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Summary of Contents for Thermo Scientific iCAP Q
- Page 1 Thermo Fisher Scientific iCAP Q Operating Manual Revision B - 1288090 Part of Thermo Fisher Scientific...
- Page 2 © 2012 Thermo Fisher Scientific Inc. All rights reserved. Original Operating Instructions Leybonol and Sogevac are a registered trademarks of Oerlikon Leybold Vacuum GmbH. Santoprene is a registered trademark of Monsanto, Inc. Viton is a registered trademark of DuPont Dow Elastomers.
- Page 3 28199 Bremen Germany Send an e-mail message to the Technical Editor at • documentation.bremen@thermofisher.com You are encouraged to report errors or omissions in the text or index. Thank you. Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B)
- Page 4 Contacting Us Suggestions to the Manual iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific...
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Page 5: Table Of Contents
Vacuum System .............. 3-11 Forepump ..............3-12 Turbomolecular Pump..........3-12 Pressure Measurement..........3-12 Gas Supply..............3-13 Connections..............3-13 Plasma and Cooling Gas ..........3-14 CCT Gas ..............3-15 Additional Gas ............. 3-17 Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B) - Page 6 System Controls..............6-4 System Status LEDs ............6-4 Power Panel ..............6-5 Starting Up the System ............. 6-6 Shutting Down the System ..........6-7 Switching to Standby Mode ........... 6-7 iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific...
- Page 7 Cleaning the Surface of the Instrument ......8-7 Cleaning Agents ............. 8-7 Checking Warning Labels ..........8-7 Checking Gas Lines for Leaks ........8-8 Maintaining the Air Filter ..........8-9 Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B)
- Page 8 Service Only..............8-26 Chapter 9 Additional Safety Information..........9-1 Fore Vacuum Pump............9-2 Recirculating Chiller ............9-4 Dionex ICS-5000.............. 9-5 Legal Documents ..............D-1 Glossary ..................G-1 Index .................... I-1 iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific...
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Page 9: Using This Manual
It describes the modes of operation and principle hardware components of your iCAP Q mass spectrometer and provides step-by-step instructions for cleaning and maintaining your instrument. Thermo Fisher Scientific... -
Page 10: Typographical Conventions
“press <Shift> + <F1>” means press and hold the <Shift> key and then press the <F1> key. Any button that you click on the screen is represented in bold face • letters. For example, “click Close”. iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific... -
Page 11: Topic Headings
Topic Headings The following headings are used to show the organization of topics within a chapter: Chapter Name Chapter 1 Second Level Topics Third Level Topics Fourth Level Topics Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B) -
Page 12: Reference Documentation
The iCAP Q Operating Manual represents the Original Operating Instructions. Thermo Fisher Scientific provides additional reference documents for the iCAP Q mass spectrometer that are not part of the Original Operating Instructions. Reference documentation for the iCAP Q mass spectrometer includes the following: iCAP Q Preinstallation Requirements Guide •... -
Page 13: Scope Of Delivery
Equipment for connecting the basic instrument • Printed manuals iCAP Q Operating Manual For a list of the manuals delivered with the iCAP Q mass spectrometer and instructions on where to find PDF files of these manual, see “Reference Documentation” page 1-4. -
Page 14: Optional System Components
Autosampler ESI, ESI FAST, or CETAC • Autosampler housing • NESLAB ThermoFlex 2500 Recirculating Chiller • Dionex ICS Ion Chromatography System • • Noise reduction cover and drip pan for fore vacuum pump iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific... -
Page 15: System Description
System Description Chapter 3 This chapter provides an overview of the functional elements of the iCAP Q instrument. It contains the following topics: • “General Description” page 3-2 “Sample Introduction System” page 3-4 • “Ion Optics” page 3-9 • “QCell”... -
Page 16: General Description
