Thermo Scientific Dionex ICS-5000+ Installation Instructions Manual
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Thermo Scientific Dionex ICS-5000+ Installation Instructions Manual

Thermo Scientific Dionex ICS-5000+ Installation Instructions Manual

Ion chromatography system
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Dionex ICS-5000
Ion Chromatography
System Installation Instructions
Document No. 065447
Revision 02
December 2014

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Summary of Contents for Thermo Scientific Dionex ICS-5000+

  • Page 1 Dionex ICS-5000 Ion Chromatography System Installation Instructions Document No. 065447 Revision 02 December 2014...
  • Page 2 © 2014 Thermo Fisher Scientific Inc. All rights reserved. Chromeleon is a registered trademark of Thermo Fisher Scientific Inc. in the United States. Microsoft and Windows are registered trademarks of Microsoft Corporation in the United States and other countries. The following are registered trademarks in the United States and possibly other countries: KIMWIPES is a registered trademark of Kimberly-Clark Corporation.

  • Page 3: Table Of Contents

    Contents 1 • Introduction Overview ..........1 Related Documentation .
  • Page 4 Dionex ICS-5000 Installation Instructions 3 • System Setup System Setup Checklist ........27 Connecting the Power Cords .
  • Page 5 Contents 3.9.2 Starting the Instrument Controller Service or Server ..49 3.9.3 Installing the USB Device Drivers ....50 3.9.4 Configuring the Modules in Chromeleon .
  • Page 6 Dionex ICS-5000 Installation Instructions 4.1.9 Filling and Flushing the ED Liquid Path ....78 4.1.10 Flushing and Conditioning the Electrolytic Devices ..79 4.1.11 Flushing and Installing the Columns .
  • Page 7 Contents A.1.3 Pressurizing the Eluent Reservoir ....124 Replumbing the Seal Wash System (DP only) ....125 B •...
  • Page 8 Dionex ICS-5000 Installation Instructions C • Networking Chromeleon 6.8 Computers Setting Up a Shared Datasource ......158 C.1.1 Setting Up a Shared Datasource on a Workgroup .

  • Page 9: Introduction

    (RFIC-EG Configurations for both capillary IC and analytical IC applications are described. Analytical IC applications can be configured with either standard bore or microbore plumbing. Installation instructions for the following Thermo Scientific modules and components are included: • Dionex ICS-5000 Dual Pump (DP) •...

  • Page 10: Related Documentation

    Dionex ICS-5000 Installation Instructions Related Documentation In addition to this manual, the following documents are provided on the Thermo Scientific Reference Library DVD (P/N 053891). • Dionex ICS-5000 Ion Chromatography System Operator’s Manual (Document No. 065447) • Dionex ICS Series Photodiode Array Detector Operator’s Manual (Document No.
  • Page 11 1 • Introduction Indicates that the function or process of the instrument may be impaired. Operation does not constitute a hazard. Messages d'avertissement en français Signale une situation de danger immédiat qui, si elle n'est pas évitée, entraînera des blessures graves à mortelles. Signale une situation de danger potentiel qui, si elle n'est pas évitée, pourrait entraîner des blessures graves à...

  • Page 12: Facility Requirements

    Dionex ICS-5000 Ion Chromatography System Operator’s Manual (Document No. 065446) for specifications. The manual is provided on the Thermo Scientific Reference Library DVD (P/N 053891). • Make sure the installation site has enough power outlets for all system components.
  • Page 13 1 • Introduction • For eluent generation, or when manually preparing eluent and regenerant, use ASTM Type I (18 megohm-cm) filtered and deionized water that meets the specifications listed in Table 1-1. Contaminant Specification Ions–Resistivity >18.0 (megohm-cm) Organics–TOC <10 ppb Iron/Transition Metals* <1 ppb Pyrogens...

  • Page 14: Configurations

    Capillary column set • Dionex AS-AP • For RFIC-EG: EG with one capillary Thermo Scientific Dionex EGC (Dionex EGC) and one capillary Thermo Scientific Dionex Continuously Regenerated Trap Column (Dionex CR-TC) • Single-Analysis Capillary IC or RFIC-EG System with •...
  • Page 15 TC with one injection valve and one Variable Wavelength analytical column set Detector, Photodiode Array • One detector: Thermo Scientific Dionex ICS Detector, or Mass Series Variable Wavelength Detector Spectrometer (Dionex VWD), Thermo Scientific Dionex ICS Series Photodiode Array Detector ™...
  • Page 16 Dionex EGC For detailed plumbing diagrams for these configurations, refer to Chapter 3, “Configurations,” in Dionex ICS-5000 Ion Chromatography System Operator’s Manual (Document No. 065446). The manual is provided on the Thermo Scientific Reference Library DVD (P/N 053891). Doc. 065447-02 12/14...

  • Page 17: Fitting And Tube Connection Guidelines

    1 • Introduction Figure 1-1 illustrates a typical dual-analysis IC system. Dionex ICS Series AS-AP Autosampler Dionex ICS-5000 Dual Pump (DP) Dionex ICS-5000 Detector/ Chromatography Module Dionex ICS-5000 Eluent Generator (EG) Figure 1-1. Dionex ICS-5000 System for Dual-Analysis RFIC-EG Fitting and Tube Connection Guidelines Follow these guidelines when connecting tube fittings in the Dionex ICS- 5000 system.

  • Page 18: Connecting High-Pressure Tube Fittings

    Dionex ICS-5000 Installation Instructions substitute different tubing. This tubing is precision cut at the factory, using a specialized cutter. Precision cut tubing is included in the Dionex IC Cube Tubing Kit (P/N 072186). 1.6.1 Connecting High-Pressure Tube Fittings 1. Install the fitting bolt and ferrule onto the tubing. Position the ferrule at least 2 mm (0.1 in) from the end of the tubing (see Figure 1-2).

  • Page 19: Tightening High-Pressure Fittings

    1 • Introduction 1.6.2 Tightening High-Pressure Fittings 1. Use your fingers to tighten the fitting bolt as tight as you can. 2. After finger-tightening, use a wrench to tighten the fitting an additional three-quarter turn (270 degrees). 3. If leaks occur, replace the fitting bolt (P/N 074449), ferrule (P/N 074373), and tubing.
  • Page 20 Dionex ICS-5000 Installation Instructions Doc. 065447-02 12/14...

  • Page 21: Unpacking Instructions

    2 • Unpacking Instructions Unpacking Guidelines • Check the shipping containers for any external signs of damage. If a container shows signs of damage, contact Technical Support for Dionex products immediately. In the U.S. and Canada, call 1-800-346-6390. Outside the U.S. and Canada, call the nearest Thermo Fisher Scientific office.

