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Elzone

II 5390 Confirm

Operator's Manual

Rev A

539-42822-01

Nov 2017

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Summary of Contents for Micromeritics Elzone II 5390

Page 1 Elzone II 5390 Confirm Operator’s Manual Rev A 539-42822-01 Nov 2017...
Page 2 Adobe Acrobat is a registered trademark of Adobe Systems, Inc. © Micromeritics Instrument Corporation 2014 - 2017. All rights reserved. The software described in this manual is furnished under a license agreement and may be used or copied only in...
Page 3 MICROMERITICS shall not be liable for consequential or other type damages resulting from the use of any of its products other than the liability stated above. This warranty is in lieu of all other warranties, express or implied, including, but not limited to, the implied warranties of merchantability or fitness for use.
Page 5 Elzone II 5390 Confirm Table of Contents TABLE OF CONTENTS 1. GENERAL INFORMATION Organization of the Manual ............1-1 Conventions .
Page 6 Table of Contents Elzone II 5390 Confirm Calibrating an Orifice Tube ............3-18 Preparing for an Analysis .
Page 7 Elzone II 5390 Confirm Table of Contents Sample Information File............4-49 Analyst .
Page 8 Table of Contents Elzone II 5390 Confirm 6. REPORTS MENU Description ..............6-1 Start Report.
Page 9 Elzone II 5390 Confirm Table of Contents Replacing the Air Filter ............8-8 Cleaning Orifice Tubes .
Page 10 Table of Contents Elzone II 5390 Confirm Aqueous ..............D-1 Organic .
Page 11 Organization of the Manual Elzone II 5390 Confirm 1. GENERAL INFORMATION This manual describes how to operate the Elzone 5390 analyzer. To help you operate the Elzone more efficiently: • read Chapter 2, User Interface, before operating the analyzer and its software •...
Page 12 Elzone II 5390 Confirm Organization of the Manual Chapter 8 TROUBLESHOOTING AND MAINTENANCE Provides information for troubleshooting and for performing routine maintenance procedures. Chapter 9 ORDERING INFORMATION Provides ordering information and part numbers for system components. Appendix A ERROR MESSAGES Provides a listing of error messages that may be displayed by the analysis program, as well as causes and actions for each.
Page 13 Organization of the Manual Elzone II 5390 Confirm Conventions This manual uses the symbols shown below to identify notes of importance, warnings, and cautions: Notes contain important information pertinent to the subject matter. Warnings contain information that help you prevent actions that may cause personal injury.
Page 14 Elzone II 5390 Confirm Internet Access Internet Access Visit www.micromeritics.com to learn more about Micromeritics, our products, and applications. Our site is user-friendly, easy to navigate, and informative. Its content is summarized below. About Micromeritics A brief history of Micromeritics, office locations, awards/cer-...
Page 15 System Description Elzone II 5390 Confirm System Description The Elzone 5390 Particle Size analyzer uses the electrical sensing method for measuring particles. It is capable of measuring particles (organic and inorganic) ranging from 0.4 to 240 m in diameter. The Elzone’s ability to measure low-concentration samples allows it to produce accurate data where other techniques are limited.
Page 16 Elzone II 5390 Confirm System Description Orifice Tubes A wide range of orifice tubes is available to accommodate many sample sizes. The orifice is drilled in a synthetic jewel which is permanently sealed into the wall of the tube. Each tube is carefully tested, using standard samples of monodispersed polymer spheres, to verify it produces distortion-free measurements.
Page 17 System Description Elzone II 5390 Confirm ElectroPrep The ElectroPrep is designed to recirculate electrolyte through a filter cartridge that retains particles greater than 0.1 to 0.2 micrometers in diameter. The electrolyte is contained in a reservoir, providing a supply of clean electrolyte at all times.
Page 18 Elzone II 5390 Confirm Specifications Specifications The Elzone 5390 analyzer has been designed and tested to meet the specifications listed below. Characteristic Specification Analysis Electrolyte: Aqueous- or organic-based liquids Concentration: From 1 to 1000 ppm (0.1%) by volume Sensing rate: From 1 to over 5,000 particles per second 0.4 to 240 m (20-30: 1 range per orifice)
Page 19 Specifications Elzone II 5390 Confirm Characteristic Specification Computer Minimum requirements: • P1 GHz or faster 32 bit (x86) or 64 bit (x64) processor • 2 GB RAM • 40 GB minimum hard drive (formatted in NTFS) (one partition) • Video Adapter capable of 1024 × 768 minimum resolution •...
Page 20 Elzone II 5390 Confirm Specifications 1-10 539-42822-01 (Rev B) - Nov 2017...
Page 21 Controls, Indicators, and Connectors Elzone II 5390 Confirm 2. USER INTERFACE The Elzone 5390 Confirm software is accessed by three different levels of users: • Administrator: installs and maintains software and updates, establishes user accounts and rights (the Administrator responsibilities are covered in a separate manual).
Page 22 Elzone II 5390 Confirm Controls, Indicators, and Connectors Front Panel Electrode (external) connector Orifice light connector Sample port Power Indicator (upper left side of front panel) Camera assembly Exit tube Stirrer assembly  (shows rotary stirrer installed) Sample Stand This door contains a reflector (used to diffuse the orifice light when the camera is installed).
Page 23 Controls, Indicators, and Connectors Elzone II 5390 Confirm Sample port For installing the orifice tube. Exit tube This tube is used to remove liquid from the sample beaker to the waste container. Stirrer assembly Enables you to maintain dispersion of the sample. Two types of stirrers are available: •...
Page 24 If the second sensor activates, the internal tubing is filled with liquid and may have spilled into the internal component area. Call your Micromeritics service representative if this occurs. Refer to Sensors, page 5-41 for additional information.
Page 25 Power connector Air Filter Voltage selector card On/Off switch Test points For use by Micromeritics service personnel only Camera USB port For connecting the camera Air Filter Helps to minimize buildup of dust within the analyzer On/Off switch For turning the analyzer on and off...
Page 26 Elzone II 5390 Confirm Using the Software Using the Software The Elzone 5390 Program operates in a Windows environment and requires familiarity with standard Windows operations such as using the mouse, menus, and dialog boxes. While this manual provides brief instructions for such standard operations, you may have to refer to your Windows documentation or to its online help system to clarify functions which are specific to Windows.
Page 27 Using the Software Elzone II 5390 Confirm Shortcut Keys Shortcut keys can be used to activate some menu commands. Shortcut keys or key combi- nations (if assigned) are listed to the right of the menu item. Instead of opening the menu and choosing the command, simply press the key combination.
Page 28 Elzone II 5390 Confirm Using the Software Dialog Boxes and Subdialog Boxes Dialog boxes are displayed when a item followed by an ellipsis (...) is selected. Subdialog boxes are displayed when certain push buttons are selected. Both types of boxes may contain one or more of the items listed below.
Page 29 Using the Software Elzone II 5390 Confirm Check box Check boxes allow you to choose multiple options from a group of options. Push button Typically, a push button is used to display subdialog boxes in which to edit, enter, or specify additional information about the subject matter.
Page 30 Elzone II 5390 Confirm Using the Software Selecting Files Sample information is stored in files and saved under file descriptions. Certain dialog boxes contain a Files list box which displays a list of files available for that particular operation. For example, the Open Sample Information File dialog.
Page 31 Using the Software Elzone II 5390 Confirm For convenience, the following shortcut keys are available when the Select Dates dialog is displayed: Clears the field Inserts the current date Displays a calendar from which you may select a date Selects the year...
Page 32 Elzone II 5390 Confirm Using the Software Selecting Reports Reports are selected from the Report Options dialog. Simply select (highlight) the report and then double-click, or press the spacebar . A report is selected when it is preceded with a check mark. Reports are deselected in the same manner.
Page 33 Menu Structure Elzone II 5390 Confirm Menu Structure All functions for the Elzone analyzer are located on menus which are accessed from the Menu bar. Each menu contains commands, and in some cases a submenu. A submenu is indicated when the command is followed by an arrow.
Page 34 Elzone II 5390 Confirm Menu Structure Windows Enables you to arrange the windows and icons on your screen. It also displays the names of all open files. (this chapter, page 2-14) Help Displays information about the Elzone program. Also provides access to the online operator’s manual.
Page 35 Menu Structure Elzone II 5390 Confirm Help Menu Operator’s  Provides a copy of the operator’s manual in Adobe Acrobat Manual PDF format. Refer to Specifications, page for tips on using the online manual. About Elzone II Displays information about the Elzone 5390 analysis program.
Page 36 Elzone II 5390 Confirm Menu Structure 2-16 539-42822-01 (Rev B) - Nov 2017...
Page 37 Creating File Templates Elzone II 5390 Confirm 3. OPERATIONAL PROCEDURES This chapter contains brief step-by-step instructions on how to: • create sample and parameter file templates, beginning on this page • create a parameter file, page • create a sample file, page 3-10 •...