System Description General Description General Description The iCAP Q mass spectrometer is designed for direct analyses of liquid samples and can be coupled to further devices for analyses of gases or solid aerosols. Three models are available: iCAP Qa, iCAP Qc and iCAP Qs. -
Page 17: Instrument Layout
System Description General Description Instrument Layout The iCAP Q instrument can be divided into four main components, which are described in the following topics: Sample introduction • Interface (ion generation) • Ion Optics (ion focussing) • Mass Analyzer • Labeled Components: 1= sample introduction, 2=interface, 3=ion optics, 4=mass analyzer Figure 3-2. -
Page 18: Sample Introduction System
System Description Sample Introduction System Sample Introduction System The sample introduction system of the iCAP Q MS comprises the peristaltic pump, the nebulizer, the Peltier-cooled spray chamber and the torch with the injector. Figure 3-3 shows a schematic view of the sample introduction system. -
Page 19: Nebulizer
Depending on the model ordered, the spray chamber is made of either quartz or PFA, see Table 3-1. Labeled Components: 1=nebulizer, 2=spray chamber, 3=injector, 4=torch Figure 3-5. Nebulizer, spray chamber, injector and torch Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B) -
Page 20: Injector
System Description Sample Introduction System For the iCAP Q instrument, the spray chamber is cooled using a Peltier cooled chiller to improve instrument performance. Injector The injector is available with various internal diameters (ID) and in various material for different types of analysis. Injectors with smaller... -
Page 21: Interface
The sample cone introduces ions from the plasma into the first vacuum stage (interface vacuum) and the skimmer cone admits the ions in the mass spectrometer. Figure 3-8. Sample cone and skimmer cone Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B) -
Page 22: Extraction Lens
Figure 3-9. Detail of extraction lens The extraction lens focusses and accelerates the ions from the back of the skimmer cone into the intermediate vacuum region of the analyzer. iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific... -
Page 23: Ion Optics
The ion optics region comprises the RAPID lens, the QCell, and the DA assembly. RAPID Lens Ions extracted from the iCAP Q interface are accelerated to the RAPID (Right Angle Positive Ion Deflection) lens which deflects analyte ions by 90 ° before they enter the QCell. -
Page 24: Da Assembly
RF voltage and DC voltage applied to the quadrupole rods. Detector Ions transmitted through the quadrupole are finally transferred to the dual mode secondary electron multiplier (SEM) and detected. 3-10 iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific... -
Page 25: Vacuum System
The ICP source operates at atmospheric pressure while the mass analyzer and detector requires a high vacuum for optimum performance. The iCAP Q instrument has a three-stage pumping system realized by a rotary pump and split-flow turbomolecular pump. Figure 3-11 shows a schematic view of the vacuum stage in the instrument. -
Page 26: Forepump
The pressure values are read back to the Dashboard of the Experiment Editor, see Figure 3-12. The values are also read back in the Vacuum pane of the Instrument Control window. Figure 3-12. Experiment Editor - Dashboard 3-12 iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific... -
Page 27: Gas Supply
System Description Gas Supply Gas Supply The iCAP Q MS uses argon gas to generate the inductively coupled plasma and to control internal functions with the aid of pneumatics. Additional gases may be required depending on the type of analysis. -
Page 28: Plasma And Cooling Gas
Inside the iCAP Q instrument, tubes are already installed from the connector to the optional mass flow controller. The connectors for additional gases are also situated on the left side of the iCAP Q instrument, see 4 and 5 in Figure 3-13. -
Page 29: Cct Gas
System Description Gas Supply Connection of the laboratory argon supply to the iCAP Q instrument is made via a push-in fitting. A recommended set-up for the argon supply is shown in Figure 3-15: Labeled Components: 1=pressure regulator, 2=shut-off valve, 3=pressure gauge, 4=argon inlet, 5=iCAP Q, 6=gas source Figure 3-15. - Page 30 Thermo Fisher Scientific does not endorse any manufacturer, nor does it endorse products other than its own. Companies and products listed in this guide are given as examples only. 3-16 iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific...