  • Page 22: Unpacking The Dionex As-Ap

    Dionex ICS-5000 Installation Instructions Unpacking the Dionex AS-AP Two or more persons must lift the Dionex AS-AP, which weighs more than 23 kg (50 lb). Lift the Dionex AS-AP only from each side of the cabinet bottom. Lifting from the front door will damage the door hinges. Au moins deux personnes peuvent soulever l'Dionex AS-AP, qui pèse plus de 23 kg (50 lb).
  • Page 23 2 • Unpacking Instructions 2. Lift up the shipping container to remove it (see Figure 2-2), and then set the container aside. Remove the top foam packing insert. Figure 2-2. Lift up the shipping container 3. Remove the Ship Kit box from the top of the module Ship Kit (see...
  • Page 24 Dionex ICS-5000 Installation Instructions 4. Remove the foam packing cage (see Figure 2-4). 5. With two or more persons, grasp each side of the Dionex AS-AP cabinet bottom, lift up the module, and then place it on the bench. 6. Remove the polyethylene bag the module is shipped 7.
  • Page 25 2 • Unpacking Instructions Foam Insert Figure 2-6. Dionex AS-AP with foam insert removed 9. Unpack the Dionex AS-AP Ship Kit (P/N 074929) (see Figure 2-7 Figure 2-8). 10. Place the items in a convenient location and check them against the packing list (see Figure 2-9).
  • Page 26 Dionex ICS-5000 Installation Instructions Figure 2-8. Ship Kit items removed from box Figure 2-9. Ship Kit items unpacked Save the shipping container and all other shipping materials for later use. Should it be necessary to return the Dionex AS-AP during the warranty period, Thermo Fisher Scientific recommends repacking the autosampler in the original shipping container.

  • Page 27: Unpacking The Dionex Ics-5000 + Modules

    2 • Unpacking Instructions Unpacking the Dionex ICS-5000 Modules This section contains step-by-step guidelines for unpacking the Dionex ICS- 5000 modules. Although the Dionex ICS-5000 Eluent Generator is pictured here, the procedure is the same for the other modules. Unpack modules in the order specified in Section 2.1.
  • Page 28 Dionex ICS-5000 Installation Instructions 2. Remove the Ship Kit from the shipping container (see Figure 2-11). 3. Using the handholds in the cardboard cradle, remove the module from the shipping container. Figure 2-11. Ship Kit packed with module (EG module shown) 4.

  • Page 29: Installing The Safety Support Bracket

    2 • Unpacking Instructions Installing the Safety Support Bracket The safety support bracket performs the following functions: • Stabilizes the system and prevents modules from tipping over • Creates enough space between the DC and the adjacent module to ensure proper ventilation It is especially important to install the bracket if a monitor NOTE...
  • Page 30 Dionex ICS-5000 Installation Instructions 3. Tighten the captive thumbscrews. Safety Support Bracket DP/SP Figure 2-13. Safety Support Bracket Installed on Module Rear Panels (P/N 062225 for a Standard DC Shown) Doc. 065447-02 12/14...

  • Page 31: Removing The Pump Shipping Screws (Optional)

    2 • Unpacking Instructions Removing the Pump Shipping Screws (Optional) For easier access to pump components during initial installation or when performing service procedures, remove the five red shipping screws on the pump component panel. The component panel can then be pulled forward to the front of the pump compartment, using one of the handles.

  • Page 32: Unpacking The Computer

    Dionex ICS-5000 Installation Instructions Unpacking the Computer Remove the computer and all documentation from the computer box and place them on a workbench. Installing the Computer Configuration options include: • Desktop or notebook PC with the Chromeleon 7 Chromatography Data System (release 7.1 SR2 or later) or Chromeleon 6.8 Chromatography Data System (release 6.8 SR12 or later).

  • Page 33: Unpacking Consumable Devices

    2 • Unpacking Instructions Unpacking Consumable Devices Remove the consumable devices (for example, Dionex EGC, CR-TC, suppressor, and CRD) from their shipping boxes. Save the EGC shipping container; it may be required for storage or disposal of the EGC. The Dionex EGC contains one of the following: a corrosive base (KOH, LiOH, or NaOH), a corrosive acid (MSA), or a concentrated solution.
  • Page 34 Dionex ICS-5000 Installation Instructions Doc. 065447-02 12/14...

  • Page 35: System Setup

    3 • System Setup This chapter provides instructions for setting up the system hardware and Chromeleon software. After completing the setup steps, go on to the plumbing instructions in Chapter Notes on USB Connections Always install Chromeleon before connecting the USB (Universal Serial Bus) cables and turning on the power to the modules and the PC.

  • Page 36: Connecting The Power Cords

    Dionex ICS-5000 Installation Instructions Connecting the Power Cords 1. Locate the power cords for the Dionex ICS-5000 system in the box that contains accessory parts. 2. Verify that the main power switch on the rear panel of each module is turned off.

  • Page 37: Plugging In The Dionex Egc And Cr-Tc (Rfic-Eg System Only)

    3 • System Setup Plugging in the Dionex EGC and CR-TC (RFIC-EG System Only) If your system does not include an eluent generator, you can NOTE skip this section and go on to either: • Installing a DC for capillary IC (Section 3.4) •...
  • Page 38 Dionex ICS-5000 Installation Instructions 4. The Dionex EGC cable is attached to the cartridge with a cable tie (see Figure 3-2). Cut the cable tie to release the cable. Cable Tie (cut to release the cable) Cable Figure 3-2. Dionex EGC Cable Attached to Cartridge (Capillary Version Shown) 5.
  • Page 39 3 • System Setup 6. If you are installing system 1: a. Orient the Dionex CR-TC with the port (yellow label) ELUENT IN toward the front of the EG and push the Dionex CR-TC firmly onto the ball studs on the left side of the EG. b.

  • Page 40: Setting Up The Dc For Capillary Ic Applications

    Dionex ICS-5000 Installation Instructions If you are installing a DC for capillary IC, go on to Section 3.4. If you are installing a DC for analytical IC, go on to Section 3.5. If you are installing a TC, go on to Section 3.6.

  • Page 41: Installing The Ic Cube Component Cartridges

    3 • System Setup 3.4.1 Installing the IC Cube Component Cartridges Capillary The Dionex IC Cube houses three removable component cartridges and one column tray for running capillary IC applications. For reference, Figure 3-6 shows an IC Cube after these items have been installed. CRD Cartridge or CRD Bypass Cartridge Suppressor Cartridge or...

  • Page 42: Installing The Eg Degas, Crd, Or Ces Cartridge

    Dionex ICS-5000 Installation Instructions 3.4.2 Installing the EG Degas, CRD, or CES Cartridge Capillary 1. To install an EG degas cartridge: a. Remove the cap from the regenerant port on the rear of the cartridge. Slide the cartridge into the right-most slot of the Dionex IC Cube (see Figure 3-6).
  • Page 43 3 • System Setup 2. Insert the capillary CD (P/N 072041) or ED (P/N 072042) into the upper compartment of the DC (see Figure 3-5). • For a single-system configuration, it does not matter on which side of the compartment the detector is installed. Typically, the left side is used.

  • Page 44: Setting Up The Dc For Analytical Ic Applications

    Dionex ICS-5000 Installation Instructions Setting Up the DC for Analytical IC Applications Figure 3-7 is an example of the interior of the DC after the components for two analytical IC systems have been installed. Upper Compartment Automation Manager Components Electrochemical Detector and Cell Conductivity Detector and...