Page 38 Elzone II 5390 Confirm Creating File Templates Perform the following steps to create a template using a sample file. Select File > Open >Sample information; the Open Sample Information dialog is displayed. Choose the desired file, then click ; the Sample Information dialog is displayed.
Page 39 Creating Parameter Files Elzone II 5390 Confirm Click Save to save the template. If Save does not become enabled, a file containing the same description currently exists. Edit the description to enable Save . The Confirm program does not allow duplicate file descriptions.
Page 40 Elzone II 5390 Confirm Creating Parameter Files Analysis Conditions Analysis conditions specify the data used to guide an analysis. Analysis Conditions, page 4-12 Refer to if you need clarification of the fields on the dialogs used in this procedure. Perform the following steps to create an analysis conditions file: Select File >New >...
Page 41 Creating Parameter Files Elzone II 5390 Confirm Select Specify Diameter range and specify a range for the size of particles to be read. Specify rinse options. You can choose to rinse before or after the analysis by draining and filling the system or simply by flushing the system.
Page 42 Elzone II 5390 Confirm Creating Parameter Files Material Properties Material properties specify data for the sample material and its electrolyte. Material Properties, page 4-22 Refer to if you need clarification of the fields on the dialog used in this procedure.
Page 43 • up to eight plots of different samples onto the current plot of the same type, and they don’t all have to contain data collected with the Elzone. You can overlay data collected with Micromeritics’ Saturn DigiSizer 5200, SediGraph 5100, and SediGraph 5120.
Page 44 Elzone II 5390 Confirm Creating Parameter Files Choose a template, then click Create ; the Report Options dialog is displayed: Enter a description (up to 42 characters) in the Report options field. Enter an identifier that gives a more intuitive description of the file’s contents. For example, Particle Diameter, Inc.
Page 45 Creating Parameter Files Elzone II 5390 Confirm 10. From the Reports to Generate list, select the reports you wish to have generated. Refer to Selecting Reports, page 2-12 for details on selecting reports. 11. Click Save ; the Save As Report Options File dialog is displayed.
Page 46 Elzone II 5390 Confirm Creating a Sample Information File Creating a Sample Information File A sample information file must be created for each analysis. The sample information file consists of information groups which, collectively, identify the sample, guide the analy- sis, and specify report options.
Page 47 Creating a Sample Information File Elzone II 5390 Confirm Click on the down arrow to the right of each of the following fields to choose appropriate parameter files, or you can accept the defaults displayed in the template: • Analysis Conditions •...
Page 48 Elzone II 5390 Confirm Creating a Sample Information File Developer A Developer’s view of the sample information dialog is more flexible than that of an Ana- lyst. A Developer is allowed to view and edit (if desired) all parameters of the file.
Page 49 Creating a Sample Information File Elzone II 5390 Confirm Select the type of data for this file; you can have data collected automatically, enter the data manually, or have the data collected and saved for a background. If you have User Parameter fields defined, enter the appropriate values; refer to...
Page 50 Elzone II 5390 Confirm Performing a Background Analysis Performing a Background Analysis Occasionally, the ratio between contaminates in the electrolyte and particles in a sample can be low and, therefore, difficult to tell the difference between the two. When performing an analysis, the desired ratio between sample particles and contamination (sometimes called signal-to-noise ratio) in the electrolyte is approximately 99:1 in 1 mL of electrolyte.
Page 51 Performing a Background Analysis Elzone II 5390 Confirm d. Enter appropriate values for other fields (stirrer speed, etc.) on the Analysis Conditions dialog. Click the Material Properties tab; select the electrolyte being used. The sample material selected is irrelevant since only the electrolyte is being used for a background analysis.
Page 52 Elzone II 5390 Confirm Performing a Background Analysis Using a mild detergent, wash the propeller, the electrode, an appropriate sample beaker (refer to the reference material booklet for the size of sample beaker to use), and the orifice tube. Use the straight brush provided in the accessories kit to scrub the inside and outside of the orifice tube, and the orifice.
Page 53 Performing a Background Analysis Elzone II 5390 Confirm Raise the sample stand. Be sure the stirrer does not strike the bottom or sides of the beaker when raising the sample stand. The stirrer will not operate if it comes in contact with the beaker.
Page 54 Elzone II 5390 Confirm Calibrating an Orifice Tube Calibrating an Orifice Tube An orifice tube must be calibrated for the instrument on which it is to be used. An orifice tube (in the drop-down list) that has not been calibrated will be indicated with an asterisk.
Page 55 Calibrating an Orifice Tube Elzone II 5390 Confirm Install the orifice tube onto the sample port (the instructions on page 3-26 explain how to install an orifice tube). If you have a camera installed on the analyzer, adjust the lens to display the orifice.
Page 56 Elzone II 5390 Confirm Calibrating an Orifice Tube 12. Close the sample compartment door on the right side; adjust the light and camera if needed. 13. Select Unit > Fill System; the Fill System dialog is displayed. This step fills the internal glassware.
Page 57 Calibrating an Orifice Tube Elzone II 5390 Confirm 17. Click Unit > Orifice Tube Calibration; the Orifice Tube Calibration dialog is displayed. 18. Click Replace ; the Open Analysis Conditions File dialog is displayed. Developer’s view of the Open Analysis Conditions File dialog.
Page 58 Elzone II 5390 Confirm Calibrating an Orifice Tube 19. Select the appropriate calibration file for the selected orifice tube. Click to return to the Orifice Calibration dialog; appropriate values for the calibration will be copied into the fields. 20. Click the down arrow to the right of the Orifice Tube field and choose the tube you plan to calibrate.
Page 59 Calibrating an Orifice Tube Elzone II 5390 Confirm 21. Click Next ; the second view of the Orifice Tube Calibration dialog is displayed. 22. The appropriate reference materials should display in the window; if not, add them as follows: a. Click ;...
Page 60 Elzone II 5390 Confirm Calibrating an Orifice Tube 23. Be sure that only the reference materials to be used in this calibration are selected (preceded with a check mark). Double-click on a reference material to place (or remove) a check mark.
Page 61 Calibrating an Orifice Tube Elzone II 5390 Confirm 27. Click Finish ; the Finish dialog is displayed. Be sure no tests are remaining. Ensure that the data are saved. Ensure that 0 (zero) is in the Number of Testers Remaining field and the data are saved.
Page 62 Elzone II 5390 Confirm Preparing for an Analysis Preparing for an Analysis Choosing and installing an Orifice tube Choose an orifice tube with an orifice that is approximately two times the diameter of If available, a microscope can be used to the largest particles in the sample.
Page 63 Preparing for an Analysis Elzone II 5390 Confirm c. Holding the orifice tube with one hand, slide the connector nut over the top of the tube. (Your hand will keep the connector nut in place.) Then slide the ferrule over the top of the tube;...
Page 64 Elzone II 5390 Confirm Preparing for an Analysis Filling the Supply Container Your supply container should always contain the same electrolyte as the one used to prepare and disperse your sample. Be sure your supply container is filled with filtered electrolyte before you begin the analysis.
Page 65 Preparing for an Analysis Elzone II 5390 Confirm Changing the Liquid in the Supply Container Your supply container should always contain the same electrolyte as the one used to prepare and disperse your sample. These instructions are written for changing to a liquid of the same type base; for example, a water-based electrolyte to a different water-based electrolyte.
Page 66 Elzone II 5390 Confirm Preparing for an Analysis Changing Liquids of Different Bases These instructions use an example of changing from a water-based electrolyte to an alcohol-based electrolyte. Select Unit > Change Orifice Tube or Liquid; the Change Orifice Tube or Liquid dialog is displayed.
Page 67 Preparing for an Analysis Elzone II 5390 Confirm When prompted to change the liquid: a. Remove the supply tube from its container, then remove the cap from the container. b. Empty the container of the alcohol, then refill it with the alcohol-based electrolyte.
Page 68 Elzone II 5390 Confirm Preparing for an Analysis Enter your password and click ; the second view of the Analysis dialog is displayed. Click Instrument Setup and ensure that Specify Diameter Range is selected and a valid range specified; click to close the dialog.
Page 69 Preparing for an Analysis Elzone II 5390 Confirm Preparing and Loading Your Sample Sample Dispersion You must disperse a sample properly before you can analyze it. Use an effective electrolyte and sample dispersion method, obtained from references or by comparative testing, for stable counts.
Page 70 Elzone II 5390 Confirm Preparing for an Analysis Procedure If possible, prepare your sample when you are ready to start the analysis. If you prepare your sample in advance, be sure to place a lint-free cover over the beaker to prevent the entry of air-borne particles.
