PerkinElmer AVIO 500 Manuals

PerkinElmer AVIO 500 Manuals

Manuals and User Guides for PerkinElmer AVIO 500. We have 1 PerkinElmer AVIO 500 manual available for free PDF download: Customer Hardware And Service Manual

PerkinElmer AVIO 500 Customer Hardware And Service Manual

PerkinElmer AVIO 500 Customer Hardware And Service Manual (355 pages)

ICP OPTICAL EMISSION

Brand: PerkinElmer | Category: Laboratory Equipment | Size: 8.94 MB

Table of Contents

Table of Contents
5
Customer Service
13
Safety and Regulatory Information
14
Using this Guide
27
Documents to Help You
27
How this Guide Is Organized
28
- Using the Index
  29
- A Word on Troubleshooting
  29
Chapter 1: Safety Practices

33
- Introduction
  34
- Laboratory Guidelines
  34
  - General
    34
  - Environmental Conditions
    35
  - Handling of the Instrument
    36
  - Laboratory Ventilation
    36
- Instrument Safety Practices
  36
  - Safety Interlocks
    37
  - Radio Frequency Radiation
    37
  - Ultraviolet Radiation
    37
  - Electrical Safety
    38
  - High Temperatures
    42
  - Hot Exhaust Gases
    42
  - Safe Use of Drain Systems
    42
  - Waste Disposal Procedures
    43
- Safe Handling of Gas Cylinders
  45
- Sample Preparation
  50
  - Dissolving Solid Samples in Organics
    51
  - Dissolving Solid Samples Using Acids
    51
  - Acid Digestions
    52
  - Fusion Mixtures
    54
- Decontamination and Cleaning
  55
  - Decontamination
    55
  - Cleaning the Instrument
    56
- References
  57
Chapter 2: Preparing Your Laboratory

61
- Chapter Overview
  61
- Environmental Conditions
  61
- Exhaust Vent Requirements
  62
  - Vent Positions
    64
- Laboratory Space Requirements
  66
- Location
  69
- Cooling Water Requirements
  69
  - Electrical Requirements
    70
- Handling of Gas Cylinders and Other Suggested Safety Practices
  72
- Gases for the Avio 500 ICP
  73
  - Plasma Shear
    75
  - Drain Vessels
    75
Chapter 3: System Description

79
- Plasma Viewing Configurations
  81
- Spectrometer
  86
  - Optical System
    86
  - Detector Cooling and Purging
    87
- ICP Source
  88
  - RF Generator
    88
  - RF Control Electronics
    90
- Sample Compartment
  90
- Sample Introduction System
  90
  - Quick-Change Adjustable Torch Module
    90
  - Torch
    91
  - Spray Chamber
    91
  - Nebulizers
    91
  - Peristaltic Pump
    95
  - Autosampler
    95
- System Initialization and Setup
  96
  - Interlocks
    96
  - Initialization Steps
    96
  - Hardware Setup and Optimization
    97
- How the Echelle Spectrometer and SCD Work
  98
  - Introduction
    98
  - Transfer Optics
    98
  - Input Module
    98
  - UV Module
    100
  - Visible Module
    102
  - Segmented-Array Charge-Coupled-Device Detector (SCD)
    102
- EMO Switch
  107
- Connections to Electrical, Gas, and Cooling Water Supplies
  108
- Specifications
  112
  - ICP System Specifications
    112
  - Gas Flow Controls
    112
  - Sample Introduction System
    113
  - Spectrometer
    114
Chapter 4: Installation

117
- Installation Summary
  118
- Setting up the Computer and Printer
  118
- Moving the Instrument
  119
- Connecting the Gases and Cooling Water
  120
  - Connecting the Gases
    120
  - Connecting the Polyscience Chiller
    123
  - Filling the Polyscience Chiller
    128
  - Starting up the Polyscience Chiller
    129
- Connecting the System Components
  130
  - Connecting the USB Cable for the Plasmacamtm
    133
- Installing the Quick-Change Adjustable Torch Module
  134
- Connecting the Scott Spray Chamber
  150
  - Connecting the Nebulizer (NEB) Tubing
    155
- Connecting the Cyclonic Spray Chamber
  157
- Setting the Torch Position
  160
- Installing the Autosampler
  162
- Fitting and Connecting the Autosampler Sampling Probe
  166
  - Fitting the Sampling Probe
    167
  - Adjusting the Sampling Probe Height
    169
- Setting the Torch Viewing Position
  171
- Switching on the System
  172
- Instrument Start-Up
  173
- Automatically Aligning the Torch Viewing Position
  174
  - Detector Calibration
    175
  - Wavelength Calibration
    176
- Setting Instrument Parameters
  178
- Shipping Lists
  183
Chapter 5: Maintenance

