keys
    72
    
    Detector Menus
    74
5.5 Information for Operating the Detector

81
- Information for Operating the Detector
  81
  - General Notes
    81
  - Setting the Wavelengths
    86
  - Turning on the Lamps
    86
  - Monitoring the Lamp Intensity
    87
  - Starting and Stopping Data Acquisition
    88
  - Setting the Display Mode
    90
  - Leak Detection
    90
  - Recording the Temperature Signals
    91
  - Adjusting the Screen Brightness and Contrast
    91
  - Smartstartup and Smartshutdown
    91
- See Page
  92
- Special Functions in Chromeleon
  92
  - Optimizing the Detector Performance
    92
- Wavelengths
  94
- 6 Troubleshooting
  
  103
  - Overview
    103
  - Messages on the Detector Display
    104
  - Chromeleon Diagnostics Messages
    112
  - Operating Problems
    117
  - Mobile Phases
    120
- 7 Service
  
  123
  - General Notes and Safety Precautions
    123
  - Wavelength Calibration and Verification
    125
  - Lamp
    127
    
    Replacing the Deuterium Lamp
    129
    
    Installing or Replacing the Tungsten Lamp
    131
  - Flow Cell
    133
    
    Dummy Flow Cell
    133
    
    Cleaning the Flow Cell
    133
    
    Replacing the Flow Cell
    134
  - Drying the Leak Sensor
    139
  - Replacing the Main Power Fuses
    140
  - Updating the Detector Firmware
    141
- 8 Technical Information
  
  143
  - Flow Cells
    144
- 9 Accessories, Consumables, and Spare Parts
  
  147
  - Standard Accessories
    147
  - Optional Accessories
    148
  - Consumables and Spare Parts
    150
- 10 Appendix
  
  153
  - Common Mobile Phases
    153
  - Digital I/O
    155
  - Declaration of Conformity for Holmium Oxide Filters
    156
- 11 Index
  
  157

Thermo Scientific Dionex UltiMate 3000 Series Operating Instructions Manual (136 pages)

Fluorescence Detectors

Brand: Thermo Scientific | Category: Security Sensors | Size: 1 MB

Table of Contents
5
1 Introduction

9
- How to Use this Manual
  9
- Safety
  11
- Intended Use
  20
- Federal Communications Commission (FCC) Note
  22
2 Overview

23
- Unit Description
  23
- Operating Principle
  24
- Configurations
  27
- Interior Components
  28
- Front Panel Elements
  29
- Rear Panel
  30
  - Power Switch
    30
  - Fuse Cartridge
    30
  - USB Port
    31
  - Analog Outputs (Optional)
    31
- Fluid Connections
  31
- Flow Cells
  32
- Lamp
  33
- Leak Sensor
  33
- Detector Control
  34
- System Wellness, Predictive Performance, and Diagnostics
  35
3 Installation

37
4 Preparation for Operation (Startup)

53
- Overview
  53
- General Precautions for Connecting Capillaries
  54
- Connecting the Drain System
  55
- Installing the Flow Cell
  56
- Equilibrating the System
  59
- General Guidelines for Detector Operation
  60
  - Mobile Phases
    60
  - Mobile Phase Delivery System
    61
  - Flow Cells
    61
5 Operation and Maintenance

63
- Power-Up
  63
- Detector Display
  63
- Menus on the Detector Display
  65
  - Detector Menus
    66
  - General Menu Layout and Structure
    67
  - Main Menu
    69
  - Configuration Menu
    70
  - Diagnostics Menu
    71
  - Service Menu
    71
- Operation with Chromeleon
  72
  - Connecting to Chromeleon
    72
  - Direct Control
    73
  - Automated Control
    75
  - Smartstartup and Smartshutdown
    79
- Operational Settings
  80
  - Detecting Liquid Leaks in the Detector
    80
  - Adjusting the Screen Brightness or Contrast
    80
- Operational Modes of the Detector
  81
  - Single-Channel Mode
    81
  - Multi-Channel Mode (FLD-3400RS Only)
    81
  - Zero Order Mode
    82
  - Scans
    82
  - Scans (Only Chromeleon 7.1 or Later)
    84
- Optimizing Detector Performance
  85
- Monitoring System Functions
  98
- Shutting down the Detector
  101
- Routine and Preventive Maintenance Intervals
  103
6 Troubleshooting

105
- Overview
  105
- Messages on the Detector Display
  106
- Operating Problems
  110
7 Service

115
- General Notes and Safety Precautions
  115
- Lamp
  116
- Flow Cell
  117
  - Flushing the Flow Cell
    117
  - Replacing the Flow Cell
    118
- Drying the Leak Sensor
  121
- Replacing the Main Power Fuses
  122
- Updating the Detector Firmware
  123
8 Technical Information

