PerkinElmer aanalyst 200 User Manual page 5

Chapter 8 Analyzing Samples
Sequence of Operations............................................................................... 8-3
Manual Flame Analyses .............................................................................. 8-4
Automated Flame Analyses....................................................................... 8-15
Manual Analyses: Data Display MHS-Technique .................................... 8-22
Running Samples in Emission Mode ........................................................ 8-23
Shutting Down The System....................................................................... 8-31
Emergency Shutdown................................................................................ 8-32
Rinsing the Burner System........................................................................ 8-33
Chapter 9 Maintenance
Introduction ................................................................................................. 9-3
General Maintenance Checklist................................................................... 9-4
Instrument Maintenance Checklist .............................................................. 9-5
Checks ......................................................................................................... 9-7
Spectrometer Maintenance Checklists ........................................................ 9-8
Burner Maintenance Checklist .................................................................... 9-9
Changing the Air Filter.............................................................................. 9-11
Extinguishing the Flame............................................................................ 9-12
Cleaning the Burner Chamber ................................................................... 9-13
Removing the Burner Door ....................................................................... 9-15
Replacing the Burner Door........................................................................ 9-16
Cleaning the Burner System...................................................................... 9-17
Cleaning the Burner Head ......................................................................... 9-19
Pre-Conditioning a New Burner or Drain Tube ........................................ 9-21
Removing the Burner Head ....................................................................... 9-22
Removing the Burner Assembly from the Instrument............................... 9-23
Disassembling the Burner Chamber .......................................................... 9-25
Reassembling the Burner System.............................................................. 9-28
Drain System Maintenance........................................................................ 9-32
Cleaning the Nebulizer .............................................................................. 9-36
Replacing Parts of Wear............................................................................ 9-45
E-Box ........................................................................................................ 9-46
Maintaining the Acetylene Supply ............................................................ 9-50
Replacing the Lamps ................................................................................. 9-51
Replacing the Deuterium Arc Background Corrector Lamp..................... 9-52
AS-90plus and AS-93plus Autosampler Maintenance.............................. 9-56
MHS-15 Mercury/Hydride System Maintenance...................................... 9-57
Replacement Parts and Accessories .......................................................... 9-60
Chapter 10 Troubleshooting
Introduction ............................................................................................... 10-3
Flame Analysis Troubleshooting............................................................... 10-4
Flame/Burner Troubleshooting ................................................................. 10-8
Lamp Troubleshooting ............................................................................ 10-11
Troubleshooting Deuterium Background Corrector Problems................ 10-13
Index