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Page 31: Additional Gas
Additional gas requirements for helium Gas Requirements Specification Purity 99.996% Maximum water content < 5 ppmv Supply rate max. 1 L/min Pressure regulator output 0.6 MPa (6 bar) Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B) 3-17... - Page 32 Additional gas requirements for argon Gas Requirements Specification Purity 99.996% Maximum water content < 5 ppmv Supply rate max. 1 L/min Pressure regulator output 0.6 MPa (6 bar) 3-18 iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific...
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Page 33: Cooling System
Connections for Water Supply The iCAP Q system can be supplied with cooling water either from a central system or from the optionally shipped recirculation water chiller NESLAB ThermoFlex 2500. The connections for the cooling water are... -
Page 34: Recirculating Chiller
System Description Cooling System Recirculating Chiller Optionally, the iCAP Q mass spectrometer is delivered with the recirculating chiller NESLAB ThermoFlex 2500 with closed circuit, cooled by a refrigerating device. NOTICE For more information, refer to the manufacturer’s manual supplied with the instrument and see “Recirculating Chiller”... -
Page 35: Exhaust System
System Description Exhaust System Exhaust System An exhaust system is needed for the iCAP Q MS to remove gases that may contain ozone and other noxious substances. Two exhaust ports are situated at the top of the instrument, see Figure 3-17. -
Page 36: Connections
Connections The main power switch, the mains inlet, the water supply connections, the pumping connections, and the gas supply connections of the iCAP Q are located at the left side of the instrument, see Figure 3-18. Labeled Components: 1=main power switch, 2=main power supply, 3=water connections, 4=pumping connections, 5=gas connection Figure 3-18. -
Page 37: Main Power Switch
Figure 3-20. Main power switch of iCAP Q MS Power Connections The main power supply connection and the power connection for the fore vacuum pump are located at the left side of the iCAP Q mass spectrometer, see Figure 3-21. -
Page 38: Fore Vacuum Pump Connections
Labeled Components: 1=power connection to fore vacuum pump, 2=pumping hose to fore vacuum pump, 3=exhaust fore vacuum pump Figure 3-22. Fore vacuum pump connection detail of left view of iCAP Q MS 3-24 iCAP Q Operating Manual (P/N 1288090, Revision B) -
Page 39: Connection To Computer And Peripherals
System Description Connections Connection to Computer and Peripherals The peripheral control connections allows transmitting digital contact closure signals from the iCAP Q mass spectrometer to other systems such as autosamplers or LC systems. Figure 3-23 shows the connection panel at the right side of iCAP Q MS. - Page 40 System Description Connections 3-26 iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific...
- Page 41 “Electrical Safety Precautions” page 4-8 • “Residual Hazards” page 4-9 • • “Personal Protective Equipment” page 4-10 “EMC Information” page 4-11 • • “In Case of Emergency” page 4-12 Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B)
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Page 42: Safety
Be sure to read and comply with all precautions described in this manual. System configuration and specifications in this manual supersede all previous information received by the purchaser. iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific... -
Page 43: Safety Symbols On The Instrument
The label indicates the presence of electricity at the main power switch. The label indicates the presence of high voltage inside the instrument. Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B) - Page 44 The label indicates the presence of noxious gases at the plasma exhaust. The label marks the gas connections. Only permitted gases may be connected here, see “Permitted Materials” page 4-7. iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific...
