Tcd Checkout Conditions And Chromatogram - Agilent Technologies 6890 Series Service Manual

610 Checkout Chromatograms

TCD checkout conditions and chromatogram

TCD checkout conditions and chromatogram
Column and sample
Type
Sample
Injection volume
Inlet
Temperature
Inlet pressure
Split/Splitless Only
Mode
Purge flow
Purge time
PTV—Splitless Mode
Inlet temperature
Initial time
Rate 1
Final temp 1
Final time 1
Rate 2
Final temp 2
Final time 2
Inlet pressure
Mode
Purge time
Purge flow
Detector
Temperature
Reference flow (He)
Makeup flow (He)
Offset
10 of 26
HP-5 30 m × 0.32 mm × 0.25 µm PN 19091J-413
FID Checkout PN 18710-60170
1 µL
250° C Purged/Packed or Split/Splitless
Oven Track Cool On-Column
40°C PTV (see below)
25 psi (Constant pressure for EPC inlets,
helium)
Splitless
60 mL/min
0.75 min
40°C
0.1 min
350°C
2 min
250°C
0 min
0.75 min
60 mL/min
300° C
20 mL/min
2 mL/min
≤
Should be 30 display counts
Performance Verification
Agilent 6890 Gas Chromatograph Service Manual
720°C/min
100°C/min
25 psi (const. press. for EPC inlets)
Splitless
Jun 2001