Page 71 Preparing for an Analysis Elzone II 5390 Confirm Add an appropriate amount of sample mix to the analysis beaker; enough to achieve a 1% coincidence level. If your sample contains large particles, manually stir the sample mixture while transferring to the analysis beaker. This is to prevent the larger particles from remaining in the transferring beaker.
Page 72 Elzone II 5390 Confirm Performing an Analysis Performing an Analysis Before you start your analysis, be sure you have: 3 cleaned and calibrated your orifice tube; page 3-52 3 filled your supply container with filtered electrolyte; page 3-28 3 emptied your waste container 3 optimized instrument settings for the current electrolyte (this also can be done on the second view of the Sample Analysis dialog before you begin your analysis);...
Page 73 Performing an Analysis Elzone II 5390 Confirm Ensure that all parameters are appropriate, then click Next ; the User Log in dialog is displayed. Enter your password and click ; the second view of the Sample Analysis dialog is displayed.
Page 74 Elzone II 5390 Confirm Printing File Contents Printing File Contents You can print the contents of one or more sample file, parameter file, or file template. For example, if you print the contents of an analysis conditions file, you will receive the parameters used for the analysis conditions associated with the file.
Page 75 Listing File Statistics Elzone II 5390 Confirm Listing File Statistics You can generate a list of the following information on a sample file, parameter file, or sample template for one or more files: • File name • Date the file was created (or last edited) •...
Page 76 The Import function allows you to import files which have been created on a computer other than the one controlling the analyzer and have them display in the Files list window. Review the Micromeritics PROGRAM License Agreement for restrictions on the use of another copy Perform the following steps to import a file: Copy the file(s) you wish to import, then paste into the Import directory.
Page 77 Exporting a Sample Information File Elzone II 5390 Confirm Exporting a Sample Information File An Analyst is not authorized to export sample files. Export allows a Developer to: • export the entire sample file to the Export directory. For example, you may wish to use this option to transfer a sample file to another computer.
Page 78 Elzone II 5390 Confirm Converting Sample Files Click Export ; the file is exported automatically to the export directory. Access the Export directory to retrieve the exported file(s). Converting Sample Files The Convert function enables you to convert two different file types to a format compatible with the current Elzone program.
Page 79 Converting Sample Files Elzone II 5390 Confirm Select the file, then click Convert . If converting multiple files, hold down the Ctrl key while selecting the files. A conversion dialog containing conversion results is displayed. Click here to close the dialog.
Page 80 Elzone II 5390 Confirm Converting Sample Files Select the file, then click . If converting multiple files, hold down the Ctrl while selecting the files. The Select Parameters for Converting (file name) dialog is displayed. This dialog enables you to select the type of data contained in the text file. If you have selected multiple files, a dialog is displayed for each file (the name of the file is in the header).
Page 81 Generating Graph Overlays Elzone II 5390 Confirm Generating Graph Overlays Use graph overlays when you wish to compare graphically results for multiple samples or multiple graphs for one sample. Graphical lines are differentiated by the use of varying symbols and reported in a legend on the report. If color output capability is available, dif- ferent colors are used instead of symbols.
Page 82 Elzone II 5390 Confirm Generating Graph Overlays Click the Report Options tab to display the Report Options dialog. Choose the desired graph and click Edit ; a graph options dialog like the following is displayed. Choose Samples from the drop-down list.
Page 83 Generating Graph Overlays Elzone II 5390 Confirm On the Report options dialog, click Overlays ; the Graph Overlay Samples dialog is displayed. Click Browse to the right of the Sample 1 field; the Plot Overlay Sample Selection dialog is displayed.
Page 84 Elzone II 5390 Confirm Generating Graph Overlays Multiple Graphs Overlay This option enables you to overlay two types of graphs from the same file. Select File > Open > Sample Information to display the Open Sample Information File dialog. Select the desired file, then click ;...
Page 85 Generating Graph Overlays Elzone II 5390 Confirm Click Edit ; the Report Options dialog enabling you to specify the plot to overlay is displayed. Make your selections and click to return to the graph options dialog, then again to return to the Report Options dialog.
Page 86 Elzone II 5390 Confirm Generating Graph Overlays Multiple Tests Overlay This option enables you to overlay all tests of the same file. Select File > Open > Sample Information to display the Open Sample Information File dialog. Select the desired file, then click ;...
Page 87 Generating Graph Overlays Elzone II 5390 Confirm Click Report ; one of the following occurs: • if you clicked Save to save specified overlay options, the Select Reports dialog is displayed. • If you did not click , a dialog stating that a preview report will be generated or Save you can cancel the operation is displayed.
Page 89 Description Elzone II 5390 Confirm 4. FILE MENU The File menu contains options that allow you to manage sample files, parameter files, and templates. Description Listed below are brief descriptions of the File menu options. Detailed descriptions follow this section Enables you to create a sample information or parameter file.
Page 90 Elzone II 5390 Confirm Description Save As Template Enables you to save the values from the open file as a template for a sample information or parameter file. Page 4-57. Save All Saves all open files. Page 4-57. Close Closes the file in the active window. Page 4-57.
Page 91 Elzone II 5390 Confirm New allows you to create a sample information or parameter file. Regardless of the type of file you are creating, a dialog allowing you to choose a template is displayed. Title bar indicates type of file you are creating.
Page 92 Elzone II 5390 Confirm Sample Information Sample Information files contain information used to control the analysis. Therefore, an analysis cannot proceed until it has been assigned a sample information file. A sample information file consists of: • Sample information • Analysis conditions •...
Page 93 Elzone II 5390 Confirm Sample This field defaults to the description of the template. You must enter a new description or edit the existing one; the Confirm program does not allow duplicate descriptions. The description you enter in this field appears in the Files list window on the Open Sample Information dialog.
Page 94 Elzone II 5390 Confirm Dilution Factor Enables you to enter the ratio of sample volume to elec- trolyte volume. This value can be easily determined using the following formula: sample volume electrolyte volume --------------------------------------------------------------------------------------------------- - sample volume Mass Concentration Enter the mass concentration of the sample you are ana- lyzing.
Page 95 Elzone II 5390 Confirm Reports to Generate Displays a list of available reports. Reports preceded by a check mark are those that have been selected for the cur- rent template. To select additional reports, simply dou- ble-click on the desired report. Alternatively, you can highlight the report and press the .
Page 96 Elzone II 5390 Confirm Developer The Sample Information dialog displays in a manner similar to that of an index card file for a Developer. Each parameter has its own tab and is accessed by clicking the tab. Or, you can use to move back and forth through the dialogs.
Page 97 Elzone II 5390 Confirm Bar code This field enables you to enter bar code information. If bar code information is not being used, you can use this field to enter additional information about the sample; for example, you may wish to enter the lot number of your sample.
Page 98 Elzone II 5390 Confirm Enter the mass per unit volume (in grams per L) for the Mass Concentration sample you are analyzing. Comments Use this field to enter any comments about the sample or the analysis conditions that you wish to note. Comments entered here are printed in the header of some reports.
Page 99 Elzone II 5390 Confirm Save Displays the Save as Sample Information File dialog (shown on page 4-7). This dialog allows you to choose the directory in which to save the file. The Save push button becomes enabled allowing you to complete the save operation after you make an entry in the Comments window.
Page 100 Elzone II 5390 Confirm Analysis Conditions An Analyst is not authorized to create Analysis Conditions files. This dialog allows you to specify analysis conditions for your sample. You can create an Analysis Conditions file as an independent parameter file or as part of a sample information file.
Page 101 Elzone II 5390 Confirm Orifice Tube This drop-down list contains existing orifice tubes. If the orifice tube has not been calibrated, its name (descrip- tion) is preceded with an asterisk (*). The diameter of the selected orifice tube is displayed adjacent to the Ori- fice Tube field.
Page 102 Elzone II 5390 Confirm If you choose Specify Diameter range on the Analysis Conditions dialog, the fields on this dialog are disabled and display the settings automatically set by the software. If you feel the settings are inappropriate, you can select Use instrument settings and edit the values as required.
Page 103 Elzone II 5390 Confirm Keep size range  If this option is selected, you can adjust the current and constant gain only. Each time you edit one, the other is automati- cally adjusted to keep the range constant for the selected ratio.
Page 104 Elzone II 5390 Confirm Stirrer Speed Allows you to specify a stirrer speed (or pulse rate). The lower the number, the lower the speed; 0 (zero) turns the stirrer (or hydropulser) off. Stirrer Direction Enables you to specify a direction for particle circulation.
Page 105 Elzone II 5390 Confirm Blockage You can choose to have blockages detected and cleared during analysis (default) and/or at the start of the analy- sis. Pump and fan off during  Turns the pump and fan off during data collection. You...
Page 106 Elzone II 5390 Confirm Calibration Displays the date and time for the type of calibration selected. Click Change to choose a different type of calibration; the Calibration Type dialog is displayed. Reference material measurement Uses data from a reference material measurement.