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Page 45: Rating Plate
615 MODEL: iCAP Q SERIAL No: This device complies with Part 18 of the FCC Rules Figure 4-1. Rating plate at the rear side of the iCAP Q MS Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B) -
Page 46: Intended Use
• designed for use in diagnostic or medical therapeutic procedures. If the iCAP Q mass spectrometer is used in a manner not specified by Thermo Fisher Scientific, the protection provided by the instrument could be impaired. Thermo Fisher Scientific assumes no responsibility and will not be liable for instrument damage and/or operator injury. -
Page 47: Qualified Personnel
Permitted Materials Qualified Personnel Only employees of Thermo Fisher Scientific or personnel acting on behalf of Thermo Fisher Scientific are permitted to install the iCAP Q mass spectrometer. Personnel that installs or operates iCAP Q mass spectrometer must have the following qualifications: Electrical Connections •... -
Page 48: Electrical Safety Precautions
Do not place any objects upon the instrument—especially not • containers with liquids—unless it is requested by the user documentation. Leaking liquids might get into contact with electronic components and cause a short circuit. iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific... -
Page 49: Residual Hazards
By making the operator aware of the potential risks, we hope to ensure maximum safety in the operation of this mass spectrometer. Users of the iCAP Q mass spectrometer must pay attention to the following residual hazards. WARNING Toxic Gases. -
Page 50: Personal Protective Equipment
19-120-2947C [size large]; Thermo Scientific P/N 23827-0008) [size medium] or P/N 23827-0009 [size large]). For handling hot objects, gloves made of heat-resistant materials (for example, leather) should be available. 4-10 iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific... -
Page 51: Emc Information
Notice on the Susceptibility to Electromagnetic Transmissions Your instrument is designed to work in a controlled electromagnetic environment. Do not use radio frequency transmitters, such as mobile phones, in close proximity to the instrument. Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B) 4-11... -
Page 52: In Case Of Emergency
Figure 4-2 shows the plasma door handle: Labeled Components: 1=plasma door closed, 2=plasma door open Figure 4-2. Plasma door handle at front of iCAP Q MS ❖ To shut off the plasma in case of emergency 1. Turn the handle 1 in Figure 4-2 clockwise for 180 degrees. - Page 53 5-7 • Only employees of Thermo Fisher Scientific or personnel acting on behalf of Thermo Fisher Scientific are allowed to install the iCAP Q mass spectrometer. Only employees of Thermo Fisher Scientific or personnel acting on behalf of Thermo Fisher Scientific are allowed to install the additional gas module (MFC).
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Page 54: System Setup
CAUTION Hazardous Gases. Danger to health. When operating the instrument with hazardous gas, an external warning sensor must be installed in the vicinity of the instrument. iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific... -
Page 55: Placing The System
System Setup Placing the System Placing the System The iCAP Q instrument is a bench top instrument to be placed on top of a table with its rear panel against a wall. Instrument Dimensions Figure 5-1 shows the typical required floor space for the system without autosampler. -
Page 56: Moving The Instrument
1400 700-1000 2100-2400 3500-3800 Labeled Components: 1=monitor, 2=mouse, 3=keyboard, 4=iCAP Q MS, 5=wall, 6=autosampler housing, 7= computer table Figure 5-2. Required floor space for iCAP Q MS with autosampler Moving the Instrument The iCAP Q mass spectrometer is provided with four retractable handles for transport. -
Page 57: Workbench For Instrument
(autosampler, liquid chromatograph, for example) and stand in a secure and level position. Only workbenches with four legs provide sufficient stability for the iCAP Q mass spectrometer. The workbench must be dry and clean. Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B) - Page 58 It is recommended to leave sufficient space on the right side of the iCAP Q system for the connections to the computer and peripheral devices. NOTICE Avoid blocking the ventilation slots at the side of the instrument.
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Page 59: Laboratory Conditions
16 A. See rating plate (page 4-5). The iCAP Q instrument must have a separate “clean” line leading to a main fuse to guarantee disturbance-free operation. Gas Supply The iCAP Q system requires argon gas to generate the inductively coupled plasma and for controlling internal functions with the aid of pneumatics. -
Page 60: Laboratory Temperature
▲ Altitude The iCAP Q instrument is designed for indoor use at an altitude of up to 2000 m (6562 ft) above sea level. For altitudes above 2000 m, contact Thermo Fisher Scientific. -
Page 61: Ventilation And Fume Exhaust
▲ Airborne Noise Emission The mean value for the emission sound pressure level of the iCAP Q instrument is below 70 dB. Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B) - Page 62 System Setup Laboratory Conditions 5-10 iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific...