  • Page 45: Installing The Suppressor In The Dc

    3 • System Setup 4. Insert the detector into the compartment and push firmly to plug the electrical plug on the back of the detector into the receptacle on the rear wall of the DC compartment. You should hear a click when the detector is fully seated. 5.

  • Page 46: Setting Up The Tc

    Dionex ICS-5000 Installation Instructions 5. If you are installing an autosampler, go on to Section 3.7. If not, go on to Section 3.8. Setting Up the TC The TC cannot be configured for capillary IC applications. NOTE 3.6.1 Installing the Temperature Stabilizer in the TC (Optional) Four column brackets are installed in the TC at the factory.
  • Page 47 3 • System Setup • When mounted on the top edge, the temperature stabilizer inlet and outlet are on the left side. When mounted on the bottom edge, the inlet and outlet are on the right side. Determine which orientation will allow you to minimize the length of connections to other system components.

  • Page 48: Installing The Columns In The Tc

    Refer to the column manual for detailed installation and start-up instructions. Column manuals are provided on the Thermo Scientific Reference Library DVD (P/N 053891). 2. Remove the guard column and separator column from their boxes. 3. Remove the fitting plugs from the ends of each column.

  • Page 49: Installing The Tc Column Id (Identification) System

    3 • System Setup 3.6.3 Installing the TC Column ID (Identification) System The TC electronic column ID system lets you store important column properties on a column ID chip card. To implement the ID system, you must complete all of the following tasks: •...

  • Page 50: Connecting The Autosampler

    Connecting the Autosampler Sample Transfer Line 1. Place the autosampler to the left of the DC (or TC) on the workbench. A Thermo Scientific Dionex AS-DV Autosampler can be placed on top of the DC, if preferred. 2. Route the sample transfer line from the autosampler to the injection valve in the DC (or TC).

  • Page 51: Connecting The Injection Valve Waste Line

    SAMPLE OUT In an analytical system, port 6 is labeled 3. Route the other end to waste. For a Thermo Scientific Dionex ICS Series AS-AP Autosampler 1. For a capillary system: Capillary a. Locate the following items in the Dionex AS-AP Ship Kit (P/N 074929): •...
  • Page 52 Dionex ICS-5000 Installation Instructions 3. Connect one end of the waste line to port 6 on the injection valve. For a capillary system with a two-piece waste line, connect the black tubing to the injection valve. In a capillary system, port 6 is labeled .

  • Page 53: Connecting Modules To The Computer

    3 • System Setup 5. To ensure the waste lines do not interfere with needle arm movement in the Dionex AS-AP, secure the excess tubing with the flexible tubing tie in the slotted compartment next to the needle (see Figure 3-16).

  • Page 54: Usb Compatibility

    Dionex ICS-5000 Installation Instructions • The DP, EG, SP, and TC Ship Kits include a 1 m (3 ft) USB cable (P/N 063246). The USB standard limits the USB cable length to 5 m (5.5 yds). Each USB module can be separated from the PC by no more than five hubs. Thus, each USB module can be located no more than 30 m (32 yds) from the PC.

  • Page 55: Usb Connection Examples

    3 • System Setup Examples of valid connections: Connect a DC (Level 1) to:  Another device with a USB 2.0 hub  Level 0 An external USB 2.0 hub Dongle  The computer Do not connect the DC to a device with a USB 1.1 hub.
  • Page 56 Dionex ICS-5000 Installation Instructions USB Cables AS-AP *Internal USB 2.0 hub Figure 3-19. Example Connections: Multiple Modules Connected via Internal Hubs If the number of Dionex ICS-5000 modules exceeds the number of available USB ports, connect the modules to the system with an external USB 2.0 hub (see Figure 3-20).

  • Page 57: Setting Up The Chromatography Software

    To install Chromeleon software and the software license, follow the instructions in the appropriate installation guide. The guides are provided on the Thermo Scientific Reference Library DVD (P/N 053891). • For Chromeleon 7, refer to Chromeleon 7 Installation Guide. •...

  • Page 58: Installing The Usb Device Drivers

    Dionex ICS-5000 Installation Instructions Starting the Chromeleon 6.8 Server On the Windows taskbar, right-click the Chromeleon icon ( in the system tray and click Start Server. The icon changes to gold ( ) to indicate that the Chromeleon Server is starting. When the Chromeleon Server is running (idle), the icon changes to gray ( If the Chromeleon icon is not on the Windows taskbar, click Start >...

  • Page 59: Configuring The Modules In Chromeleon

    For instructions on how to manually create a timebase in Chromeleon 6.8, refer to the Chromeleon 6.8 Help or to Installing Chromeleon with a Dionex Ion Chromatograph (Document No. 031883). The software installation manuals are provided on the Thermo Scientific Reference Library DVD (P/N 053891). Doc. 065447-02 12/14...

  • Page 60: Selecting Configuration Properties

    Dionex ICS-5000 Installation Instructions 3.9.5 Selecting Configuration Properties When you add a module to an instrument or timebase, default configuration properties are selected. For each module, verify the default settings and select other settings as required. To open a configuration properties dialog box, right-click the module in the instrument or timebase and click Properties.
  • Page 61 3 • System Setup DC Configuration Properties Capillary On the IC Cubes tab page, double-click the IC Cube name. The Device Configuration dialog box appears (see Figure 3-22). Figure 3-22. IC Cube Configuration Example • Verify that the IC Cube is assigned to the correct instrument (or timebase).
  • Page 62 Dionex ICS-5000 Installation Instructions instrument (or timebase) and that it is linked to the pump (see Figure 3-23). Figure 3-23. IC Cube Suppressor Configuration Example Doc. 065447-02 12/14...
  • Page 63 3 • System Setup • Click Configure next to Valve and verify that the IC Cube injection valve is assigned to the correct instrument (or timebase) (see Figure 3-24). For Controlled by, verify that AS is selected. This setting assigns control of the valve to the autosampler.
  • Page 64 Dionex ICS-5000 Installation Instructions DC Configuration Properties On the High Pressure Valves tab page (see Figure 3-25), under Controlled by, verify that AS is selected for InjectValve_1 (and InjectValve_2, if installed). This setting assigns control of the injection valve in the DC to the autosampler.
  • Page 65 3 • System Setup TC Configuration Properties On the Components tab page (see Figure 3-26): • If the TC valve is connected to a Dionex AS-AP or Dionex AS-DV, select the controlled by AS check box for the valve (Left Valve and/or Right Valve).

  • Page 66: Starting The Chromeleon Client

    Dionex ICS-5000 Installation Instructions 3.9.6 Starting the Chromeleon Client 1. Start the Chromeleon client: • To start Chromeleon 7, click Start > All Programs > Thermo Chromeleon 7 > Chromeleon 7. • To start Chromeleon 6.8, click Start > All Programs > Chromeleon >...