Page 107 Elzone II 5390 Confirm Correct for  Select this option to have coincidence correction applied. Coincidence It is always possible that two or more particles may pass through the orifice at the same time, this is known as coincidence. Coincidences cause a portion of the true dis- tribution to be absent and a distorted distribution of over- size, spurious particles.
Page 108 Elzone II 5390 Confirm Smoothing Select Smooth Data to reduce data scattering. Use the Groups of drop-down list to choose the number of size classes to be included. The smoothing process defaults to 1; however, you can have it repeated by choosing 2 from the Repetitions drop-down list.
Page 109 Elzone II 5390 Confirm Total count Analysis ends when the specified number of particles over the entire range is reached. Modal count Analysis ends when the specified number for the particle size is reached. Save Displays the Save as Analysis Conditions File dialog...
Page 110 Elzone II 5390 Confirm Material Properties An Analyst is not authorized to create Material Properties files. This dialog allows you to specify the properties of the sample material being analyzed and the electrolyte solution in which it is dispersed. You can create a Material Properties file as an independent parameter file or as part of a sample information file.
Page 111 Elzone II 5390 Confirm Sample Material Displays a list of available sample materials. After you select a sample material from the list, its description and properties are displayed. Description Displays the sample material you select from the list. This field is also used to add sample materials to the list.
Page 112 Elzone II 5390 Confirm Dispersion Enables you to enter pertinent information about the dis- persion. The information you enter in this window appears in the Options report. Save Displays the Save as Materials Properties File dialog (see page 4-21 for an example of this dialog).
Page 113 Elzone II 5390 Confirm Report Options An Analyst is not authorized to create Report Options files. This dialog enables you to select report options. You can create a Report Options file as an independent parameter file or as part of a sample information file. You can also save...
Page 114 Elzone II 5390 Confirm Show report title Select this option to have a title appear at the top of your report; use the adjacent field to enter the text. You can enter up to 40 characters. Show graphic Select this option to have a graphic (bitmap or enhanced metafile) display above the report title.
Page 115 Elzone II 5390 Confirm Specification Displays the Specification Samples dialog so that you can specify the sample files to be used for the boundaries of the coarse and fine specifications; produces an Out of Specification report. Then you can quickly determine if the results of the current sample are within the specified boundaries.
Page 116 Elzone II 5390 Confirm Overlays After choosing the desired files, be sure to edit the type (continued) of graph you are overlaying and choose the Overlay samples option. Peaks Displays the Peak Detection Settings dialog, allowing you to choose how peaks are detected.
Page 117 Elzone II 5390 Confirm Auto where a = the smaller peak (continued) b = lowest point between the two peaks If the depth is greater than the value you enter as the minimum, the two peaks are treated as separate;...
Page 118 Elzone II 5390 Confirm Save Displays the Save as Report Options File dialog (see page 4-21 for an example of this dialog). If the Save push button is not enabled, a file with the same ID currently exists. You must edit the identification of the current file before it can be saved.
Page 119 Elzone II 5390 Confirm Graphs All graph report options are similar and are edited in the same manner. Click for a Edit selected graph report; a dialog similar to the following is displayed. Data Plot From this group, choose the type of plot desired.
Page 120 Elzone II 5390 Confirm Samples Enables you to overlay the current curve with the same type of curve from multiple sample files. Click Overlays on the Report Options dialog to choose the sample file(s) containing the desired curves. Tests Enables you to overlay the same type of curve from all tests performed with this file.
Page 121 Elzone II 5390 Confirm Editing Tables Select a table to edit; a dialog similar to this one is displayed. The table and editing push buttons do not display if you are editing the Standard Class Size or Standard Sieve Table.
Page 122 Elzone II 5390 Confirm Insert Inserts a point above the selected point.  to add points at the beginning of the table and Ctrl to add points at the end of the table. Ctrl Not included on the dialogs for the Standard Class Size Table and the Standard Sieve Table.
Page 123 Elzone II 5390 Confirm Log Probability Report The Log Probability Report provides a comparison of the collected data to that of a log- normal distribution; it cannot be edited. Summary Report The Summary report provides a condensed listing of analysis statistics and data results.
Page 124 Elzone II 5390 Confirm Percentiles Displays the Summary Percentiles dialog. This dialog allows you to report the particle diameter (or radius) corresponding to each specified coarser (or finer) percentile. You can enter up to 10 values in any order. If you enter zero (0.00), a blank line is shown on the...
Page 125 Elzone II 5390 Confirm Peaks Displays the Summary Peaks dialog. This dialog enables you to specify the types of data to display in the columns of the peak table. Column 1 is fixed and cannot be edited. Sample Choose the sample parameters you wish to include in the report.
Page 126 Elzone II 5390 Confirm Background Report Select Background to edit; the Background Options dialog is displayed. Overlay backgrounds Choose this option to overlay the background of this sample analysis with the background(s) of other analyses. Click Overlays on the Report Options dialog to choose the files containing the backgrounds you wish to overlay.
Page 127 Elzone II 5390 Confirm Pulse Length vs. Particle Size Report Select Pulse Length vs. Particle Size to edit; the Pulse Length vs. Particle Size Report Options dialog is displayed. This dialog enables you to specify a variable for the x- and y-axes. You must also ensure that the pulse length and particle size data are stored to obtain this report.
Page 128 Elzone II 5390 Confirm Pulse Length Report Select Pulse Length to edit; the Pulse Length Report Options dialog is displayed. When generating this type of report, you must choose Full Resolution data (page 4-20) on the Data Setup dialog before analysis.
Page 129 Elzone II 5390 Confirm Autoscale Select this option to have the X- and/or Y-axis scaled automatically. Both axes begin at zero; the highest values collected during analysis are the ending points. If you deselect this option, the adjacent fields become enabled so that you may specify a range.
Page 130 Elzone II 5390 Confirm Combined Report Select the Combined Report to edit; the Combined Report Options dialog is displayed. The list of reports for the Combined Report is almost identical (the Combined report, of course, is not included in this list) to the list of reports generated in the normal manner.
Page 131 Elzone II 5390 Confirm Collected Data The tab for Collected Data does not appear on the Developer’s Advanced dialog presentation until after analysis. Table Displays data points for the current test selected from the Test drop-down menu. Test Displays the current test for this sample file. If you wish to view data for another test, click on the down arrow to select the desired test.
Page 132 Elzone II 5390 Confirm Full scale volume Select this option if you analyzed part of the sample by percent another method but you do not wish to merge the results with the reports for the current test. Specify the volume percent of the sample actually analyzed by the analyzer versus the percent that is manually analyzed.
Page 133 Elzone II 5390 Confirm From Graph This option enables you to choose a size range marked on the graph by a set of cross hairs. This button does not become enabled until you have marked the range. Simply click in the graph at the point you wish to begin the range to place the first cross hair.
Page 134 Elzone II 5390 Confirm Save Displays the Save as Sample Information File dialog (see page for an explanation of this dialog). If this is not the first time the file has been saved, a dialog prompting you for a reason for the change is displayed.
Page 135 Elzone II 5390 Confirm Entered Data An Entered Data tab displays when you select Manually entered on the Sample information dialog. The dialog for Entered Data enables you to enter data as opposed to having it collected automatically during analysis.
Page 136 Elzone II 5390 Confirm Save Displays the Save as Sample Information File dialog (see page for an explanation of this dialog). If this is not the first time the file has been saved, a dialog prompting you for a reason for the change is displayed.
Page 137 Open Elzone II 5390 Confirm Open Open enables you to open an existing sample or parameter file, as well as a sample or parameter template. Sample Information File The following dialog displays for the Analyst and Developer when File > Open >...
Page 138 Elzone II 5390 Confirm Open Status This drop-down list allows you to choose the types of sample files to display in the Files window. All files of the type you choose, within the range of dates, and in the current directory are displayed. Refer to Table 2-2.
Page 139 Open Elzone II 5390 Confirm Developer When a Developer opens a sample information file, the dialog displays in this manner: A Developer can view all parameters of the file, as well as edit certain parameters; those parameters are enabled. Report options can also be edited and reports generated.
Page 140 Elzone II 5390 Confirm Open Templates Sample and Parameter templates can be opened and their contents viewed by a Developer or an Analyst. However, you cannot make changes to an existing template. If you wish to make changes, a Developer will have to create a new template. An Analyst is not authorized to create templates.
Page 141 Open Elzone II 5390 Confirm Parameter A Developer or an Analyst can view the contents of a Parameter Template by selecting File > Open > (parameter); in this example Analysis conditions is chosen as the parameter. The Open Analysis Conditions Template dialog is displayed.
Page 142 Elzone II 5390 Confirm Open Parameter Files Parameter files (Analysis Conditions, Material Properties, and Report Options) can be opened only by a Developer. When you select File > Open > (parameter file), an Open (parameter) dialog is displayed. Title bar displays the type of file you are opening.