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Page 63: Operation
“Starting Up the System” page 6-6 • “Shutting Down the System” page 6-7 • “Getting Ready” page 6-9 • “Working with LabBooks” page 6-14 • “After Operation” page 6-16 • Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B) -
Page 64: Safety Guidelines For Operation
Operation Safety Guidelines for Operation Safety Guidelines for Operation When operating the iCAP Q system, please pay attention to the following general safety guidelines. WARNING Toxic Gases. Danger of intoxication. Toxic gases are released that might lead to severe bodily harm when the plasma exhaust is not connected to an exhaust system or the spray chamber is disassembled. - Page 65 CAUTION Rotating Parts Hazard. Danger of injuries. The peristaltic pump rollers can pull in hair, clothing, ties and other loose objects. Stay clear from the peristaltic pump during operation. Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B)
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Page 66: System Controls
Figure 6-1. ICP-MS front with system control LEDs System Status LEDs Three LEDs at the front of the instrument (see Figure 6-1) indicate the status of the main items of the iCAP Q MS. Table 6-1 lists their meaning. Table 6-1. -
Page 67: Power Panel
Figure 6-2. iCAP Q MS front with main power switch detail In the OFF position, the power to the instrument and the forepump is switched off. In the ON position, power is supplied to the instrument. -
Page 68: Starting Up The System
4. If the system was vented, the detector should be calibrated regardless of whether it was changed or not. The Get Ready procedure can now be started, see “Getting Ready” page 6-9. iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific... -
Page 69: Shutting Down The System
NOTICE If the plasma is not lit, start with step ▲ ❖ To shut down the instrument 1. Click inside the Experiment Editor window. The plasma is switched off. Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B) -
Page 70: Shutting Down The Instrument Only (Instrument Not Vented)
▲ ❖ To shut down the instrument 1. Click inside the Experiment Editor window. The plasma is switched off. 2. Switch the main power switch to Off position. iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific... -
Page 71: Getting Ready
Getting Ready Getting Ready Thermo Fisher Scientific provides a tool to easily start up the iCAP Q mass spectrometer. An automatic sequence can be started that switches on the plasma and will carry out a routine check of the instrument’s performance by generating a performance report. - Page 72 Figure 6-4. Experiment Editor - Example of Get Ready window 4. If required, configure a delay for warmup of the instrument. 6-10 iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific...
- Page 73 If the sensitivity test has been failed, a source autotune procedure is triggered. Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B) 6-11...
- Page 74 Get Ready procedure indicates its successful completion. If other modes have been selected in the Get Ready procedure, they will be tested once the STD mode performance report has been passed successfully. 6-12 iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific...
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Page 75: Going To Operation Status With Instrument Control
❖ To switch on the instrument 1. Open Instrument Control. 2. Click On in the iCAP Q ribbon. The start-up procedure is triggered and the plasma is lit. 3. Select the measurement mode from the drop down menu in the Measurement Mode ribbon tab. -
Page 76: Working With Labbooks
In the Browse for LabBook dialog box, select a LabBook. c. Click OK to open the LabBook. 3. The LabBook opens in a new tab of the Experiment Editor. 6-14 iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific... -
Page 77: Submitting A Labbook
The acquisition queue itself is started independently once all LabBooks to be acquired are submitted. Starting the Data Acquisition ❖ To start the acquisition queue Click in the Scheduler pane to start data acquisition. Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B) 6-15... -
Page 78: After Operation
Emptying the waste container • Run the System with Blanks After operation it is recommended to flush the iCAP Q mass spectrometer with appropriate blanks to such as diluted nitric acid or ultrapure water.This ensures that neither high amounts of analytes nor matrix stay inside the sample introduction system over a longer period of time. - Page 79 “Safety Guidelines for Troubleshooting” page 7-2 • “Error Messages” page 7-4 • • “Sensitivity Problems/No Signal” page 7-7 “Signal Drifts with Time” page 7-8 • • “Poor Signal Stability” page 7-9 Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B)
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Page 80: Troubleshooting
Instrument Control window are required. Safety Guidelines for Troubleshooting When performing troubleshooting on the iCAP Q system, please pay attention to the following general safety guidelines. CAUTION Service by the customer must be performed by trained qualified personnel only and is restricted to servicing mechanical parts. - Page 81 Thermo Fisher Scientific personnel. To ensure that the instrument is free from all electric current, always disconnect the power cords of mass spectrometer and fore vacuum pump before attempting any type of maintenance. Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B)
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Page 82: Error Messages
Low Argon Pressure not satisfied page 7-11 Low Cool Gas Flow not satisfied page 7-11 Low Exhaust Flow not satisfied page 7-12 Plasma Lit Sensor not satisfied page 7-12 iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific... -
Page 83: Plasma Not Lit
12. Make sure the plasma torch is dry. 13. Make sure the torch body is aligned correctly inside the torch holder, see “Maintaining the Torch” page 8-15. Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B) - Page 84 18. Make sure the Forward Power during ignition is 900 W or greater. 19. Make sure that the cooling water meets the conductivity requirements. If the problem remains, contact the Qtegra Administrator for further troubleshooting. iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific...
