Thermo Scientific Dionex ICS-5000 Manuals

Thermo Scientific Dionex ICS-5000 Manuals

Manuals and User Guides for Thermo Scientific Dionex ICS-5000. We have 1 Thermo Scientific Dionex ICS-5000 manual available for free PDF download: Operator's Manual

Thermo Scientific Dionex ICS-5000 Operator's Manual

Thermo Scientific Dionex ICS-5000 Operator's Manual (482 pages)

Ion Chromatography System

Brand: Thermo Scientific | Category: Laboratory Equipment | Size: 7.37 MB

Table of Contents

Table of Contents
3
1 Introduction

17
2 Description

37
- DP/SP Description
  
  37
  - DP/SP Front Features
    37
  - DP/SP Interior Components
    39
    
    Pump Heads
    40
    
    Pressure Transducer
    41
    
    Proportioning Valves (Gradient Pump Only)
    41
    
    Vacuum Degassing Module
    41
    
    Piston Seal Wash System
    42
    
    Pulse Damper (Capillary IC Only)
    43
    
    Static Mixer (Analytical IC Only)
    43
  - DP/SP Flow Schematics
    44
    
    Isocratic Pump Flow Schematic
    44
    
    Gradient Pump Flow Schematic
    45
  - DP/SP Rear Panel
    46
  - Eluent Reservoirs
    50
    
    EO (Optional)
    50
    
    Pressurizing Eluent Reservoirs
    50
    
    Filtering Eluent
    52
- EG Description
  
  53
  - EG Front Features
    53
  - EG Interior Components
    54
  - EG Rear Panel
    61
  - EG Flow Schematics
    63
- DC Description
  
  67
  - DC Front Features
    67
  - DC Interior Components
    69
    
    DC Interior Components for Capillary IC
    70
    
    IC Cube for Capillary IC
    71
    
    DC Interior Components for Analytical IC
    77
  - DC Temperature Control Zones
    79
  - High-Pressure Valves
    81
    
    4-Port Valve
    82
    
    6-Port Valve
    83
    
    10-Port Valve
    84
  - CD Conductivity Detector
    85
    
    Heated Conductivity Cell
    85
    
    Suppressor
    87
    
    System Flow Schematics for Conductivity Detection
    88
  - ED Electrochemical Detector
    91
    
    Electrochemical Detector Cell
    91
    
    Combination Ph-Ag/Agcl Reference Electrode
    93
    
    Palladium Hydrogen (Pdh) Reference Electrode
    95
  - DC Rear Panel
    96
  - I/O Option
    99
    
    I/O Option Connections
    100
    
    Analog Outputs
    101
    
    Power, Relay, and TTL Outputs
    103
    
    TTL Inputs
    105
  - Automation Manager
    110
    
    AM High-Pressure Switching Valves
    112
    
    AM Low-Pressure Valves
    113
    
    AM High- and Low-Pressure Valve Control
    114
    
    Reaction Coil Heater
    117
  - Electrochemical Detection Modes
    118
    
    DC Amperometric Detection
    118
    
    Integrated and Pulsed Amperometric Detection
    119
    
    Cyclic Voltammetry
    121
    
    Waveforms
    121
    
    Storing and Reprocessing Amperometry Data
    125
- TC Description
  
  131
  - TC Front Features
    131
  - TC Interior Components
    133
  - TC Rear Panel
    135
  - Injection Valves
    138
    
    Injection Valve Operation
    138
    
    Injection Valve Plumbing
    140
  - Column Identification (ID) System
    141
  - Gas and Humidity Sensors
    142
  - TC Theory of Operation
    143
    
    Predictive Performance
    144
3 Configurations

145
- Overview
  145
4 Startup

157
- Operating Precautions
  157
  - EG Operating Precautions
    157
  - ED Cell Operating Precautions
    159
- System Startup Checklist
  162
- Preparing Samples
  163
  - Collecting and Storing Samples
    163
  - Pretreating Samples
    163
  - Diluting Samples
    164
  - Filling the Autosampler Vials and Loading the Sample
    165
    
    Tray
    165
- Starting Chromeleon 7
  165
  - Starting the Chromeleon 7 Instrument Controller Service
    165
  - Starting the Chromeleon 7 Client
    165
- Starting Chromeleon 6.8
  166
  - Starting the Chromeleon 6.8 Server
    166
  - Starting the Chromeleon 6.8 Client
    167
- DP/SP Startup
  
  169
  - Setting up the Eluent Reservoirs
    169
  - Setting up the Piston Seal Wash System
    170
  - Starting the Pump
    173
- EG Startup
  
  177
  - Entering the Eluent Concentration
    177
  - Selecting an Eluent Concentration
    178
- DC Startup
  
  181
  - Starting the DC
    181
  - Equilibrating the System and Verifying Operational Readiness
    182
- TC Startup
  
  185
  - Starting the TC
    185
  - Equilibrating the System and Verifying Operational Readiness
    186
5 Operation

187
6 Shutdown

199
- DP/SP Shutdown
  
  199
- EG Shutdown
  
  201
  - Short-Term Shutdown
    201
  - Long-Term Shutdown
    201
- DC Shutdown
  
  203
  - Consumables Storage
    203
  - ED Cell Storage
    203
    
    Electrode
    203
    
    Short-Term Storage of the ED Cell
    203
- TC Shutdown
  
  205
  - Consumables Storage
    205
  - Short-Term Shutdown
    205
  - Long-Term Shutdown
    205
7 Maintenance