Page 143 Save Elzone II 5390 Confirm Save Save enables you to save any changes made to the file in the active window. The file is saved under its current name. If a sample information file is in the active window, a dialog requesting a comment on the change is displayed.
Page 144 Elzone II 5390 Confirm Save As Enter a description in the ID field; you can use up to 50 characters. You must also enter a comment in the Comment window to enable the Save push button. If the Save push button does not become enabled, a file with the same description already exists.
Page 145 Save As Template Elzone II 5390 Confirm Save As Template An Analyst is not authorized to create sample and parameter file templates. Save As Template is unavailable for an Analyst; a Developer can use this function to: • save the values of the sample file in the active window as a sample template •...
Page 146 Elzone II 5390 Confirm Close All Close All Close All enables you to close all open files under their current names. The following message displays for every file containing changes that have not been saved: (file name) has been changed. Save changes before closing?
Page 147 Print Elzone II 5390 Confirm Print Print enables you to print details of a sample file, sample template, or parameter file. For example, if you choose to print the contents of an analysis conditions file, you will receive the parameters used for all analysis conditions associated with the file.
Page 148 Elzone II 5390 Confirm Print Preview Choose Preview to view the file on the computer screen; Print you can then print the file from the preview window. Export Choose Print to send the file directly to the printer; you can print up to 4 copies.
Page 149 Print Elzone II 5390 Confirm Parameter Files and Templates The contents of a parameter file can be printed only by a Developer. The contents of parameter file templates can be printed by a Developer or an Analyst. This type of dialog displays for a Developer.
Page 150 Elzone II 5390 Confirm List List List enables you to list the following statistics for a selected sample file, parameter file, or a sample template. • File name • Date the file was created • Time the file was created •...
Page 151 Import Elzone II 5390 Confirm Import An Analyst is not authorized to import sample and parameter files. A Developer can use this option to import files that have been created external to the Confirm software and copied into the Import directory. If the files are not copied into the Import directory, they will not display in the Files window Use Windows Explorer to copy the files into the Import directory.
Page 152 Elzone II 5390 Confirm Export Export An Analyst is not authorized to Export sample files. A Developer can use the Export option to: • export the entire sample file to the Export directory. For example, you may wish to use this option to transfer a sample file to another computer.
Page 153 Convert Elzone II 5390 Confirm Convert An Analyst is not authorized to convert sample files. Convert allows a Developer to convert, two types of files: • Elzone: copies and converts data from sample files used with the Model 5380 Series of analyzers •...
Page 154 Elzone II 5390 Confirm Convert Category  Use these drop-down lists to choose a location for the Subcategory converted file(s). Refer to Add Archive Location, page for information on creating directories. These drop- down lists do not display when importing parameter files.
Page 155 Blend Elzone II 5390 Confirm Blend Blend enables you to merge data from multiple analyses in which different orifice tubes were used. A single orifice tube is capable of measuring particles within a certain size range. You can use multiple orifice tubes to measure the distribution over a wider range.
Page 156 Elzone II 5390 Confirm Blend Show Blend Select this option to blend the data from all files and plot the graph as if it were one distribution. Show Overlays Plots the data from each file as overlays. Size Classes Defaults to the number of size classes for the first data set (field 1);...
Page 157 Average Elzone II 5390 Confirm Average Average enables you to choose up to five sample files and average the data from all files. Or, you can choose Add to add and combine the data from the selected files. A graph is drawn on the right side of the dialog and updates automatically each time a file is added (or removed).
Page 158 Elzone II 5390 Confirm Average Enables you to obtain a total of all data sets in the selected sample files. Average Enables you to obtain an average for all data sets in the selected sample files. Save As Allows you to save the data as a sample file.
Page 159 Log In Elzone II 5390 Confirm Log In Log in enables you to log into the application; the User Log in dialog is displayed. Simply enter your user name and password, then click O User name Typically in this field, you should enter your Windows User name, unless your Administrator has specified a dif- ferent user name.
Page 160 Elzone II 5390 Confirm Log Out Log Out Select this option to log out of the system. If files are open and contain changes that have not been saved, you are prompted to save or discard them before you can log out.
Page 161 Description Elzone II 5390 Confirm 5. UNIT MENU The Unit menu contains the operations which can be performed with the Elzone analyzer. The main menu contains a Unit menu for each attached analyzer. For example, if you have two attached analyzers, the main menu contains two Unit menus. The unit number and the serial number appear in the title bar of the operational window(s).
Page 162 Elzone II 5390 Confirm Description QuickStart Analysis Use this mode of operation to perform successive sample analyses. Page 5-14. Change Orifice Tube or  Enables you to change the orifice tube or the liquid. Page Liquid 5-19. Rinse Enables you to rinse the system (internal glassware).
Page 163 Calibration Enables you to perform certain instrument calibrations. The options on this menu are enabled only with the direc- tion of a Micromeritics service representative. 5-49. Service Test Allows you to perform certain troubleshooting proce- dures. This option is enabled only under the direction of a Micromeritics service representative.
Page 164 Elzone II 5390 Confirm Sample Analysis View Allows you to view one of the following in the current window: • the current operation • the instrument schematic • the instrument log Displays the Create a File for Analysis dialog, allowing you to choose a template from which to create a new file.
Page 165 Sample Analysis Elzone II 5390 Confirm Orifice Tube Displays a description of the orifice tube specified in the Analysis Conditions file. If the identification is preceded with an asterisk, the orifice tube has not been calibrated for this instrument. Orifice tubes should be calibrated to obtain accurate results.
Page 166 Elzone II 5390 Confirm Sample Analysis Allows you to enter the number of analyses you wish to Number of tests perform using this sample file; you can perform up to eight tests with each file. This option enables you to have the data collected in this Background analysis saved as a background.
Page 167 Sample Analysis Elzone II 5390 Confirm Preview Prints the report to the monitor screen. This option allows you to customize reports with details such as font and column placement. Refer to Onscreen Reports, page for the options available for onscreen reports.
Page 168 Elzone II 5390 Confirm Sample Analysis Next Click this push button to advance to the next view of the Analysis dialog; a logon dialog is displayed. This dialog is used to verify that the logged-in user is per- forming the analysis.
Page 169 Sample Analysis Elzone II 5390 Confirm Report Enables you to generate a report for the data collected up to the time you request the report. Sparkle Display Displays during data collection or while in Preview mode. The Sparkle display emulates an oscilloscope (turned 90º...
Page 170 Elzone II 5390 Confirm Sample Analysis Optimize Settings Enables you to have the optimum Load Resistor, Current, and Gain determined. These values will be stored in the analysis conditions file as well as in the collected data, and as the optimized settings for the orifice/electrolyte combination.
Page 171 Sample Analysis Elzone II 5390 Confirm From Graph This option enables you to choose a size range marked on the graph by a set of cross hairs. This button does not become enabled until you have marked the range. Simply click in the graph at the point you wish to begin the range to place the first cross hair.
Page 172 Elzone II 5390 Confirm Sample Analysis Enables you to start or continue (when stopped) data col- Start/Continu lection. Stop Stops data collection. Clear Discards all data collected for this analysis. This action is recorded in the instrument log. Save Enables you to save the collected data into the sample file as the next test.
Page 173 Sample Analysis Elzone II 5390 Confirm Click Start to begin the analysis; data starts to collect and the dialog now looks like this: Becomes enabled when progress bar shows 100%. Progress Bar After data are collected (progress bar reaches 100%),...
Page 174 Elzone II 5390 Confirm QuickStart Analysis QuickStart Analysis Use this mode of operation to analyze a series of samples of the same type which contain the same analysis conditions; sample files are created automatically. When you select this option from the Unit menu, the QuickStart dialog is displayed.
Page 175 QuickStart Analysis Elzone II 5390 Confirm Export after Analysis Select this option to export full-resolution data or reduced data automatically after analysis. Refer to page for an explanation of export output options. Next Advances you to the next view of the QuickStart dialog.
Page 176 Elzone II 5390 Confirm QuickStart Analysis Measure Conductivity Select this option to measure the conductivity for the current orifice tube and liquid. The date and time of the last recorded measurement for this tube/liquid combination displays to the right of the push button.
Page 177 QuickStart Analysis Elzone II 5390 Confirm Indicates maximum (value in right Indicates 0 to minimum (value in left range field) to 10000. range field) Indicates minimum to maximum (range specified in the range fields). The bar will be colored up to the measured concentra- tion.
Page 178 Elzone II 5390 Confirm QuickStart Analysis This view of the dialog displays the data as they are collected. Sparkle Display Displays during data collection. The Sparkle display emulates an oscilloscope (turned 90º to the right). The analyzer measures the change of resis- tance across the orifice and displays a dynamic scan of pulses (tips) in real time.