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Page 85: Sensitivity Problems/No Signal
Make sure that the cones and sample cone gasket are in good condition. If none of the above shows any improvements on the signal, contact the Qtegra Administrator for further troubleshooting. Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B) -
Page 86: Signal Drifts With Time
14. Check that the tension on the peristaltic pump tubing is correct and that the pump tubing is in good condition. If none of the above shows any improvements on the signal, contact the Qtegra Administrator for further troubleshooting. iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific... -
Page 87: Poor Signal Stability
13. Make sure that the pump speed of the Peristaltic pump is stable. 14. Make sure that the vacuum system is stable. If none of the above shows any improvements on the signal, contact the Qtegra Administrator for further troubleshooting. Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B) -
Page 88: Interlocks
To reset the Low Water Flow interlock 1. Make sure that the water cooler is switched on. 2. Make sure that the water cooling lines are properly connected. 7-10 iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific... -
Page 89: Hardware Lock Open
1. Check that the argon supply is switched on and can supply 6 bar. 2. Make sure that the gas lines are securely connected, free from kinks, and not trapped. Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B) 7-11... -
Page 90: Low Exhaust Gas Flow
Also see the readback values in the Plasma pane, Figure 7-1 page 7-4. “Plasma not Lit” page 7-5 for more information on the troubleshooting procedure. 7-12 iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific... -
Page 91: Maintenance
Maintenance Chapter 8 This chapter describes routine maintenance procedures that must be performed to ensure optimum performance of the iCAP Q mass spectrometer: “Safety Guidelines for Maintenance” page 8-2 • “General Advice for Maintenance” page 8-4 • “Servicing Plan” page 8-5 •... -
Page 92: Safety Guidelines For Maintenance
Maintenance Safety Guidelines for Maintenance Safety Guidelines for Maintenance When performing maintenance on the iCAP Q system, please pay attention to the following general safety guidelines. WARNING Toxic Gases. Danger of intoxication. Toxic gases are released that might lead to severe bodily harm when the plasma exhaust is not connected to an exhaust system or the spray chamber is disassembled. - Page 93 Thermo Fisher Scientific field service engineer. Only use fuses of the type and current rating specified. Do not use repaired fuses and do not short-circuit the fuse holder. Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B)
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Page 94: General Advice For Maintenance
Maintenance General Advice for Maintenance General Advice for Maintenance When performing maintenance on the iCAP Q mass spectrometer, observe the following advice: Accurate results can be obtained only if the system is in good • condition and properly calibrated. •... -
Page 95: Servicing Plan
Annually page 8-8 Air Filter Check fan Monthly page 8-9 Clean filter If necessary page 8-9 Instrument Clean surface If necessary page 8-7 Check warning labels Annually page 8-7 Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B) - Page 96 Annually or depending on operation condition Chiller Replace fluid bag Depending on operation see manufacturer’s condition manual Replace condenser filter Depending on operation condition Clean reservoir Depending on operation condition iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific...