  • Page 67: Connecting Drain Lines

    3 • System Setup • To display the Chromeleon 6.8 panel tabset, click View > Default Panel Tabset or click the toolbar button to display the panel tabset. Figure 3-28. Example Chromeleon 6.8 Panel Tabset 3.10 Connecting Drain Lines Any leaks or condensation that may occur are routed to the drain port on the rear of each module.
  • Page 68 Dionex ICS-5000 Installation Instructions 3. Place the open end of each hose into a waste container or appropriate drain. For correct drainage, make sure drain hoses lay flat on the bench and are not bent, pinched, or elevated at any point. Do not allow the ends of the drain hoses to be submerged in waste liquid.
  • Page 69 3 • System Setup The fittings and shorter tubing pieces are bagged NOTE together in the Ship Kit PTFE Tubing (5 pieces) Elbow Fitting (3) Corrugated Drain Hose Fitting Union Fitting Vent Plug Figure 3-29. Low-Temperature DC Drain Line Parts 2.
  • Page 70 Dionex ICS-5000 Installation Instructions Figure 3-31. Drain Line Routed to Side of Bench Figure 3-32. Drain Line Routed to Front of Bench 3. Determine how you want to route the drain line to the waste container or drain. Then, lay out parts on the bench to determine which parts will be required.
  • Page 71 3 • System Setup you need. Make sure to cut the tubing squarely to ensure a good connection between the tubing and the fittings. 4. To assemble the rigid drain line: a. Push the PTFE tubing into the fittings. b. Verify that the black o-ring inside the drain port opening on the DC is fully seated in the groove, and then push the short length of tubing straight into the drain port.

  • Page 72: Degassing The Water

    Dionex ICS-5000 Installation Instructions Removing a Tube from a Fitting After a tube has been pushed fully into a fitting, it is locked in place. To remove the tube, use the fingers of one hand to press the rubber ring on the fitting and simultaneously pull out the tubing with the other hand.
  • Page 73 IQ. For eluent preparation instructions, refer to the manual for the column that will be installed. Column manuals are provided on the Thermo Scientific Reference Library DVD (P/N 053891). 2. Place the reservoir in the Dionex ICS-5000 Eluent Organizer (EO): •...
  • Page 74 Dionex ICS-5000 Installation Instructions 3. Install an end-line filter (P/N 045987) on each reservoir’s eluent line (if they are not already installed). The filters are in the pump ship kit: Pump Ship Kit Part Number DP Ship Kit, Dual-Capillary 072112 DP Ship Kit, Capillary and Analytical 072111 SP Ship Kit, Capillary...

  • Page 75: Setting Up The Piston Seal Wash System

    3 • System Setup 9. The DP/SP does not require pressurized eluent reservoirs. However, Thermo Fisher Scientific recommends pressurizing reservoirs with helium or nitrogen under the following circumstances: • When using eluents that are sensitive to contamination. • When combining aqueous and nonaqueous components (for example, water and acetonitrile).

  • Page 76: 3.13.2 Activating The Piston Seal Wash Function

    Dionex ICS-5000 Installation Instructions 2. Place the cap on the reservoir and tighten fingertight. 3. Insert the reservoir into the holder on the component panel. 4. Check that the tubing is engaged in the peristaltic pump (see Figure 3-34). If it is not, lift the lever on the peristaltic pump to the right, insert the tubing neatly between the lever and the rotor, and release the lever to secure the tubing.

  • Page 77: Priming The Pump

    3 • System Setup 3.14 Priming the Pump 1. Before priming, check that the following tasks have been done: • Eluent reservoirs are filled. • Reservoir caps are installed and hand-tightened. • Liquid lines from the pump to the reservoir caps are connected. •...

  • Page 78: Checking The Conductivity Of The Water

    Dionex ICS-5000 Installation Instructions 6. Set the Purge Rate to 2.0 mL/min for a capillary IC pump and 6.0 mL/min for an analytical IC pump. Set the Duration to 1800 s. 7. Click the Prime button. A warning message asks you to verify that the purge (priming) valve is open.

  • Page 79: System Plumbing

    4 • System Plumbing This chapter provides instructions for plumbing the Dionex ICS-5000 system. Instructions for setting up and installing electrolytic devices and columns and equilibrating the system are also included. • Instructions for plumbing a capillary IC system begin below. •...
  • Page 80 Dionex ICS-5000 Installation Instructions Pre-Assembled Tubing Chain A pre-assembled tubing chain is included in the Dionex ICS-5000 IC Cube Ship Kit (P/N 072003). The chain includes several lengths of tubing connected to each other with unions (see Figure 4-1). The tubing will be used to plumb the pump outlet, Dionex EGC, CR-TC, and EG degas.

  • Page 81: System Plumbing Checklists

    4 • System Plumbing 4.1.2 System Plumbing Checklists Capillary The system plumbing steps and the order in which they are performed vary slightly, depending on the installed detector. The following checklists outline the steps for each detection type. CD System Plumbing Checklist for Capillary IC Page ...

  • Page 82: Installing The Trap Column For Koh-Based Separations

    4.1.3 Installing the Trap Column for KOH-Based Separations Capillary Installation of a Thermo Scientific Dionex ASTC 500 Anion Trap Column (P/N 085359) is recommended for all KOH-based separations performed on capillary systems. The Dionex ASTC 500 trap column removes trace contaminants from deionized water.

  • Page 83: Connecting The Pump Outlet

    4 • System Plumbing 4.1.4 Connecting the Pump Outlet Capillary If you did not install the Dionex ASTC 500 Anion Trap Column (see Section 4.1.3), connect the pump outlet tubing directly to the pump pulse damper. On the pre-assembled tubing chain (see Figure 4-1), connect the black PEEK tubing labeled...
  • Page 84 Dionex ICS-5000 Installation Instructions 3. Use the two tubing assemblies to connect the injection valve ELUENT OUT port to the cell port (see Figure 4-3). Fill and flush regenerant path (CD): To waste Pump purge mode at 0.1 mL/min for 30 min EG DEGAS ELUENT IN ELUENT OUT...

  • Page 85: Checking The Background Conductivity

    4 • System Plumbing 8. Check the backpressure to confirm that the regenerant path is ready: a. Note the pump pressure. b. Disconnect the CES from the CD (the high-pressure REGEN IN side) and note the difference in the pump pressure. c.

  • Page 86: Completing The Operational Qualification

    Dionex ICS-5000 Installation Instructions 4.1.8 Completing the Operational Qualification Capillary If you purchased the Operational Qualification (OQ) option, complete the procedure now for a CD system. For an ED system, complete the OQ after filling and flushing the liquid path, setting up the EG, and performing the system function test.