125
9 Accessories, Consumables, and Spare Parts

127
- Standard Accessories
  127
- Optional Accessories
  128
- Consumables and Spare Parts
  129
10 Appendix: Common Mobile Phases

131
11 Index

133

Thermo Scientific Dionex UltiMate 3000 Series Operating Instructions Manual (138 pages)

Column Compartments

Brand: Thermo Scientific | Category: Security Sensors | Size: 1 MB

Table of Contents
5
1 Introduction

9
- How to Use this Manual
  9
- Safety
  11
- Intended Use
  20
- Federal Communications Commission (FCC) Note
  21
2 Overview

23
- Unit Description
  23
- Operating Principle
  24
- Configurations
  25
- Front Panel Elements
  26
- Rear Panel
  27
  - Power Switch
    28
  - Fuse Cartridge
    28
  - USB Port
    28
  - Digital I/O
    28
- Interior Components
  29
- Gas and Humidity Sensors
  30
- Column Switching Valve
  30
- Column Identification System (Column ID)
  32
- Pre-Column Heater
  32
- Post-Column Cooler
  33
- Operation from Chromeleon
  34
- System Wellness, Predictive Performance, and Diagnostics
  35
3 Installation

37
- Facility Requirements
  37
- Unpacking
  37
- Positioning the TCC in the Ultimate 3000 System
  39
- Connecting the TCC
  41
  - General Information
    41
  - Connecting the USB Cable
    41
  - Connecting the Power Cord
    42
  - Connecting the Digital I/O
    42
- Setting up the TCC in Chromeleon
  43
  - Loading the USB Driver for the TCC
    43
  - Installing the TCC
    45
  - Configuring the TCC
    46
- Setting up the TCC in Dcmslink
  52
4 Preparation for Operation (Startup)

53
5 Operation and Maintenance

67
6 Troubleshooting

95
- Overview
  95
- Messages on the TCC Display
  96
- Chromeleon Diagnostics Messages
  99
- Operating Problems
  100
7 Service

103
- General Notes and Safety Precautions
  103
- Removing Gases and Humidity from the Column Chamber
  105
- Column Switching Valve
  106
- Replacing the Main Power Fuses
  117
- Updating the TCC Firmware
  118
8 Technical Information

121
9 Accessories, Consumables, and Spare Parts

123
- Standard Accessories
  123
- Optional Accessories
  125
- Consumables and Spare Parts
  128
10 Appendix - Digital I/O (Pin Assignment)

133
11 Index

135

Thermo Scientific Dionex UltiMate 3000 Series Standard Applications Manual (103 pages)

RSLCnano

Brand: Thermo Scientific | Category: Laboratory Equipment | Size: 4 MB

Table of Contents
5
1 Using this Manual

9
- About this Manual
  10
- Conventions
  11
  - Special Notices and Informational Notes
    11
  - Typographical Conventions
    12
- Reference Documentation
  13
2 Application Setup

14
- General Recommendations for Applications
  15
- Available Trapping Columns
  21
  - Available Formats
    21
  - The Difference between Forward Flush and Back Flush
    22
- Installing the Ultimate 3000 Rslcnano System
  24
- Application Overview
  37
- Direct Injection Onto a Nano Column
  38
  - Hardware Layout
    38
  - Fluidic Setup
    39
  - Installation Tips
    40
  - Testing the Application
    40
  - Large Volume Injections
    41
- Direct Injection Onto a Capillary Column
  42
- Hardware Layout
  42
- Fluidic Setup
  43
- Installation Tips
  45
- Testing the Application
  45
- Pre-Concentration Onto a Nano Column
  47
  - Hardware Layout
    47
  - Fluidic Setup
    48
  - Installation Tips
    49
  - Testing the Application
    50
- Pre-Concentration Onto a 200 ΜM Monolithic Column
  51
  - Hardware Layout
    51
  - Fluidic Setup
    52
  - Installation Tips
    53
  - Testing the Application
    53
- Pre-Concentration Onto a Capillary Column
  55
  - Hardware Layout
    55
  - Fluidic Setup
    56
  - Installation Tips
    57
  - Testing the Application
    58
- EASY-Spray Columns with the Rslcnano
  59
- Salt Plugs with Nano Column
  66
  - Hardware-Layout
    66
  - Fluidic Setup
    67
  - Installation Tips
    68
  - Testing the Application
    69
  - Salt Solution Preparation
    70
- Tandem Nano LC
  71
3 Faqs

83
4 Appendix

93

Thermo Scientific Dionex UltiMate 3000 Series Operating Instructions Manual (88 pages)