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Page 97: General Maintenance Routines
Symbols on the Instrument” page 4-3 for an overview of the warning labels on the instrument. Also check the warning labels on the fore vacuum pump and the peripherals. Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B) -
Page 98: Checking Gas Lines For Leaks
5. When you cannot find a leak in the gas line, we recommend calling a Thermo Fisher Scientific field service engineer to check for gas leaks within the instrument. iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific... -
Page 99: Maintaining The Air Filter
Slightly lift up the cover. b. Pull off the cover. Figure 8-2. Open fan cover 2. Visual inspect the filter for dirt or damage. 3. Close the cover again. Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B) - Page 100 8-2. 2. Carefully pull out the filter. Figure 8-3. Remove filter 3. Clean the filter with a vacuum cleaner. 4. Insert the filter again. 5. Close the cover. 8-10 iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific...
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Page 101: Maintaining The Inlet System
To remove the nebulizer 1. Pull off the tubing. 2. Carefully turn the nebulizer counterclockwise. 3. Pull out the nebulizer. Labeled Components: 1=tubing, 2=nebulizer Figure 8-4. Inlet system with nebulizer Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B) 8-11... -
Page 102: Maintaining The Peristaltic Pump
Pinch Point Hazard. Danger of injuries. Keep hands clear from the peristaltic pump during operation. 2. Wipe the surface of the peristaltic pump rollers and tension arms with a dry cloth to remove any dust. 8-12 iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific... -
Page 103: Maintaining The Spray Chamber
Pull back the holder spring to release the spray chamber. 3. Carefully pull out the spray chamber and the elbow connector from the torch assembly by pulling out the elbow connector. Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B) 8-13... -
Page 104: Maintaining The Injector
8-11. 2. Remove the spray chamber, see “Removing the Spray Chamber” page 8-13. 3. Carefully remove the injector and the injector holder. Figure 8-5. Injector with holder 8-14 iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific... -
Page 105: Maintaining The Torch
5. Pull out the torch assembly. 6. Carefully remove the torch body from the torch holder. Labeled Components: 1=torch body, 2=gas inlet, 3=release button, 4=torch holder Figure 8-6. Torch disassembled Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B) 8-15... -
Page 106: Cleaning The Glassware
4. Allow it to air dry completely. If any components are to be stored for some time before use, they should be placed in metal-free sealed plastic bags. 8-16 iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific... -
Page 107: Maintaining The Interface
“Shutting Down the System” page 6-7. Tools The iCAP Q instrument is provided with a cone tool for easy disassembly of the cones. The cone tool is magnetic to hold the cones in place when removing them from the interface block. Figure 8-7 shows the cone tools with the cones arranged at their respective tool side. - Page 108 Figure 8-9. Sample cone and holder in cone tool d. Remove the sample cone and the cone holder from the tool. The sample cone can now be cleaned. 8-18 iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific...
- Page 109 Inserting the Sample Cone ❖ To insert the sample cone 1. Make sure that the sample cone gasket is in good condition, see Figure 8-11. Replace it if required. Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B) 8-19...
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Page 110: Maintaining The Skimmer Cone
Align the two lugs in the cone tool in the outer edge of the cone surface. c. Turn the tool counterclockwise, it will be held in place magnetically. 8-20 iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific... - Page 111 Maintaining the Skimmer Cone Insert ❖ To replace the skimmer cone insert using the insert tool 1. Align the insert tool with the holes in the skimmer cone insert. Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B) 8-21...
- Page 112 Figure 8-15. Figure 8-15. Skimmer cone insert and tool. NOTICE Make sure to mount the insert with the correct side facing the tool, see Figure 8-15. ▲ 8-22 iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific...
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Page 113: Maintaining The Extraction Lens
2. Open the interface door. 3. Turn the extraction lens assembly counterclockwise, see Figure 8-16. Figure 8-16. Turn the extraction lens 4. Pull out the extraction lens assembly, see Figure 8-17. Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B) 8-23... - Page 114 • Make yourself aware of all safety procedures in case of spillage or exposure to skin or eyes before commencing the cleaning. The acid cleaning should take place in a fume hood. 8-24 iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific...
- Page 115 Figure 8-17. Be careful not to tilt the assembly. 3. Turn the extraction lens clockwise to fix it to the extraction lens housing. Figure 8-19. Insert extraction lens Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B) 8-25...