  • Page 87: 4.1.10 Flushing And Conditioning The Electrolytic Devices

    4 • System Plumbing 3. Remove the lines from the pre- EG DEGAS IN EG DEGAS OUT assembled tubing chain (see Figure 4-1) and connect them to their respective ports on the EG degas cartridge. 4. Connect the EG degas line to the injection valve ELUENT OUT ELUENT IN...
  • Page 88 Dionex ICS-5000 Installation Instructions 4. Unscrew the vent fitting from the top of the cartridge and install the Luer luer fitting shipped with the Fitting Dionex EGC. Save the vent fitting. To ensure proper ventilation, always install the luer fitting before operation.
  • Page 89 4 • System Plumbing Conditioning the Dionex EGC EGC Conditioning: (capillary) EGC concentration at 50 mM Pump flow at 0.03 mL/min for 30 min EGC IN Backpressure Tubing (P/N 068658) (P/N 074852) (Temporary connection) EGC OUT / TO CR-TC EL IN (P/N 072204) From pump To waste...
  • Page 90 Dionex ICS-5000 Installation Instructions Flushing the CR-TC 1. Remove the plugs from the ports on the CR-TC. 2. Connect the plumbing for flushing the CR-TC as shown in Figure 4-7. The same plumbing is also used for conditioning the CR-TC. CR-TC Flushing: Pump flow at 0.03 mL/min for 10 min CR-TC Conditioning:...
  • Page 91 4 • System Plumbing 3. Turn off the Dionex EGC current, the CR-TC voltage, and the pump flow. Remove the backpressure tubing. If you are installing an ED system, complete the IQ NOTE checklist, system function test, and OQ (if purchased) now.

  • Page 92: 4.1.11 Flushing And Installing The Columns

    Capillary For detailed information about a column, refer to the column NOTE manual, included on the Thermo Scientific Reference Library DVD (P/N 053891). Flushing the Capillary Columns 1. Locate the Dionex IC Cube Tubing Kit (P/N 072186) in the Dionex ICS- 5000 Ship Kit (P/N 075161).
  • Page 93 4 • System Plumbing 3. To flush the separator column: a. If you did not install a guard column, connect the 210 mm (8.27 in) precision cut tubing, labeled (P/N 072187), to the VALVE PORT 3 port (3) of the injection valve. Connect the other end to ELUENT OUT the separator column.
  • Page 94 Dionex ICS-5000 Installation Instructions 3. Raise the lid of the column tray to open it. Note the fitting and tubing clips on the base of the tray (see Figure 4-10). To indicate the placement of columns in the tray, labels and tubing guides are molded into the tray. Column Guide Label Tubing Clip...
  • Page 95 4 • System Plumbing 5. Coil the columns and precision cut tubing inside the cartridge as required for your configuration (refer to the following figures). Secure the tubing under the tubing clips and press the fittings onto the fitting clips. 65 mm (2.56 in) Precision Cut Tubing Separator...
  • Page 96 Dionex ICS-5000 Installation Instructions 65 mm (2.56 in) Precision Cut Tubing Separator Column Inlet Separator Column Outlet Guard Column Outlet Guard Column 125 mm (4.92 in) Inlet Precision Cut Tubing (inlet line) Figure 4-14. 150 mm Separator Column and 35 mm Guard Column Installed in Capillary Column Tray Separator Column Inlet...
  • Page 97 4 • System Plumbing 6. Press the inlet line down into the slot on the front of the column tray and close the lid (you should hear a click). The column tray lid should close easily. If not, do not force it. NOTE Open the lid and verify that the columns and tubing are installed correctly and secured in the clips.

  • Page 98: 4.1.12 Completing The Plumbing For Conductivity Detection

    Dionex ICS-5000 Installation Instructions 4.1.12 Completing the Plumbing for Conductivity Detection Capillary To gas separator waste tube (capillary) REGEN OUT CR-TC ELUENT IN ELUENT OUT REGEN IN From pump ELUENT IN ELUENT OUT ELUENT IN ELUENT IN DEGAS ELUENT IN ELUENT OUT ELUENT OUT ELUENT OUT...
  • Page 99 4 • System Plumbing If a CRD is not installed, connect the CES line to the CD ELUENT OUT port. 3. Connect the waste line from the CR-TC port to the gas REGEN OUT separator waste tube (see Section 4.3). 4.

  • Page 100: 4.1.13 Completing The Plumbing For Electrochemical Detection

    Dionex ICS-5000 Installation Instructions 4.1.13 Completing the Plumbing for Electrochemical Detection Capillary (capillary) To gas separator waste tube REGEN OUT CR-TC ELUENT IN ELUENT OUT REGEN IN From pump ELUENT IN ELUENT OUT ELUENT IN SUPPRESSOR BYPASS BYPASS ELUENT IN DEGAS ELUENT IN ELUENT OUT...

  • Page 101: 4.1.14 Routing The Ic Cube Tubing

    4 • System Plumbing 2. Connect the Suppressor Bypass line to the ED cell port. REGEN IN 3. Connect the waste line from the CR-TC port to the gas REGEN OUT separator waste tube (see Section 4.3). 4. Route the IC Cube tubing as described in Section 4.1.14.
  • Page 102 Dionex ICS-5000 Installation Instructions 2. Route tubing inside the DC through the tubing trays below the IC Cube (see Figure 4-18): a. Press the sample in and sample out lines from the injection valve into the tubing tray on the front of the IC Cube and then route the lines through the DC left-side slot to the autosampler.

  • Page 103: Plumbing An Analytical Ic System

    4 • System Plumbing Plumbing an Analytical IC System 4.2.1 Tubing and Fittings One tubing package with precut and labeled tubing (either microbore or standard bore) is included for each system configured in the ICS-5000 (see Table 4-1). The tubing is used for plumbing the columns, detector cell, suppressor, and system waste.

  • Page 104: System Plumbing Checklists

    Dionex ICS-5000 Installation Instructions 4.2.2 System Plumbing Checklists The system plumbing steps and the order in which they are performed vary slightly, depending on the installed detector. The following checklists outline the steps for each detection type. CD System Plumbing Checklist for Analytical IC Page ...
  • Page 105 Before installing a trap column, refer to the trap column manual for conditioning, equilibration, or plumbing details required for your application. The column manuals are provided on the Thermo Scientific Reference Library DVD (P/N 053891). 1. Remove the static mixer from the mounting clip on the component panel...

  • Page 106: Completing The Iq Checklist

    4. For a Dionex ATC 500, ATC-HC 500, ATC-HC Borate, or CTC 500: a. Locate the mounting clip required for your column in the pump ship kit. Thermo Scientific High-Pressure Trap Use This Mounting Clip ... Column Dionex ATC 500, 2 mm (P/N 079018)

