Thermo Scientific iCAP Q ICP-MS Manuals

Manuals and User Guides for Thermo Scientific iCAP Q ICP-MS. We have 1 Thermo Scientific iCAP Q ICP-MS manual available for free PDF download: Operating Manual

Thermo Scientific iCAP Q Operating Manual (134 pages)

Brand: Thermo Scientific | Category: Laboratory Equipment | Size: 2 MB

Table of Contents
5
Chapter 1 Using this Manual

9
- About this Manual
  9
- Typographical Conventions
  10
  - Signal Word
    10
  - Viewpoint Orientation
    10
  - Data Input
    10
  - Topic Headings
    11
- Reference Documentation
  12
Chapter 2 Scope of Delivery

13
- Standard System Components
  13
- Optional System Components
  14
Chapter 3 System Description

15
General Description

16
- Instrument Layout
  17
Sample Introduction System

18
- Peristaltic Pump
  18
- Nebulizer
  19
- Spray Chamber
  19
- Injector
  20
- Torch
  20
- Interface
  21
  - Sample Cone and Skimmer Cone
    21
  - Extraction Lens
    22
Ion Optics

23
- RAPID Lens
  23
Qcell

23
- DA Assembly
  24
Mass Analyzer

24
- Quadrupole
  24
Detector

24
Vacuum System

25
- Forepump
  26
- Turbomolecular Pump
  26
- Pressure Measurement
  26
Gas Supply

27
- Connections
  27
- Plasma and Cooling Gas
  28
- CCT Gas
  29
- Additional Gas
  31
Cooling System

33
- Connections for Water Supply
  33
- Recirculating Chiller
  34
Exhaust System

35
Connections

36
- Main Power Switch
  37
- Power Connections
  37
- Fore Vacuum Pump Connections
  38
- Connection to Computer and Peripherals
  39
Chapter 4 Safety

42
Safety Symbols and Signal Words in this Manual

42
- Observing this Manual
  42
Safety Symbols on the Instrument

43
Rating Plate

45
Intended Use

46
- Qualified Personnel
  47
Permitted Materials

47
Electrical Safety Precautions

48
Residual Hazards

49
Personal Protective Equipment

50
EMC Information

51
In Case of Emergency

52
Chapter 5 System Setup

54
- Safety Guidelines for Installation
  54
- Placing the System
  55
  - Instrument Dimensions
    55
  - Moving the Instrument
    56
  - Workbench for Instrument
    57
- Laboratory Conditions
  59
  - Power Supply
    59
  - Gas Supply
    59
  - Laboratory Temperature
    60
  - Humidity
    60
  - Ventilation and Fume Exhaust
    61
  - Vibration
    61
  - Airborne Noise Emission
    61
Chapter 6 Operation

63
Safety Guidelines for Operation

64
System Controls

66
- System Status Leds
  66
- Power Panel
  67
Starting up the System

68
Shutting down the System

69
Getting Ready

71
Working with Labbooks

76
- Loading a Labbook
  76
- Submitting a Labbook
  77
- Starting the Data Acquisition
  77
After Operation

78
Chapter 7 Troubleshooting

80
General Remarks

80
- Administrator/User
  80
Safety Guidelines for Troubleshooting

80
Error Messages

82
- Plasma Not Lit
  83
Sensitivity Problems/No Signal

85
Signal Drifts with Time

86
Poor Signal Stability

87
- Interlocks
  88
  - Door Lock
    88
  - Interface Temperature
    88
  - Low Water Flow
    88
  - Hardware Lock Open
    89
  - Water Valve Closed
    89
  - Low Argon Pressure
    89
  - Low Cool Gas Flow
    89
  - Low Exhaust Gas Flow
    90
  - Plasma Lit Sensor
    90
Chapter 8 Maintenance

91
Safety Guidelines for Maintenance

92
General Advice for Maintenance

94
- Returning Parts
  94
Servicing Plan

95
General Maintenance Routines

97
Maintaining the Air Filter

99
Maintaining the Inlet System

101
- Maintaining the Nebulizer
  101
- Maintaining the Peristaltic Pump
  102
- Maintaining the Spray Chamber
  103
- Maintaining the Injector
  104
- Maintaining the Torch
  105
- Cleaning the Glassware
  106
Maintaining the Interface

107
- Tools
  107
- Maintaining the Sample Cone
  107
- Maintaining the Skimmer Cone
  110
- Maintaining the Extraction Lens
  113
Thermo Fisher Scientific Service

116
- Health and Safety Form
  116
- Services to be Performed by Thermo Fisher Scientific Service Only
  116
Chapter 9 Additional Safety Information

118
- Fore Vacuum Pump
  118
- Recirculating Chiller
  120
- Dionex ICS-5000
  121
Legal Documents

124
Glossary

127
Index

131

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More Thermo Scientific Manuals

Thermo Scientific iCAP Q ICP-MS Manuals

Thermo Scientific iCAP Q Operating Manual (134 pages)

Table of Contents

Chapter 1 Using this Manual

Chapter 2 Scope of Delivery

Chapter 3 System Description

General Description

Sample Introduction System

Ion Optics

Qcell

Mass Analyzer

Detector

Vacuum System

Gas Supply

Cooling System

Exhaust System

Connections

Chapter 4 Safety

Safety Symbols and Signal Words in this Manual

Safety Symbols on the Instrument

Rating Plate

Intended Use

Permitted Materials

Electrical Safety Precautions

Residual Hazards

Personal Protective Equipment

EMC Information

In Case of Emergency

Chapter 5 System Setup

Chapter 6 Operation

Safety Guidelines for Operation

System Controls

Starting up the System

Shutting down the System

Getting Ready

Working with Labbooks

After Operation

Chapter 7 Troubleshooting

General Remarks

Safety Guidelines for Troubleshooting

Error Messages

Sensitivity Problems/No Signal

Signal Drifts with Time

Poor Signal Stability

Chapter 8 Maintenance

Safety Guidelines for Maintenance

General Advice for Maintenance

Servicing Plan

General Maintenance Routines

Maintaining the Air Filter

Maintaining the Inlet System

Maintaining the Interface

Thermo Fisher Scientific Service

Chapter 9 Additional Safety Information

Legal Documents

Glossary

Index

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Thermo Scientific Categories