Thermo Scientific Dionex ICS-2000 Manuals

Manuals and User Guides for Thermo Scientific Dionex ICS-2000. We have 3 Thermo Scientific Dionex ICS-2000 manuals available for free PDF download: Operator's Manual, Manual, Preventive Maintenance Procedure

Thermo Scientific Dionex ICS-2000 Operator's Manual (390 pages)

ION CHROMATOGRAPHY SYSTEM

Brand: Thermo Scientific | Category: Analytical Instruments | Size: 5 MB

Table of Contents
3
Introduction
13
Introduction to Ion Chromatography (IC)
13
Overview of the ICS-2000
16
About this Manual
17
Safety Messages and Notes
18
Safety Labels
20
Features
21
Operating Features
21
Front Panel
21
Top Cover
26
Component Panel
27
Rear Panel
30
The Chromeleon Interface
32
The Chromeleon Main Window and Browser
32
The ICS-2000 Control Panels
33
Flow Schematics
43
System Component Details
50
Vacuum Degas Assembly
50
Eluent Valve
52
Pump
52
Eluent Generator
55
Injection Valve
60
Column Heater
62
Suppressor
62
DS6 Heated Conductivity Cell
63
Operation and Maintenance
65
Operation Overview
65
Power up the System
67
Start Chromeleon
68
Set up the Eluent Reservoir
70
Filter the Deionized Water
70
Fill the Reservoir
71
Set the Eluent Level
71
Connect the Reservoir
73
Check All Connections
73
Prime the Pump
74
Set System Operating Conditions
75
Equilibrate the System and Verify Operational Status
76
Prepare Samples
77
Collecting and Storing Samples
77
Pretreating Samples
77
Diluting Samples
78
Loading and Injecting Samples
78
Loading Samples with a Syringe
79
Loading Samples with a Vacuum Syringe
80
Loading Samples with an Autosampler
80
Injecting Samples
81
Example Chromeleon Commands for Loading and
81
Process Samples
82
Manual Sample Processing
82
Automatic (Batch) Sample Processing
83
Maintenance
85
Troubleshooting
87
Error Messages
87
Troubleshooting Error Messages
89
Liquid Leaks
98
Pump Difficult to Prime or Loses Prime
100
Pump Does Not Start
102
No Flow
103
Erratic Flow/Pressure Reading
104
Excessive System Backpressure
104
Peak "Ghosting
105
Nonreproducible Peak Height or Retention Time
106
Abnormal Retention Time or Selectivity
106
No Cell Response
106
High Cell Output
107
Baseline Noise or Drift
108
Vacuum Degas Assembly Does Not Run
109
Service
111
Diagnostic and Calibration Procedures
111
Chromeleon Wellness Panel Overview
112
Diagnostic and Calibration Touch Screen Overview
114
Calibrating the Conductivity Cell
115
Calibrating the Flow Rate
117
Calibrating the Vacuum Degas Assembly
119
Isolating a Restriction in the Liquid Lines
120
Replacing Tubing and Fittings
124
Rebuilding the Injection Valve
125
Cleaning and Replacing the Pump Check Valves
126
Replacing a Pump Piston Seal and Piston Rinse Seal
128
Replacing a Pump Piston
132
Replacing the Waste Valve or Priming Valve O-Ring
133
Replacing the Conductivity Cell
135
Replacing the Suppressor
138
Replacing the Column Heater
139
Replacing the Column Heater Heat Exchanger
142
Replacing the Eluent Valve
143
Replacing the Leak Sensor
145
Priming the Pump with Isopropyl Alcohol
146
Changing Main Power Fuses
147
Replacing an Elugen Cartridge
148
Replacing a KOH, Lioh, MSA, or Naoh Elugen
149
Cartridge
151
Replacing the CR-TC
170
Replacing the EPM Electrolytic Ph Modifier
174
Recording the EPM Serial Number in Chromeleon
175
Plumbing the EPM for Hydrating and Conditioning
176
Hydrating and Conditioning the EPM
178
Filling the EGC CO3 Mixer with Eluent
183
Replacing the EGC Holder and Degas Assembly
190
Disconnecting and Removing the Elugen Cartridge
190
Removing the CR-TC and Reinstalling It in the New EGC
193
Holder
193
Removing the EPM and Reinstalling It in the New EGC
195
Holder
195
Installing the New EGC Holder Without a CR-TC or EPM
197
Reinstalling the Elugen Cartridge
198
A • Specifications
199
Electrical
199
Physical
199
Environmental
199
Front Panel
200
Pump
200
Detector
201
Conductivity Cell with Heat Exchanger
201
Injection Valve
201
Vacuum Degas Assembly
201
Column Heater
202
Eluent Generator
202
B • Installation
205
Facility Requirements
205
Unpacking the ICS-2000 System
206
Unpacking the Computer (North America Only
208
Unpacking the Computer (Outside North America
208
Installing Chromeleon
208
Installing the Chromeleon Software License
208
Connecting the ICS-2000 to the Chromeleon PC
214
Connecting the ICS-2000 to the PC
214
Connecting Additional USB Devices
215
Connecting the Power Cord
216
Turning on the ICS-2000 Power
217
Setting up Chromeleon
219
Assigning the ICS-2000 to a Timebase
219
Assigning DX-LAN Devices to the Timebase (Optional
224
Installing and Plumbing the Columns and Suppressor
227
Setting up the Column Heater
227
Installing the Columns
228
Installing the Suppressor
229
Connecting the Waste Lines
231
Installing the Gas Separator Waste Tube
231
Setting up the Eluent Reservoir
233
Setting the Eluent Level
234
Priming the Pump
235
Priming the Eluent Lines with a Syringe
236
Priming the Pump Heads with the Prime Button
238
Setting up the Eluent Generator
239
Eluent Generator Setup for KOH, Lioh, MSA, and Naoh
240
Eluents
240
Eluent Generator Setup for Carbonate/Bicarbonate Eluent
256
Eluent Generator Setup for Carbonate Eluent
282
Setting up a Chromeleon Application
299
Verifying Chromeleon Communication
308
Equilibrating the System
309
Elugen Cartridge Backpressure Requirements
310
Verifying Operational Status
310
Connecting an as or AS50 (USB) Autosampler (Optional
311
AS or AS50 (USB) Connections
312

Thermo Scientific Dionex ICS-2000 Manual (16 pages)

Preventive Maintenance Procedure for Ion Chromatography Systems

Brand: Thermo Scientific | Category: Laboratory Equipment | Size: 0 MB

Thermo Scientific Dionex ICS-2000 Preventive Maintenance Procedure (12 pages)

Brand: Thermo Scientific | Category: Laboratory Equipment | Size: 1 MB

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