  • Page 107: Performing The System Function Test

    The manuals are provided on the Thermo Scientific Reference Library DVD (P/N 053891). The Dionex EGC-CO EGC and Thermo Scientific Dionex NOTE EPM Electrolytic pH Modifier require specialized procedures for installation and conditioning. For details, refer to the product manuals.
  • Page 108 Dionex ICS-5000 Installation Instructions injection valve and the port on the Dionex EGC ELUENT OUT (see Section 4.4.1). EGC VENT RFIC Eluent Degasser To Waste Vent (via EG rear wall) Eluent Eluent Inlet Outlet Waste (via EG TO PUMP rear wall) Coupler TO INJ VALVE - P Coupler...
  • Page 109 4 • System Plumbing EGC VENT RFIC Eluent Degasser Vent To Waste Eluent Eluent (via EG rear wall) Inlet Outlet To Waste (via EG TO PUMP rear wall) Coupler TO INJ VALVE - P Coupler TO SRS/AES REGEN OUT To CR-TC Regen In (orange label) TO CR...
  • Page 110 Dionex ICS-5000 Installation Instructions La cartouche de Dionex EGC contient un de ce qui suit: une base corrosive (KOH, LiOH, ou NaOH), un acide corrosif (MSA), ou une solution concentrée de K . Porter des lunettes et des gants protectives en manipulant la cartouche. Die Dionex EGC-Kartusche enthält eine korrosive Base (KOH, LiOH oder NaOH), eine korrosive Säure (MSA) oder eine konzentrierte K Lösung.
  • Page 111 4 • System Plumbing 4. Turn the Dionex EGC upside down and place it on the EG drip tray (see Figure 4-24). This is the “service position” for the cartridge. EGC (Standard-Pressure Analytical) EGC (High-Pressure Analytical) Generation Generation Chamber Chamber Electrolyte Reservoir Drip Tray...
  • Page 112 Dionex ICS-5000 Installation Instructions 6. Connect the outlet line from the pump to the Dionex EGC port. INLET 7. Connect the line from the port of the Dionex RFIC Eluent ELUENT IN Degasser to the Dionex EGC port (see Figure 4-28).
  • Page 113 4 • System Plumbing 11. Push the Dionex EGC electrical cable firmly onto the EGC 1 EGC 2 bulkhead connector (see Figure 4-26). Twist the ring on the cable connector fingertight to secure it. EGC (Standard-Pressure Analytical) EGC (High-Pressure Analytical) Figure 4-26.
  • Page 114 Dionex ICS-5000 Installation Instructions Flushing and Conditioning the Dionex EGC 1. Locate the yellow 0.5 mL/min, 7 MPa (1000 psi) backpressure coil (P/N 053765) in the EG Ship Kit (P/N 072047). 2. Connect the coil to the port of the RFIC Eluent Degasser ELUENT OUT (see...
  • Page 115 4 • System Plumbing 3. On the Chromeleon 7 ePanel Set or Chromeleon 6.8 panel tabset: • Verify that the suppressor and the CR-TC are off. To avoid damaging the suppressor and Dionex CR-TC, always turn them off before conditioning the Dionex EGC. The pump flow is on during conditioning;...
  • Page 116 Dionex ICS-5000 Installation Instructions 10. Reconnect the Dionex EGC electrical cable. Hydrating the Dionex CR-TC 1. Remove the plugs from the Dionex CR-TC ports. 2. Locate the CR-TC Hydration Tubing Kit (P/N 063487) provided in the EG Ship Kit (P/N 072047). 3.
  • Page 117 4 • System Plumbing 8. In Chromeleon: a. Verify that the suppressor and Dionex EGC are turned off. To avoid damaging the suppressor, always turn off the suppressor before hydrating the Dionex CR-TC. The pump flow is on during conditioning; however, no flow reaches the suppressor. b.

  • Page 118: Plumbing The Dc For Analytical Ic Applications

    Also refer to the example plumbing diagrams on the DC lower door or in Chapter 3, “Configurations,” in Dionex ICS-5000 Ion Chromatography Operator’s Manual (Document No. 065446). The manuals are provided on the Thermo Scientific Reference Library DVD (P/N 053891). 2. Remove the guard column, separator column, and suppressor from their boxes.
  • Page 119 4 • System Plumbing 3. Remove the fitting plugs from the ends of each column and from all ports on the suppressor. 4. Discard any tubing temporarily connecting the suppressor ports. Unless instructed otherwise, use tubing from the system tub- NOTE ing package (described on page...
  • Page 120 Dionex ICS-5000 Installation Instructions To Waste Separator GUARD Guard Temp. C(3) Stabilizer Backpressure Device* From AS-AP To AS-AP/ From Eluent *A backpressure Waste Degasser device is not required for all systems Figure 4-32. Example DC Plumbing for Analytical IC with Electrochemical Detection: System 1 (Left Side) Shown Doc.
  • Page 121 4 • System Plumbing Plumbing the DC Injection Valve 1. Cut a length of 0.25 mm (0.010 in) ID black PEEK tubing long enough to connect from the Dionex RFIC Eluent Degasser to the injection valve. 2. Connect one end of this tubing to the coupler on the line from the Dionex RFIC Eluent Degasser labeled (white label).

  • Page 122: Plumbing The Tc For Analytical Ic Applications

    For detailed column startup and operational instructions, refer to the column manual provided on the Thermo Scientific Reference Library DVD (P/N 053891). 2. Locate these items in the TC Ship Kit (P/N 064789):...
  • Page 123 4 • System Plumbing • Sample loop, 25 µL (P/N 042857) (two sample loops are included) • 0.75 mm (0.030 in) ID PEEK tubing (green) (P/N 044777); used for the injection valve waste line • Standard bore systems: 0.25 mm (0.010 in) ID PEEK tubing (black) (P/N 052306);...

  • Page 124: Connecting Waste Lines To The Gas Separator Waste Tube

    The outlet line from the separator column in the TC can be connected to various types of detectors, including the Dionex VWD, Dionex PDA, and Thermo Scientific MSQ Mass Spectrometer. Refer to the detector manual for detailed installation instructions. Manuals for Dionex detectors are provided on the Thermo Scientific Reference Library DVD (P/N 053891).
  • Page 125 4 • System Plumbing separator waste tube and the waste container are open to the atmosphere (see Figure 4-35). If necessary, you can extend the black tubing. Locate the compression coupler (P/N 045463) and 13 mm (0.52 in) ID tubing (P/N 045822) provided in the DC Ship Kit (P/N 072011, standard DC;...

  • Page 126: Equilibrating The System

    Dionex ICS-5000 Installation Instructions NE FERMEZ PAS LE CONTENEUR DE GAZ RÉSIDUEL: Le Dionex ICS- 5000 Eluent Generator (EG) et les electrolytic suppressor travaillent avec un proces d´électrolyse, qui produit des petites quantités de gaz d´oxygène ou d´hydrogène. Afin de garantir que le gaz ne soit pas enfermé...
  • Page 127 3. View the detector signal and monitor the background. Refer to the column manual for the appropriate background for your application. The column manuals are provided on the Thermo Scientific Reference Library DVD (P/N 053891). 4. Offset the detector background and zero the reading by clicking the Autozero button.

  • Page 128: Installing A Backpressure Coil

    Dionex ICS-5000 Installation Instructions Because capillary IC systems use low flow rates and consume very little Capillary eluent, you can leave a capillary IC system on at all times, allowing it to remain equilibrated and always ready to run the next sample. 4.4.1 Installing a Backpressure Coil In an analytical IC system, if the system pressure is below 14 MPa (2000 psi)

  • Page 129: A • Installing Pump Options

    A • Installing Pump Options This appendix provides instructions for the following pump options: • Pressurizing eluent reservoirs (Section A.1) • Replumbing the piston seal wash system (Section A.2) Pressurizing Eluent Reservoirs The DP/SP does not require pressurized eluent reservoirs. However, Thermo Fisher Scientific recommends pressurizing reservoirs with helium or nitrogen under the following circumstances: •...