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Page 116: Thermo Fisher Scientific Service
The Preventive Maintenance Guide provided by Thermo Fisher Scientific lists services that must be performed by a Thermo Fisher Scientific field service engineer or their representatives only. Refer to this guide for more information. 8-26 iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific... - Page 117 Additional Safety Information Chapter 9 This chapter contains excerpts from component suppliers’ documents with safety-relevant information that may concern users of the iCAP Q mass spectrometer. It contains the following topics: “Fore Vacuum Pump” page 9-2 • “Recirculating Chiller” page 9-4 •...
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Page 118: Additional Safety Information
ATEX areas. Contact the pump manufacturer if you are planning such an application. Before installing the pump, you must reliably disconnect it from the electrical power supply and prevent the pump form running up inadvertently. iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific... - Page 119 Do not smoke with PFPE on your fingers. Touch the inner sections of the pumps only while wearing clean gloves, and use clean tools; do the necessary work in clean and dry rooms. Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B)
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Page 120: Recirculating Chiller
Use caution when removing the assembly. Water-cooled units also have a fan with sharp blades, ensure that the unit is off before removing the assembly. iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific... -
Page 121: Dionex Ics-5000
Wear protective eye wear and gloves when handling the cartridge. The power supply cord is used as the main disconnect device. Make sure the socket-outlet is located near the Detector/Chromatography Module (DC) and is easily accessible. Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B) - Page 122 Additional Safety Information Dionex ICS-5000 iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific...
- Page 123 Legal Documents This chapter provides legal documents. It contains the following documentation: • “FCC Compliance Statement” page D-2 “WEEE Compliance” page D-3 • • “Declaration of Conformity” page D-4 Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B)
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Page 124: Legal Documents
Legal Documents FCC Compliance Statement FCC Compliance Statement This device complies with part 18 of the FCC rules. iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific... - Page 125 Directives, the recyclers in your country, and information on Thermo Fisher Scientific products which may assist the detection of substances subject to the RoHS Directive are available at http://www.thermoscientific.com/rohsweee. Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B)
- Page 126 Legal Documents Declaration of Conformity Declaration of Conformity iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific...
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Page 127: Glossary
12u; unit of mass for expressing masses of atoms or atomic mass (atomic mass constant). molecules. DAC Abbr. for digital-to-analog converter; a device that converts data from digital to analog form. Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B) - Page 128 HR Abbr. for High Resolution m/z mass-to-charge ratio HV high voltage Hz hertz (cycles per second) OD outside diameter ICIS™ Interactive Chemical Information System PCB printed circuit board ID inside diameter iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific...
- Page 129 WEEE European Union Waste Electrical and Electronic Equipment Directive. Provides guidelines square fit regression type: the fit is performed with a for disposal of electronic waste. second order (quadratic) function. Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B)
- Page 130 Glossary: WEEE–WEEE iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific...
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Page 131: Index
DA lens 3-10 DA plate 3-10 Dashboard 3-12 injector dashboard in-line filter 3-19 deposition, of matrix installation test 3-16 diagnosing, potential problems Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B) - Page 132 6-10 STD mode organic solvents 3-17 system control LED oxygen 3-17 System LED system status LED Peltier cooler performance report temperature peristaltic pump 8-12 coolant water 7-8–7-9 iCAP Q Operating Manual (P/N 1288090, Revision B) Thermo Fisher Scientific...
- Page 133 Vacuum LED torch vibration total dissolved solids level 7-8–7-9 tQuant 6-14 transport pallet trQuant 6-14 wall receptacle turbomolecular pump 3-12 warning labels Water Valve Closed interlock 7-11 Thermo Fisher Scientific iCAP Q Operating Manual (P/N 1288090, Revision B)
- Page 134 Thermo isher Scientific Inc. 81 Wyman Street P.O. ox 9046 Waltham, Massachussetts 02454-9046 United States www.thermoscientific.com Part of Thermo isher Scientific...
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