UHPLC+ focused, Automated Fraction Collector

Brand: Thermo Scientific | Category: Laboratory Equipment | Size: 2 MB

Table of Contents
5
1 Introduction

7
2 Overview

19
- Unit Description
  19
- Operating Principle
  20
- Fraction Collector Configurations
  21
- Front Panel Elements
  23
- Rear Panel
  24
  - Power Switch
    25
  - USB Port
    25
  - RS-232 (Serial) Port
    25
  - Auxiliary I/O Connection
    25
- Universal Fraction Tray, Racks and Tubes
  26
- Chromeleon Software
  27
3 Installation

29
4 Verifying Installation

49
5 Operation and Maintenance

51
6 Troubleshooting

65
7 Service

67
8 Technical Information

77
9 Accessories, Spare Parts, and Consumables

79
10 Appendix - Chromeleon Example Program

83
11 Index

87

Thermo Scientific Dionex UltiMate 3000 Series Operating Instructions Manual (64 pages)

Solvent Racks

Brand: Thermo Scientific | Category: Laboratory Equipment | Size: 0 MB

Table of Contents
5
1 Introduction

7
2 Overview

17
- Unit Description
  17
- SRD Configurations
  17
- Front Panel Elements
  19
- Rear Panel
  20
- Fluid Connections
  21
- Leak Sensor
  22
- Wellness
  22
3 Installation

23
4 Preparation for Operation (Startup)

29
- Overview
  29
- Connecting Drain Tubing
  29
- Solvent Reservoirs
  30
5 Operation and Maintenance

35
6 Troubleshooting

45
- Overview
  45
- Messages on the Pump Display
  46
- Chromeleon Diagnostics Message
  46
- Operating Problems
  47
7 Service

51
8 Technical Information

55
9 Accessories, Consumables, and Spare Parts

57
- Standard Accessories
  57
- Optional Accessories
  59
- Consumables and Spare Parts
  59
10 Pin Assignment

61
- 15-Pin D-Sub Port
  61
- DC Input
  61
11 Index

63

Thermo Scientific Dionex UltiMate 3000 Series Operating Instructions Manual (26 pages)

Solvent Rack

Brand: Thermo Scientific | Category: Laboratory Equipment | Size: 0 MB

Table of Contents
5
1 Introduction

7
2 Installation and Maintenance

17
- General Information
  17
- Unpacking
  17
- Positioning the Solvent Rack in the Ultimate 3000 System
  18
- Inside View
  19
- Solvent Reservoirs
  20
  - General Precautions
    20
  - Connecting the Solvent Reservoirs
    21
- Routine and Preventive Maintenance
  22
3 Technical Information

23
4 Accessories, Consumables, and Spare Parts

25
- Standard Accessories
  25
- Consumables and Spare Parts
  25

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Thermo Scientific Dionex UltiMate 3000 Series Manuals

Table of Contents

1 Introduction

2 Overview

3 Installation

4 Preparation for Operation (Startup)

5 Operation and Maintenance

6 Troubleshooting

7 Service

8 Module-Specific Information

9 Proflow Flow Meter Upgrade

10 Technical Information

11 Accessories, Consumables, and Spare Parts

12 Reference Information

13 Appendix

14 Index

Table of Contents

Table of Contents

Table of Contents

1 Introduction

2 Overview

3 Installation

4 Preparation for Operation (Startup)

5 Operation and Maintenance

5.5 Information for Operating the Detector

6 Troubleshooting

7 Service

8 Technical Information

9 Accessories, Consumables, and Spare Parts

10 Appendix

11 Index

Table of Contents

1 Introduction

2 Overview

3 Installation

4 Preparation for Operation (Startup)

5 Operation and Maintenance

6 Troubleshooting

7 Service

8 Technical Information

9 Accessories, Consumables, and Spare Parts

10 Appendix: Common Mobile Phases

11 Index

Table of Contents

1 Introduction

2 Overview

3 Installation

4 Preparation for Operation (Startup)

5 Operation and Maintenance

6 Troubleshooting

7 Service

8 Technical Information

9 Accessories, Consumables, and Spare Parts

10 Appendix - Digital I/O (Pin Assignment)

11 Index

Table of Contents

1 Using this Manual

2 Application Setup

3 Faqs

4 Appendix

Table of Contents

1 Introduction

2 Overview

3 Installation

4 Verifying Installation

5 Operation and Maintenance

6 Troubleshooting

7 Service

8 Technical Information

9 Accessories, Spare Parts, and Consumables

10 Appendix - Chromeleon Example Program

11 Index

Table of Contents

1 Introduction

2 Overview

3 Installation

4 Preparation for Operation (Startup)

5 Operation and Maintenance

6 Troubleshooting

7 Service