Page 179 Change Orifice Tube or Liquid Elzone II 5390 Confirm Change Orifice Tube or Liquid This option enables you to change the orifice tube or liquid; the Change Orifice Tube or Liquid dialog is displayed. This dialog is the first of a series of dialogs that guide you through the process of chang- ing the orifice tube or liquid.
Page 180 Elzone II 5390 Confirm Rinse Rinse This option enables you to rinse the system (internal glassware); the Rinse dialog is displayed. Drain and fill Choose this option to drain, rinse, and refill the system with liquid. Flush Choose this option to flush the system with liquid; liquid remains in the glassware at all times.
Page 181 Fill System Elzone II 5390 Confirm Fill System This option enables you to fill a drained system (internal glassware) with liquid. Before selecting this option, place a beaker of electrolyte on the sample stand and raise the stand. Start Click this push button to begin filling the beaker.
Page 182 Elzone II 5390 Confirm Drain System Drain System This option enables you to drain the liquid from the system; the Drain System dialog is displayed. Before selecting this option, be sure that the sample stand is in its lowest position; your orifice tube should not be submerged for this operation.
Page 183 Orifice Tube Calibration Elzone II 5390 Confirm Orifice Tube Calibration This option enables you to calibrate an orifice tube to a selected sample and electrolyte solution. A sample file for the calibration is created automatically and stored in the calib/ serial number subdirectories, which are located in the data subdirectory of the applica- tion.
Page 184 Elzone II 5390 Confirm Orifice Tube Calibration Click Next to advance to the next view of the calibration dialog. Be sure the reference materials required in the calibration are checked. View Allows you to view one of the following in the current window: •...
Page 185 Orifice Tube Calibration Elzone II 5390 Confirm Displays the Reference Material dialog so that you can add a new reference material to the list. The information required in these fields can be found on the reference material bottle or its accompanying booklet.
Page 186 Elzone II 5390 Confirm Orifice Tube Calibration Electrolyte Solution Displays a list of available electrolyte solutions (dispers- ing liquids). After you select a solution from the list, its description and properties are displayed. Description Displays the electrolyte solution you select form the list.
Page 187 Orifice Tube Calibration Elzone II 5390 Confirm Save Enabled when the calibration is complete (progress bar reaches 100%) allowing you to save the data. Finish Displays the Finish Analysis dialog. Be sure 0 (zero) is displayed here. Indicates the data were saved.
Page 188 Elzone II 5390 Confirm Orifice Tube Calibration The values on the right side of the dialog are specific to a reference material. The refer- ence material is selected from the drop-down list just above the information. Report Generates the calibration report to the computer screen.
Page 189 Orifice Tube Calibration Elzone II 5390 Confirm From Graph This option enables you to: • set the pulse height at the position of a single cross hair  Simply click in the graph at the desired location for a single cross hair, then click From Graph •...
Page 190 Elzone II 5390 Confirm Orifice Tube Calibration Fit Order Enables you to choose the highest order for the polyno- mial fit. If the fit is invalid, the order will decrease to the next lowest selection and refit. The coefficients of the polynomial fit are displayed on the left side of the dialog.
Page 191 Background List Elzone II 5390 Confirm Background List The software maintains a list of backgrounds performed on the analyzer; the Maintain Backgrounds dialog is displayed. Orifice Tube Contains a list of the orifice tubes that have been used with the analyzer.
Page 192 Elzone II 5390 Confirm Zero Pressure Scale List All Generates a report of the window contents to the screen, enabling you to print or save the list. Close Closes the dialog. Zero Pressure Scale This option enables you to zero the pressure transducer to atmospheric pressures; the Zero Pressure Scale dialog is displayed.
Page 193 Diagnostics Elzone II 5390 Confirm Diagnostics This option enables you to perform a diagnostic test to determine if the signal processing circuitry is operating properly. This test actually emulates an analysis sending electronic pulses through a series of predefined ranges. Your service representative may request this test when data results are inaccurate and you have been unable to resolve the problem.
Page 194 Elzone II 5390 Confirm Diagnostics Report after test Select this option to have a report generated automati- cally after the test; page provides an explanation of output options. If you do not select this option, you can still have a report generated from the report window.
Page 195 Diagnostics Elzone II 5390 Confirm Next Returns you to the first view of the Service Test window. Close Closes the dialog. 539-42822-01 (Rev A) - Nov 2017 5-35...
Page 196 Elzone II 5390 Confirm Enable Manual Control Enable Manual Control Select this option to manually control the system. Manual control typically is only used for service issues; normal operation does not require manual control. If the instrument schematic is not displayed, select Show Instrument Schematic from the Unit menu.
Page 197 Enable Manual Control Elzone II 5390 Confirm A component is selected when it is surrounded by a dotted line. Each component has a shortcut menu displaying the operations available for that paticular component. These menus may be accessed by right-clicking on the desired component, or by using the shortcut keys when the component is selected.
Page 198 Elzone II 5390 Confirm Enable Manual Control Volumetric pump Move Volume displays a dialog enabling you to specify flow direction, the total volume to move, and the flow rate. Arrow (continued) Move Steps displays a dialog enabling you to specify flow direction, the number of steps to move, and the rate at which to move the steps.
Page 199 Enable Manual Control Elzone II 5390 Confirm Stirrer/Orifice tube A stirrer or optional hydropulser is used to maintain par- ticle suspension in the sample beaker. The current speed Electrodes Stirrer is displayed in the icon. Actions: Turn On (green) Turn Off (yellow)
Page 200 Elzone II 5390 Confirm Enable Manual Control Servo valve Regulates system vacuum pressure. Actions: Turn On Turn Off Vent Set Target Flow Vent allows air into the system. Set Target displays the Set Target dialog enabling you to specify a target differential pressure.
Page 201 Enable Manual Control Elzone II 5390 Confirm Sensors There are two sensors displayed on the schematic; one for the waste container and one for overflow of the waste container.  Colors: White; indicates no liquid present at the sensor level ...
Page 202 Elzone II 5390 Confirm Show Instrument Schematic Show Instrument Schematic Select this option to display a schematic of the Elzone analyzer. You can determine the state of the valves and pumps by color. • Valves: Closed = White* Open = Green •...
Page 203 Show Status Elzone II 5390 Confirm Show Status Select this option to show only the status window of an operation in progress. You may wish to use this option if: • You have an automatic operation in progress and you wish to edit a sample file, for example.
Page 204 Elzone II 5390 Confirm Show Instrument Log Show Instrument Log Select this option to display a log of recent analyses, calibrations, errors or messages, and conductivity details. By default, information for analyses and messages are retained 60 days; calibration and conductivity information is retained 90 days. You may change the time for which this information is retained in the Unit section of the WIN5390.INI file.
Page 205 Show Instrument Log Elzone II 5390 Confirm Start Date Use this field to specify a date at which to begin listing entries. You can specify a start date using any of the fol- lowing methods: • Highlight the field (or press to clear the field) and type in the desired date.
Page 206 Elzone II 5390 Confirm Show Instrument Log Conductivity Report Enables you to display on the screen or print a report of conductivity for a selected orifice tube and electrolyte solution; the Conductivity Report Settings dialog is dis- played. The Orifice Tube and Electrolyte solution drop-down lists enable you to choose the combination desired.
Page 207 Unit Configuration Elzone II 5390 Confirm Unit Configuration Select this option to display software/hardware configurations for the selected analyzer. When you select Unit Configuration from the Unit menu, the Unit Configuration dialog is displayed. Software Versions Displays the software versions for components being used by the analyzer.
Page 208 Displays the Unit IP Setup dialog. Change This dialog shows the IP address and Subnet mask that were assigned during installation. Do not edit these num- bers unless directed by a Micromeritics service representative. 5-48 539-42822-01 (Rev A) - Nov 2017...
Page 209 Calibration The Calibration option provides a method of storing instrument calibration data. Your Micromeritics service representative may use this option to enter calibration data or per- form component calibrations for future reference when servicing the analyzer. This option is enabled only when the analysis program is operating in Service Test mode...
Page 211 Description Elzone II 5390 Confirm 6. REPORTS MENU The options on the Reports menu enable you to generate reports on: • sample analyses • orifice tube calibrations • statistical process control parameters • historical particle size distribution This chapter provides a description of these options, as well as sample copies of some of the reports available with the Elzone program.
Page 212 Elzone II 5390 Confirm Description Allows you to generate a regression report. Page 6-11. Regression Report Control Chart Allows you to generate a control chart report. Page 6-15. PSD History Allows you to generate a particle size distribution history report. Page 6-19.
Page 213 Start Report Elzone II 5390 Confirm Start Report Select this option to generate a report on a sample analysis. Select Start report from the Reports menu to display the Start Report dialog Category/Subcategory Use these drop-down lists (directories) to navigate to the desired file(s).