  • Page 130: Installing The Tc/Vwd/Pda Regulator Bracket

    Dionex ICS-5000 Installation Instructions A.1.1 Installing the TC/VWD/PDA Regulator Bracket The TC/VWD/PDA Regulator Bracket Kit (P/N 074424) includes a regulator bracket (P/N 074435), two screws (P/N 045687), and two washers (P/N 010645). 1. Place one leg of the regulator TC/VWD/PDA bracket on top of the TC or Regulator Bracket (P/N 074435)
  • Page 131 A • Installing Pump Options 50 psi). If needed for your gas source, use the adapter to connect the tubing to the gas source. EO Gas Regulator (P/N 074425) GAS IN Fitting Orange Air Line Tubing (P/N 052297) EO Regulator Support Bracket (P/N 074226) DC Rear Panel Figure A-2.

  • Page 132: Pressurizing The Eluent Reservoir

    Dionex ICS-5000 Installation Instructions 8. Remove the black cap from the quick-disconnect fitting, twist off the end of the quick-disconnect fitting, and then connect the free end of the blue tubing to a quick-disconnect fitting on the side of the EO Gas Regulator. Gas Source One-Way Tubing Assembly...

  • Page 133: Replumbing The Seal Wash System (Dp Only)

    A • Installing Pump Options 4. Turn the gas regulator knob clockwise to pressurize the eluent reservoir. Adjust the pressure to between 30 and 40 kPa (5 and 6 psi). Never pressurize eluent reservoirs above 70 kPa (10 psi). Pressurizing reservoirs above this limit can cause the reservoir to explode.
  • Page 134 Dionex ICS-5000 Installation Instructions 2. Move these lines from pump 1 to pump 2: • The short piece of tubing between the primary and secondary pump heads • The tubing from the secondary pump head that connects to the seal wash pump •...

  • Page 135: B • Installing Dc Options

    B • Installing DC Options This appendix provides instructions for installing the following DC options: • ED amperometry cell (Section B.1) • Low-pressure valves (Section B.2) • Injection valve panel (Section B.3) • Dionex ICS-5000 Automation Manager (Section B.4) • Dionex ICS-5000 IC Cube (Section...
  • Page 136 Dionex ICS-5000 Installation Instructions 2. Loosen the yoke knob that holds the spacer block to the cell body by unscrewing it two to three turns. 3. Squeeze the tabs on the sides of the yoke block and pull the knob with yoke block off the spacer block.
  • Page 137 B • Installing DC Options 5. Remove the protective film from the alignment pins on the cell body (see Figure B-3). Remove the cell protective film Figure B-3. Removing the Cell Protective Film 6. If you are installing the ED cell in a capillary IC system, use an open-end Capillary wrench to remove the titanium inlet line from the cell (see Figure...

  • Page 138: Installing A Disposable Working Electrode

    For installation instructions for disposable working electrodes, refer to the installation guide shipped with the electrodes (see below) or to Product Manual for Disposable Electrodes (Document No. 065040), which is provided on the Thermo Scientific Reference Library DVD (P/N 053891). • Disposable Silver Electrode Installation Guide for ED (Document No.
  • Page 139 B • Installing DC Options Items Needed for Installing a Conventional Working Electrode • ED cell gasket for conventional working electrodes (P/N 045972) • Blunt-end tweezers Install the working electrode before connecting the cell to the NOTE 1. Use tweezers to install the gasket over the alignment pins on the cell body (see Figure B-5).
  • Page 140 Dionex ICS-5000 Installation Instructions 3. Orient the working electrode block as shown in Figure B-6 and then slide it onto the alignment pins. Conventional Working Electrode Block Cell Body Cell Gasket Yoke Knob and Block Figure B-6. ED Cell Components 4.

  • Page 141: Installing The Ph-Ag/Agcl Reference Electrode

    B • Installing DC Options B.1.4 Installing the pH-Ag/AgCl Reference Electrode Preparing the pH-Ag/AgCl Reference Electrode 1. Orient the cell assembly with the yoke knob on the left and push the cell onto its mounting location on the ED. 2. Remove the pH-Ag/AgCl reference electrode (P/N 061879) from its box. 3.
  • Page 142 Dionex ICS-5000 Installation Instructions Calibration Procedure 1. Connect the cell electrical cable to the ED. 2. Connect the reference electrode electrical cable to the ED. Do not install the electrode in the cell yet. 3. On the Chromeleon 7 ePanel Set, click the ED tab. On the Chromeleon 6.8 panel tabset, click the EC Detector tab.
  • Page 143 B • Installing DC Options 8. Install the pH-Ag/AgCl reference electrode in the cell: • For a capillary IC system, follow the instructions in the next section. • For an analytical IC system, go on to page 137. Installing the pH-Ag/AgCl Reference Electrode in the Cell for Capillary IC Capillary Systems 1.
  • Page 144 Dionex ICS-5000 Installation Instructions 3. Using tweezers, install the reference electrode gasket for capillary IC (P/N 072162) into the bottom of the reference electrode well (see Figure B-10). Reference Electrode Gasket for Capillary IC Figure B-10. Reference Electrode Gasket for Capillary IC 4.
  • Page 145 B • Installing DC Options 5. Verify that the reference electrode O-ring has been removed and the reference electrode gasket is correctly installed in the bottom of the well. 6. Screw the pH-Ag/AgCl reference electrode into the reference electrode well and tighten it fingertight (see Figure B-12).
  • Page 146 Dionex ICS-5000 Installation Instructions 3. Orient the cell assembly with the yoke knob on the left and then push the cell onto its mounting location on the ED (see Figure B-14). 4. If the detector is already installed, connect the reference electrode cable and the cell cable.

  • Page 147: Installing The Pdh Reference Electrode In A Capillary Ic

    B • Installing DC Options B.1.5 Installing the PdH Reference Electrode in a Capillary IC Capillary System 1. To avoid any hydraulic pressure buildup when inserting the reference electrode into the cell, make sure that fitting plugs are not installed on the cell inlet and outlet fittings.
  • Page 148 Dionex ICS-5000 Installation Instructions 4. Orient the fitting on the end of the PdH reference electrode so that the knobs on the fitting align with the grooves in the reference electrode well (see Figure B-17). 5. Insert the fitting into the well. PdH Reference Electrode Knobs...

  • Page 149: Installing Low-Pressure Valves In The Dc

    B • Installing DC Options 8. If the detector is already installed, connect the reference electrode cable and the cell cable. 9. To complete the cell plumbing, go on to Section 4.1.13. Installing Low-Pressure Valves in the DC Three locations are available for installing low-pressure valves in the DC: on the rear panel, in the lower compartment, and on the Dionex ICS-5000 Automation Manager (AM).

  • Page 150: Installing A Low-Pressure Valve Inside The Dc

    Dionex ICS-5000 Installation Instructions 4. Note which rear panel connector each valve is connected to. This information is required to control the valves in Chromeleon. Location of Valve Mounting Slots External Low- Pressure Valve Connectors Figure B-19. DC Rear Panel: External Low-Pressure Valve Connections B.2.2 Installing a Low-Pressure Valve Inside the DC 1.

