Related Manuals for Thermo Scientific Dionex ICS-900
Summary of Contents for Thermo Scientific Dionex ICS-900
- Page 1 Dionex ICS-900 Ion Chromatography System Installation and Quick Start Instructions Document No. 065214 Revision 02 January 2012...
- Page 2 © 2012 by Thermo Fisher Scientific Inc. All rights reserved. Chromeleon, Dionex AMMS, and Dionex CMMS, are registered trademarks of Thermo Fisher Scientific Inc. in the United States. Microsoft, Windows 2000, and Windows XP are registered trademarks of Microsoft Corporation in the United States and other countries.
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Page 3: Facility Requirements
Deionized Water ASTM Type I (18-megohm) 2. Using the cardboard side handles, carefully filtered, deionized water for lift the Dionex ICS-900 out of the box (see eluent and regenerant Figure 2) and set it on the workbench. Additional Documentation... - Page 4 5. Inspect the Dionex ICS-900 for any shipping damage. Connect a Thermo Scientific Dionex AS Autosampler (Optional) Waste Line 1. Place the AS to the left of the Dionex ICS-900 Autosampler Needle Seal on the workbench. Line 2. Route the needle seal line that extends from the inject port in the AS through the Figure 4.
- Page 5 ICS-900 on the workbench. screw. 2. Route the outlet line from the AS40 through the Dionex ICS-900 left side slot to the When attaching wires to the connector injection valve. plug, be careful not to allow stray strands of wire to short to the adjoining 3.
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Page 6: Install The Software
Dionex ICS-900 Installation and Quick Start Instructions Install the Software Chromeleon CD-ROM and double-click autorun. If you purchased Chromeleon or Chromeleon 6. When asked whether to add the Server Xpress and a PC from Thermo Fisher Scientific, Monitor program to the Startup group, select omit this section and go directly to “Start the... - Page 7 b. Accept the default option (Install the 3. Click the Preferences button and select the software automatically) and click License tab (see Figure 11). Next>. It is not necessary to insert a hardware installation CD-ROM. 4. After installing the software, the wizard displays a screen similar to the example in Figure Figure 11.
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Page 8: Connect To The Pc
Dionex ICS-900 Installation and Quick Start Instructions To connect the Dionex ICS-900 directly to the If the Server Monitor icon is not on the Windows taskbar, follow these steps to start the Chromeleon server: 1. Locate the USB cable (P/N 960777) provided in the Dionex ICS-900 Ship Kit. -
Page 9: Connect The Power Cord
To connect the Dionex ICS-900 to an external SHOCK HAZARD—To avoid electrical hub: shock, use a grounded receptacle. Do not operate the Dionex ICS-900 or The Dionex ICS-900 Ship Kit includes one USB connect it to AC power mains without cable an earthed ground connection. - Page 10 If a Microsoft Windows message box asks for the USB configuration file (cmwdmusb.inf), it indicates that you connected the Dionex ICS-900 to the PC and turned on the Dionex ICS-900 power before installing Chromeleon or Figure 16. Found New Hardware Wizard Chromeleon Xpress.
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Page 11: Configure Devices
1. In the Server Configuration, right-click the Dionex ICS-900 device in the timebase and select Properties. Figure 18. USB Auto Configuration Wizard: 2. Verify that the correct device is assigned to... - Page 12 Dionex ICS-900 Installation and Quick Start Instructions If the timebase includes an AS40 or no 4. Select the TTL and relay output settings: autosampler, the Controlled By setting a. On the Dionex ICS-900 Properties dialog must be Dionex ICS-900 (see Figure 21).
- Page 13 24). Default Panel Tabset on the toolbar to display the panel tabset. Figure 24. Dionex ICS-900 Control panel on the panel tabset NOTE When the Dionex ICS-900 Control panel is opened as part of the panel tabset, controls for an AS40 Automated Sampler are included, even if one is not present.
- Page 14 For anions, verify that the cap is labeled and the line ANION REGEN BOTTLE OUT NOTE To avoid staining the Dionex ICS-900, be extends to the bottom of the bottle. careful not to spill TBAOH on the instru- • For cations, verify that the cap is labeled ment.
- Page 15 Connect Bottle Lines Set Up Waste Lines Connect the liquid lines from the Dionex ICS-900 1. Untape the coiled waste and liquid lines from to the corresponding lines exiting the eluent and the rear panel. regenerant bottles (see Figure 25).
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Page 16: Set The Eluent Level
Dionex ICS-900 Installation and Quick Start Instructions Set the Eluent Level Prime the Pump On the Dionex ICS-900 Control panel, move the The priming procedure for a new pump consists of Eluent Remaining slider to indicate the volume two parts:... - Page 17 From cell outlet 2. Direct the line to a waste container. GUARD IN To pump inlet 3. On the Dionex ICS-900 Control panel, set the flow rate to 1 mL/min. Backpressure Coil Regenerant (1 or 2, depending on 4. Start the pump and let it run for 15 minutes.
- Page 18 COL IN Backpressure Coil waste container. (Connect 1 or 2, depending on flow rate) 7. On the Dionex ICS-900 Control panel, set the flow rate to the recommended rate for the Figure 32. Dionex ICS-900 with columns and column. suppressor 8.
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Page 19: Equilibrate The System
0.3 to 0.5 mL/min 1 (red) systems that do not include a guard column. Expect the Dionex ICS-900 system pressure Less than 0.3 mL/min 2 (red) (with a guard column) to be 15% to 20% 2. - Page 20 Dionex ICS-900 Installation and Quick Start Instructions Set Up an Application 4. Click Next>. 5. Under Generate program and method files, Application templates let you quickly get started click in a new sequence via Sequence running. This section explains how to use an...
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Page 21: Run The Sequence
To save the sequence: Figure 36 shows the Application Wizard after a sample has been defined. 1. Enter a Sequence Name and specify where to save the sequence (see Figure 38). Figure 36. Example Application Wizard: Figure 38. Example Application Wizard: Unknown Samples Saving the sequence 3. -
Page 22: Installation Troubleshooting
Windows message box appears asking for a USB configuration file (cmwdmusb.inf). Possible Cause: The USB cable was connected to the PC and the Dionex ICS-900 power turned on before Chromeleon or Chromeleon Xpress was Figure 40. Loaded sequence installed. - Page 23 Connected the backpressure coils; verified that the correct type and number are installed Checklist Filled the regenerant line Unpacked the Dionex ICS-900; checked for Equilibrated the system damage and verified that all items were received Connected the autosampler (if used) ...
- Page 24 Dionex ICS-900 Installation and Quick Start Instructions Doc. 065214-02 1/12...
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