Page 214 Elzone II 5390 Confirm Start Report Preview Choose this option to have the report(s) generated to the screen. If a printed copy is desired, you can print the report from the report window. Options for customizing and fine-tuning data are avail- able for onscreen reports (page 6-22).
Page 215 Start Report Elzone II 5390 Confirm If you choose a single sample file, the Selected Reports dialog is displayed when you click Report . The reports selected are the ones you specified in the sample file. This dia- log allows you to deselect reports or select additional ones.
Page 216 Elzone II 5390 Confirm Close Reports Close Reports This option enables you to close all open report windows at one time. This avoids having to select close on each report window. Open Report This option enables you to open a report that has been saved from the Report window; the Report window opens with an Open dialog positioned on top.
Page 217 Orifice Tube Calibration Elzone II 5390 Confirm Orifice Tube Calibration This option enables you to generate a report on an orifice tube calibration; the Start Ori- fice Tube Report dialog is displayed. Not displayed for an Analyst. Instrument Drop-down list containing the serial number of the instrument(s) installed on the current computer.
Page 218 Elzone II 5390 Confirm SPC Report Options SPC Report Options When you select SPC Report Options, the SPC Calculations dialog is displayed. Displays the range for the selected field. Test This drop-down list contains analysis choices for SPC calculations. Last reports statistics for the last analysis performed.
Page 219 SPC Report Options Elzone II 5390 Confirm Sample Displays the Sample SPC Options dialog, allowing you to select the sample parameters you wish to have reported. Specific parameters can be designated for the fields labeled Parameter [n]. Refer to Edit...
Page 220 Elzone II 5390 Confirm SPC Report Options Sizes Displays the SPC Size Options dialog, allowing you to specify up to 10 sizes and 5 distribution types at which the cumulative percent finer (or coarser, depending on the selection in the Units dialog) is to be reported.
Page 221 Regression Report Elzone II 5390 Confirm Regression Report Select this option to generate a regression report. The regression report is used to deter- mine the interdependency between two variables. Up to three dependent variables (Y- axis) may be plotted against a single independent variable (X-axis). The degree of corre- lation between the variables also is reported.
Page 222 Elzone II 5390 Confirm Regression Report X- and Y-Axes  Allows you to designate the X- and Y-axes variables. Variable fields Click on the down arrow to display a list of variables. The variables in this list are the ones you specified in the SPC report options.
Page 223 Regression Report Elzone II 5390 Confirm Category Drop-down lists containing current directories. The Cat- Subcategory egory represents the Directory, and the Subcategory rep- resents the Subdirectory of the selected Directory. Status This drop-down list determines the type of sample files...
Page 224 Elzone II 5390 Confirm Regression Report Moves the selected file to the Selected Files pane. Alter- natively, you can simply double-click on the desired file(s). You can select multiple files by holding down Ctrl while making your selections. You can include up to 200 sample files.
Page 225 Control Chart Elzone II 5390 Confirm Control Chart This option enables you to generate a control chart report which plots the changes in a statistic. Not displayed for an Analyst. Select this option to have a title display on your report.
Page 226 Elzone II 5390 Confirm Control Chart X-axis Order by Time places the files on the graph at numerical points in the order of the date/time the files are analyzed. (continued) File name places the files on the graph at numerical points in alphanumeric order.
Page 227 Control Chart Elzone II 5390 Confirm Limit Lines Displays the options available for limiting lines. You can have the lines placed at some multiple of the standard deviation or at specified positions (Entered). When you select Entered, the High limit and Low limit fields are enabled, allowing you to enter appropriate val- ues.
Page 228 Elzone II 5390 Confirm Control Chart Summary Statistics Allows you to select the statistics to display in the report. Coefficient of Variation is the Standard Deviation divided by the Mean. Confidence Interval of the mean value (shown on the same line below the graph on the report). When you select this option, the Confidence Level field is enabled allowing you to enter the percentage.
Page 229 PSD History Elzone II 5390 Confirm PSD History This option enables you to report a sequence of full particle size distribution graphs. Not displayed for an Analyst.  Show report title Select this option to have a title display on your report.
Page 230 Elzone II 5390 Confirm PSD History This dialog functions in the same manner as the Regres- sion Report Sample Selection Dialog explained earlier in this chapter. Refer to page 6-12 if you need assistance on the fields of this dialog.
Page 231 Printed Reports Elzone II 5390 Confirm Printed Reports Header All printed reports (either to the screen or to a printer) contain a header displaying file statistics, as shown in this example. The report header may contain a graphic (such as a company logo) and/or title if speci- fied.
Page 232 Elzone II 5390 Confirm Onscreen Reports Onscreen Reports When you choose Preview as the report destination, reports are printed to the screen. Onscreen reports provide many options for customizing and manipulating reports: • a tool bar • shortcut menus • zoom feature •...
Page 233 Onscreen Reports Elzone II 5390 Confirm Tool Bar Reports Contains a list of all requested reports. Show Shows the selected report in the report window. If the report has been hidden, it and its associated tab will become visible. Delete Deletes the selected report.
Page 234 Elzone II 5390 Confirm Onscreen Reports Print A list of available reports is displayed in the window on (continued) the right side of the dialog For convenience in selecting which reports to print, push buttons are provided beneath the report window. Or, you can make your selection by clicking on the desired reports.
Page 235 Onscreen Reports Elzone II 5390 Confirm Default Style Displays the Default Style dialog so that you can edit report defaults. Fonts Contains a list of report elements for which the font can be edited. Simply highlight the desired element and click ;...
Page 236 Elzone II 5390 Confirm Onscreen Reports Shortcut Menus Shortcut menus are accessed when you right-click on the tabular or graphical portion of a report. Tabular Reports Resize column Displays a dialog so that you can specify the width of the selected column (in inches).
Page 237 Onscreen Reports Elzone II 5390 Confirm Edit title Allows you to edit the table title and font. Copy table as text Enables you to copy the entire table (column headers and data) and then insert it into another program. Columns...
Page 238 Elzone II 5390 Confirm Onscreen Reports Edit curve Displays the Curve Properties dialog, allowing you to edit curve properties. Title Displays the title of the curve you are editing. You can edit the title if desired. Style This drop-down list contains the styles in which collected data can be displayed.
Page 239 Onscreen Reports Elzone II 5390 Confirm Edit axis Displays the Axis Properties dialog, allowing you to edit axis properties. Title Displays the title of the axis you are editing; use the Title push button to edit font attributes if desired.
Page 240 Elzone II 5390 Confirm Onscreen Reports Edit title Displays the Title Properties dialog, allowing you to edit the current graph’s title and font. Copy as metafile Copies the graph and places it on the clipboard, allowing you to paste it into other applications accepting Windows metafiles.
Page 241 Onscreen Reports Elzone II 5390 Confirm Axis Cross Hair A cross-hair function is available so that you can view axis coordinates. To use this fea- ture, simply left-click in the desired area of the graph. X-axis position Point of Coordination...
Page 242 Elzone II 5390 Confirm Report Examples Report Examples The remainder of this chapter contains samples of some of the reports that can be gener- ated by the Elzone 5390 Confirm Program. Most of the reports can be varied through entries on the report options screens.
Page 243 Report Examples Elzone II 5390 Confirm Combined Report 539-42822-01 (Rev B) - Nov 2017 6-33...
Page 244 Elzone II 5390 Confirm Report Examples Incremental Number vs. Particle Diameter 6-34 539-42822-01 (Rev B) - Nov 2017...
Page 245 Report Examples Elzone II 5390 Confirm Incremental Volume Percent vs. Particle Diameter 539-42822-01 (Rev B) - Nov 2017 6-35...
Page 246 Elzone II 5390 Confirm Report Examples Standard Class Size Table 6-36 539-42822-01 (Rev B) - Nov 2017...
Page 247 Description Elzone II 5390 Confirm 7. OPTIONS MENU The choices on the Options menu allow you to configure the system to your laboratory’s requirements. With the options on this menu, you can: • Add directories • Edit labels for sample files and directories •...
Page 248 Liquid analysis match those of the previous analysis. Page 7-7. Service Test Mode Enables you to perform certain troubleshooting procedures. under the direction of a Micromeritics service representative. Page 7-8. 539-42822-01 (Rev A) - Nov 2017...
Page 249 Add Archive Location Elzone II 5390 Confirm Add Archive Location Archive locations (directories) can be added by an Analyst or a Developer; the Add Archive Location dialog is displayed. Category These fields allow you to create new directories and/or sub- Subcategory directories for the repository.
Page 250 Elzone II 5390 Confirm Edit Labels Edit Labels An Analyst is not authorized to edit sample file labels. Edit labels allows the Developer to edit the labels that display on the sample file editor; the Edit Labels dialog is displayed.