  • Page 151: Installing The Injection Valve Panel In The Dc

    B • Installing DC Options Installing the Injection Valve Panel in the DC Follow the instructions in this section to install the injection valve panel in the lower compartment of the DC. The panel can be ordered with 0, 1, or 2 valves mounted on the panel, and with either microbore or standard bore plumbing.
  • Page 152 Dionex ICS-5000 Installation Instructions Figure B-20 shows the components shipped with a single-valve panel. Injection Valve Panel (Single valve installed) Temperature Stabilizer System Tubing Package Figure B-20. Injection Valve Panel Ship Kit: Single-Valve Configuration Always turn off the DC power before installing a valve panel 1.
  • Page 153 B • Installing DC Options 4. Connect the system 1 injection valve cable (labeled ) (see SYS 1 Figure B-21) to the connector on the back of the system 1 valve (left side). For a dual-valve panel, also connect the cable to the system 2 SYS 2 valve (right side).

  • Page 154: Installing The Automation Manager (Am) In The Dc

    Dionex ICS-5000 Installation Instructions Installing the Automation Manager (AM) in the DC The AM consists of a tray for installation of valves and other components that are used for performing matrix elimination, large volume preconcentration, and other functions (see Figure B-24).
  • Page 155 B • Installing DC Options The AM is available in the following configurations: AM Configuration Part Number Two 10-port high-pressure valves, 075950 two low-pressure 3-way valves One 10-port high-pressure valve, 075951 one low-pressure 3-way valve One 6-port high-pressure valve, 075952 one low-pressure 3-way valve AutoPrep configuration: 075953...

  • Page 156: Installing A High-Pressure Valve On The Am

    Dionex ICS-5000 Installation Instructions B.4.1 Installing a High-Pressure Valve on the AM 1. While facing the rear of the AM, squeeze the release tabs on the outside edge of the plug that is installed in the valve mounting hole. Remove the plug.

  • Page 157: Installing A Low-Pressure Valve On The Am

    B • Installing DC Options B.4.2 Installing a Low-Pressure Valve on the AM 1. Insert the two tabs on the valve mounting plate into the slots for either the left or right valve mounting position. 2. While holding the valve mounting plate firmly against the AM, tighten the captive thumbscrew (see...

  • Page 158: Installing The Temperature Stabilizer On The Am

    Dionex ICS-5000 Installation Instructions B.4.4 Installing the Temperature Stabilizer on the AM 1. Remove the plate on the right side of the AM that covers the temperature stabilizer mounting location. 2. Slide the temperature stabilizer into the opening and tighten the captive thumbscrews (see Figure B-24).
  • Page 159 B • Installing DC Options 6. For each bracket, align the two captive screws on the bracket with the openings on the AM component tray. See Figure B-28 for the right- side location and Figure B-29 for the Openings for left-side location.

  • Page 160: Installing An Ic Cube In The Dc

    Dionex ICS-5000 Installation Instructions Installing an IC Cube in the DC Capillary Always turn off the DC power before installing an IC Cube 1. If the DC power is on, press the button on the front of the DC for POWER 2 seconds to turn off the power before continuing.
  • Page 161 B • Installing DC Options 6. To install an IC Cube guide: a. Note that one side of the guide is grooved (see Figure B-32). Also, note the two alignment pegs and the two attachment screws on the bottom of the guide. Groove Attachment Screws Alignment Pegs...
  • Page 162 Dionex ICS-5000 Installation Instructions c. Press the guide onto the tray (see Figure B-29). Use a slotted screwdriver to tighten the attachment screws. Tighten the attachment screws Figure B-34. IC Cube Guide Installed 7. Slide the IC Cube into the guides. Push the IC Cube firmly into the back wall of the DC until the connector on the rear of the IC Cube is fully seated.

  • Page 163: C • Networking Chromeleon 6.8 Computers

    C • Networking Chromeleon 6.8 Computers For routine Chromeleon 6.8 operation, the three Chromeleon 6.8 components shown in Figure C-1 (datasource, server, and client) must be able to communicate. These three components can all be installed on one computer, on three different computers, or in any other computer/component configuration.
  • Page 164 Dionex ICS-5000 Installation Instructions Workgroup Example Workgroup Chromeleon Client Chromeleon Datasource Figure C-2. Workgroup Example This workgroup example consists of the following components: • One Dionex ICS-5000 system • One desktop PC located at the system (not shown), with a monitor installed on the DC.
  • Page 165 C • Networking Chromeleon 6.8 Computers Domain Example Chromeleon Client Chromeleon Domain Datasource Chromeleon Chromeleon Chromeleon Client Client Client Chromeleon Chromeleon Chromeleon Server Server Server Figure C-3. Domain Example This domain example consists of the following components: • Three Dionex ICS-5000 systems •...

  • Page 166: Setting Up A Shared Datasource

    Dionex ICS-5000 Installation Instructions Setting Up a Shared Datasource Create a shared datasource if you want multiple clients and/or servers to access a single datasource. Details about how to set up and share a datasource differ slightly for the two network types. C.1.1 Setting Up a Shared Datasource on a Workgroup 1.

  • Page 167: Setting Up A Shared Datasource On A Domain

    C • Networking Chromeleon 6.8 Computers 5. Select the Allow network users to change my files check box and click All computers in the workgroup can now access any datasource installed in any subfolder of the shared folder. C.1.2 Setting Up a Shared Datasource on a Domain 1.
  • Page 168 Dionex ICS-5000 Installation Instructions c. For each user (or user group) that will log in locally to access data or control equipment, select the Allow Full Control check box. To add additional users or groups, click Add. d. Click Apply. 3.
  • Page 169 C • Networking Chromeleon 6.8 Computers 4. Create the new database in the Chromeleon 6.8 client: a. Open the Chromeleon 6.8 Browser. b. On the File menu, click Datasources. The Datasource Manager dialog box appears. c. Click New. The New Datasource dialog box appears (see Figure C-7).

  • Page 170: Connecting A Client To A Remote Datasource

    Dionex ICS-5000 Installation Instructions Connecting a Client to a Remote Datasource 1. Open the Chromeleon 6.8 client and go to the Browser. 2. On the File menu, click Mount Datasource and then click Browse. The Open dialog box appears. 3. Use the Open dialog box to browse to the network folder where the datasource is located.

  • Page 171: Connecting A Server To A Remote Datasource

    C • Networking Chromeleon 6.8 Computers C.2.1 Connecting a Server to a Remote Datasource The Network Failure Protection option is required for com- NOTE munication between a server and a network datasource. The Network Failure Protection and Multiple Network Control options are bundled together as a single license in Chrome- leon 6.8.
  • Page 172 Dionex ICS-5000 Installation Instructions The Connect to Chromeleon Server dialog box appears (see Figure C-10). Figure C-10. Connect to Chromeleon Server Dialog Box 2. Follow these steps to connect to a Chromeleon 6.8 server on a network computer: a. Click the plus sign next to the Network Neighborhood icon. b.
  • Page 173 C • Networking Chromeleon 6.8 Computers c. Select the Chromeleon 6.8 Server (see Figure C-11). Figure C-11. Select the Chromeleon 6.8 Server 3. Under Protocol, select the correct option from the drop-down list: • For a local computer, select My Computer. •...
  • Page 174 Dionex ICS-5000 Installation Instructions Doc. 065447-02 12/14...

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