207
- System Maintenance Checklists
  207
  - Daily Maintenance
    207
  - Weekly Maintenance
    207
  - Periodic Maintenance
    208
  - Annual Maintenance
    208
- DP/SP Routine Maintenance
  
  211
  - DP/SP Daily Maintenance
    211
  - DP/SP Weekly Maintenance
    211
  - DP/SP Periodic Maintenance
    212
  - DP/SP Annual Maintenance
    212
- EG Routine Maintenance
  
  213
  - EG Daily Maintenance
    213
  - EG Weekly Maintenance
    213
  - EG Annual Maintenance
    213
- DC Routine Maintenance
  
  215
  - DC Daily Maintenance
    215
  - DC Weekly Maintenance
    215
  - DC Periodic Maintenance
    215
  - DC Annual Maintenance
    216
- TC Routine Maintenance
  
  217
  - TC Daily Maintenance
    217
  - TC Weekly Maintenance
    217
  - TC Periodic Maintenance
    217
  - TC Annual Maintenance
    218
8 Troubleshooting

219
- Audit Trail Error Messages
  219
  - DP/SP Error Messages
    220
  - EG Error Messages
    221
  - DC Error Messages
    223
  - TC Error Messages
    225
- Noisy Baseline
  230
- Poor Retention Time Reproducibility
  234
- Peak Retention Times Are too Early
  236
- Peak Retention Times Are too Late
  236
- No Peaks
  236
- Tailing Peaks
  238
- Low System Backpressure
  239
- High System Backpressure
  239
- Low Detector Output
  240
- High Background
  241
- DP/SP Troubleshooting
  
  243
  - Troubleshooting DP/SP Error Messages
    243
  - DP/SP Does Not Start
    251
  - DP/SP Stops
    252
  - DP/SP Liquid Leaks/Leak Alarm
    253
  - Vacuum Degassing Module Low Vacuum
    254
  - Vacuum Degassing Module Does Not Run
    254
  - DP/SP Digital I/O Port Inoperative
    255
- EG Troubleshooting
  
  257
  - Troubleshooting EG Error Messages
    257
  - EG ALARM LED Is Lighted
    269
  - EG POWER LED Fails to Light
    270
  - Liquid Leaks in the EG
    270
  - No Flow
    271
  - EG Stops Operation
    272
- DC Troubleshooting
  
  275
- TC Troubleshooting
  
  291
9 Service

319
- Connecting Capillary Tubing
  319
- Tightening Guidelines for High-Pressure Fittings
  321
- DP/SP Service
  
  322
  - Replacing Tubing and Fittings
    322
  - Cleaning Eluent Reservoirs
    324
  - Priming the DP/SP
    324
    
    Priming with the PUMP PRIME Button
    325
    
    Priming from the Chromeleon Panel
    326
  - Replacing the Check Valves
    328
    
    Removing the Check Valves
    329
    
    Installing the New Check Valves
    330
  - Replacing Piston Seals
    332
    
    Removing the Pump Head and Piston
    333
    
    Cleaning the Piston
    336
    
    Removing the Main Piston Seal
    336
    
    Installing the Piston Seals and O-Ring
    337
    
    Removing the Piston Seal Wash Seal
    337
    
    Reinstalling the Piston and Pump Head
    339
  - Replacing the Piston
    339
    
    Removing the Pump Head and Piston
    340
    
    Reinstalling the New Piston
    341
    
    Reinstalling the Pump Head
    341
  - Replacing the Piston Seal Wash Tubing
    342
  - Replacing the DP/SP Priming Valve Knob Seal
    345
  - Changing the DP/SP Main Power Fuses
    346
- EG Service
  
  349
  - Replacing Tubing and Fittings
    349
    
    Tubing and Fittings for Capillary IC EG Channels
    349
    
    Tubing and Fittings for Analytical IC EG Channels
    351
  - Isolating a Restriction in the Liquid Lines
    352
  - Replacing the EGC
    352
    
    Removing the Old EGC
    353
    
    Disposing of the Old EGC
    355
    
    Storing an Old EGC
    355
    
    Installing and Conditioning a New Capillary EGC
    356
    
    Installing and Conditioning a New Analytical EGC
    361
  - Replacing the CR-TC
    365
    
    Installing and Flushing the New CR-TC
    366
    
    Removing the Old CR-TC
    366
    
    Completing the New CR-TC Plumbing
    369
  - Replacing the RFIC Eluent Degasser
    371
  - Installing a Backpressure Coil
    371
  - Changing the EG Main Power Fuses
    373
- DC Service
  
  375
- TC Service
  
  423
  - Replacing Tubing and Fittings
    423
  - Setting up the Column ID System
    424
  - Rebuilding an Injection Valve
    426
  - Replacing an Injection Valve Pod
    427
  - Changing the Main Power Fuses
    429
A • Specifications

431
- DP/SP Specifications
  
  431
- EG Specifications
  
  435
- DC Specifications
  
  439
- TC Specifications
  
  449
B • Reordering Information

451
- DP/SP Reordering Information
  
  451
- EG Reordering Information
  
  455
- DC Reordering Information
  
  457
- TC Reordering Information
  
  461

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