199
- Daily Checks
  200
  - Daily Cleaning
    200
  - Argon Supply
    200
  - Purge Gas Supply
    200
  - Shear Gas Supply
    200
  - Chiller
    201
  - Vent
    201
  - Torch and Plasma Induction Plates
    201
  - Nebulizer
    202
  - Peristaltic Pump and Drain
    202
- Periodic Checks
  203
  - Torch Assembly and Plasma Induction Plates
    203
  - Purge Viewing Window/Tubes
    204
  - Nebulizer
    204
  - Spray Chamber
    204
  - Peristaltic Pump
    204
  - Drains
    204
  - General System Maintenance
    204
  - Torch Viewing Position Alignment
    205
  - Performance Checks
    205
  - Cleaning the Sample Introduction System
    206
- Quick-Change Adjustable Torch Module
  207
  - Plasma Torch
    208
  - Plasma Induction Plates
    210
  - Removing the Injector
    210
  - Removing and Disassembling the Torch
    211
  - Cleaning the Torch
    219
  - Replacing the Torch
    220
  - Replacing the Torch on the Mount
    222
- Scott Spray Chamber
  224
- Cyclonic Spray Chamber
  228
- Replacing the Plasma Induction Plates
  232
- Windows
  234
  - Removing and Cleaning the Windows
    234
  - Removing and Replacing the Windows
    235
  - Cleaning the Windows
    242
- Replacing and Adjusting the Shear Gas Nozzle
  243
  - Removing the Shear Gas Nozzle
    244
  - Returning the Shear Gas Nozzle
    247
- Remove and Replacing the Axial Heat Sink Cooling Tube
  249
- Removing and Replacing the Axial Flat Optic
  251
- Nebulizers
  256
- Gemtip Cross-Flow Nebulizer
  259
- Removing the Argon Tip from the End Cap, N0780546
  267
- Connecting the Nebulizer Argon Tubing (Cross-Flow End Cap, N0780546)
  270
- Replacing the Nebulizer Argon Tubing (Cross-Flow End Cap, N0780546)
  270
- Replacing the Nebulizer/End Cap
  272
- Gemcone Nebulizer
  273
- Concentric Glass Nebulizer
  278
- Mira Mist Nebulizer
  284
  - Sample Capillary Tubing
    285
  - Gas Line
    285
  - Sample Introduction / Maximizing Stability
    286
  - Cleaning the Nebulizer
    286
- Peristaltic Pump
  287
  - Replacement Pump Tubing
    287
  - Installing the Sample and Drain Tubing
    287
  - Installing the Sample Tubing
    289
  - Connecting the Drain Tubing Assembly
    291
  - Installing the Drain Tubing
    293
  - Adjusting the Pump Tubing
    294
  - Cleaning the Pump
    295
  - Removing the Pump Head on the Peristaltic Pump
    295
  - Drain
    296
- General System Maintenance
  298
  - Cleaning the Instrument
    298
  - Air Filters
    298
  - Changing the Air Filters
    298
  - Chiller and Filters
    299
  - Fuses
    300
- Replacement Parts: General
  301
  - Consumables and Supplies
    315
Chapter 6: Troubleshooting

319
- What the Performance Checks Measure
  320
- Sodium Bullet Test
  321
- Performance Problems
  322
  - Checking the Sample Introduction System
    322
- Performance Problems: Troubleshooting Table
  326
- Plasma Ignition and Stability Problems
  330
  - Plasma Ignition Problems
    330
  - Plasma Stability Problems
    332
- Printing Problems
  333
- Pump Problems
  334
- Autosampler Problems
  335
- RF Generator/Sample Introduction System Troubleshooting Form
  336
  - Troubleshooting Form
    336
  - General
    336
  - Sample Introduction Configuration
    336
  - Operating Conditions
    336
  - Instrument Environment
    336
  - Troubleshooting Tasks Performed
    337
  - Common Setup Problems
    337

Advertisement

Advertisement

Related Products

PerkinElmer Categories

Laboratory Equipment Measuring Instruments Dispenser eBook Reader Microscope

More PerkinElmer Manuals