Thermo Scientific Dionex ICS-5000 Operator's Manual page 474

Dionex ICS-5000 Operator's Manual
Operation
Analyzing samples, 172
Creating a sequence, 173 – 174
Direct control of modules, 171
Filling vials, 146, 149
Loading samples, 178
Overview, 172
Sample preparation, 147
Starting a sequence, 176 – 177
Organic solvent, 77
Oven (TC), 116
See also Temperature control (TC)
Oven LED (TC)
LED is flashing, 116, 300
LED is lighted, 116
Oven LEDs (DC)
LED is flashing, 51
LED is lighted, 51
P
PAD
See Pulsed amperometry
Palladium hydrogen (PdH) reference
electrode, 79
Replacement procedure, 400
Panel tabset, 11
Home panel, 11, 149, 151
How to display, 157, 165, 169, 255 – 256
Parameters
Chromeleon commands, 172
Peak height
Reproducibility, 69
Peaks
Fronting, 118
Reversed, 86
Tailing, 118, 222
Periodic maintenance
DC, 199
DP/SP, 196
TC, 201
pH gradient, 77
Index-12
pH half-cell, 77
pH limits, 145
pH modifier, 43
pH reading
Adjusting potentials for, 77
Always 7.0, 271
Cannot be set to 7.0, 272
Effect on potentials, 77
Monitoring, 78
Nonexistent, 273
pH-Ag/AgCl reference electrode, 75, 77
Long-term storage, 187
O-ring replacement procedure, 399
Replacement procedure, 392
See also Reference electrode
Photodiode Array Detector, 3, 9
Regulator Bracket Kit, 35
Piston seal wash solution, 26, 183
Piston seal wash system, 26, 154
Activation, 26
Dual pump seal wash option, 27, 154, 436
Replumbing the DP connections, 154
Setup, 156
Piston seals
Replacement procedure, 316
Pistons
Replacement procedure, 323
Platinum working electrodes, 75
Plot, I-t, 111
Plumbing
Replacing DC tubing and fittings, 359
Replacing DP/SP tubing and fittings, 306
Replacing EG tubing and fittings, 333
Replacing TC tubing and fittings, 407
Plumbing configuration drawings, 129 – 139
Polarity
Analog output, 86
Polishing kit (ED)
Reordering, 443
Polishing working electrodes, 389
Post-column reagent addition, 61, 94, 139
Potassium carbonate eluent, 41, 43
Potassium hydroxide eluent, 41
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