Page 251 Update File List Elzone II 5390 Confirm User Parameters Once specified, these parameters display on the sample editor (continued) and in the SPC Sample Options dialog (accessed through the SPC Report Options dialog). These fields can also be used to record analysis conditions or sample information so that it can be printed on the Summary report.
Page 252 Elzone II 5390 Confirm Invert Size Axis Invert Size Axis An Analyst is not authorized to invert the size axis. Select this option to invert the size axis. Graph Grid Lines Graph Grid Lines enables you to choose the type(s) of grid lines to show on your reports; the Graph Grid Lines dialog is displayed.
Page 253 Sieve Table Elzone II 5390 Confirm Sieve Table An Analyst is not authorized to specify sieve defaults. Displays the Sieve Table allowing you to specify default sieve sizes for sieve data. Indicates the size is selected. To select sizes, move to the desired size, then double-click the left mouse button or press Spacebar .
Page 254 Certain service tests are included in the operating program, but can be performed only with the assistance of a trained Micromeritics service representative. These tests are designed to provide your service representative with instrument readouts, as well as to assist him in trou- bleshooting potential problems and, perhaps, eliminating unnecessary repair services.
Page 255 Elzone II 5390 Confirm 8. TROUBLESHOOTING AND MAINTENANCE The Elzone II 5390 analyzer has been designed to provide efficient and continuous ser- vice. However, in order to obtain the best results over the longest period of time, certain maintenance and service procedures should be followed. This chapter contains informa- tion regarding common operational problems and corrective action, and maintenance and service procedures.
Page 256 • Drain System; if you use this option, be sure to refill the system • Fill System Faulty circuit board. Contact your Micromeritics service representative. The orifice tube is not filled Fill the orifice tube. completely. 539-42822-01 (Rev A) - Nov 2017...
Page 257 Troubleshooting Elzone II 5390 Confirm Problem Reason Solution System won’t fill. Waste container lid may not be Tighten lid on waste container, securely screwed onto the then try to fill the system. container. Supply tube may not be sub- Be sure the supply tube is com- merged in the Supply container.
Page 258 ElzoneII 5390 Confirm Preventive Maintenance Preventive Maintenance Table 8-2 lists the preventive maintenance procedures you should perform to keep your system operating at peak performance. Instructions for each procedure follow the table. Table 8-2. Preventive Maintenance Schedule Maintenance Required Frequency Maintain orifice condition, page Daily Clean the sample area, page...
Page 259 Preventive Maintenance Elzone II 5390 Confirm Preventing Orifice Blockages Sample materials are seldom sources of fibers or debris in sufficient amount to cause fre- quent blockages. If blockages do occur due to sample materials, you can “scalp off” debris by wet-sieving the prepared suspension through a clean mesh that is roughly 75% of the orifice diameter.
Page 260 ElzoneII 5390 Confirm Preventive Maintenance Cleaning the Sample Area For this procedure you will need the following: • Lint-free cloth • Isopropyl alcohol (IPA), mild detergent, or hydrogen peroxide solution Use a clean, lint-free cloth to wipe up spills as they occur. All surfaces of the analyzer should be kept clean and dry at all times.
Page 261 Preventive Maintenance Elzone II 5390 Confirm 5. Select Unit > Rinse to display the Rinse dialog. Select Drain and fill and enter 1 in the Rinses field (as shown in the dialog). 6. Click Start ; the dialog closes automatically when the rinsing operation is complete.
Page 262 ElzoneII 5390 Confirm Preventive Maintenance Replacing the Air Filter The air filter on the rear panel should be replaced every 30 days (more often in environ- ments with increased levels of dust). 1. Remove the filter by inserting a pointed object, such as a flat-blade screwdriver, into the outer edge of the retaining cover;...
Page 263 Preventive Maintenance Elzone II 5390 Confirm Cleaning Orifice Tubes Orifice tubes must be kept clean to ensure accurate analysis results. Follow the procedure below to clean an orifice tube when: • the orifice tube will not be used for at least one week •...
Page 264 ElzoneII 5390 Confirm Preventive Maintenance 3. Rinse off the detergent with water. 4. Rinse the inside and outside of the tube with acetone. 5. Let the tube dry and store it, or place it on the analyzer. Orifice tubes should be cleaned on a monthly basis as follows: 1.
Page 265 Clearing Blockages Elzone II 5390 Confirm Clearing Blockages Occasionally, a particle may become lodged in the orifice and cannot be cleared through the use of the software. Perform the following steps to manually clear a blockage from the orifice. 1. Click...
Page 266 You may have to hold the tube against a darker background to obtain a clear view of the stream of water. If the orifice is still blocked, call your Micromeritics Service representative. 12. Reinstall the orifice tube.
Page 267 Installing the Hydropulser Elzone II 5390 Confirm Installing the Hydropulser The hydropulser and stirrer are installed in the same location, the back wall of the sample compartment. These instructions are assuming you have a stirrer currently installed on your analyzer.
Page 268 ElzoneII 5390 Confirm Installing the Hydropulser 4. Turn the four captive thumb screws counterclockwise to loosen the stirrer assembly. 5. Slide the stirrer assembly out and store in a secure location for future use. 6. Insert the hydropulser assembly, ensuring that the back plate of the hydropulser assembly slides into the two slots inside the opening.
Page 269 Installing the Hydropulser Elzone II 5390 Confirm 9. Gently slide the external electrode back into its red connector. 10. Use the clip to attach the hydropulser tube to the orifice tube when performing an analysis. Retaining clip 539-42822-01 (Rev A) - Nov 2017...
Page 270 ElzoneII 5390 Confirm Installing the Hydropulser Cleaning the Hydropulser The hydropulser tube should be cleaned daily between sample analyses and more thor- oughly on a monthly basis, or when the hydropulser is not to be used for long periods of time.
Page 271 Installing the Hydropulser Elzone II 5390 Confirm Fill a squeeze bottle with clean, filtered electrolyte or water and thoroughly rinse the Do not squeeze electrolyte up hydropulser tube, the orifice tube, and the electrode. into the hydropulser tube. Do not squeeze electrolyte up into the hydropulser tube. Liquid may get into the hydropulser assembly and damage the assembly, or cause erratic results.
Page 272 ElzoneII 5390 Confirm Installing the Hydropulser Place the tube into a beaker of diluted detergent, then place the beaker into an ultrasonic bath for approximately five minutes. If an ultrasonic bath is not available, use a pipette or a syringe attached to the end of the tube;...
Page 273 The Elzone 5390 system components and accessories can be ordered using one of the follow- ing methods: • Call our Customer Service Department at (770) 662-3636 • Access our web site at www.micromeritics.com • Contact your local sales representative When ordering, please use the information provided below to place your order:...
Page 274 Elzone II 5390 Confirm Ordering Information Part Number Item and Description 539-33617-00 Orifice Tube Kit; includes one 300-m orifice tube, reference materials, and reference booklet 539-33618-00 Orifice Tube Kit; includes one 380-m orifice tube, reference materials, and reference booklet Reference material, 1 m; approx. 8 mL 004-16840-00 Reference material, 2 m;...
Page 275 Ordering Information Elzone II 5390 Confirm Part Number Item and Description 539-60804-01 Sensor cable, for supply liquid 539-25856-00 Clip, hydropulser tube 539-32803-04 Tubing, flexible, hydropulser 539-32802-08 Tubing, rigid, hydropulser 004-27015-00 Air filter (rear panel), package of 10 539-42822-00 Operator’s manual 539-33022-00 Software package, Elzone 5390;...
Page 277 Appendix A Elzone II 5390 Confirm A. ERROR MESSAGES This appendix contains a numerical listing of the error messages associated with the Elzone program. The 1000-series error messages (used primarily for software testing) are not included in this appendix. These errors should not occur during normal operation.
Page 278 Elzone II 5390 Confirm Appendix A 2334- Incorrect user name or password. Cause A: You entered an incorrect user name or password in the User Logon dia- log box. Action A: Reenter your user name and password. Ensure that Caps Lock is not enabled;...
Page 279 Appendix A Elzone II 5390 Confirm 2338- Your password has expired or needs to be changed. You will not be able to log in without changing the password. Cause: The allowed time using a password has expired. Action: Change your password.
Page 280 Elzone II 5390 Confirm Appendix A 2343- This password is already in use. Please enter a valid password. Cause: You attempted to change your password but entered one that has already been used. Action: Choose a different password. 2344- Application locked.
Page 281 Appendix A Elzone II 5390 Confirm 2400 Series 2401- FATAL ERROR: (Error message) Cause: An internal processing and/or hardware error has occurred. Action: Contact your service representative if you continue to receive this error message. 2430- Error accessing file (file name), error code = (number) Cause A: Hard disk may be damaged.
Page 282 Elzone II 5390 Confirm Appendix A 2433- New entries have been found in this directory. Refresh the directory information? Cause: Several files (sample information, analysis conditions, or report options) have been added to this directory by some function other than the AutoChem program.
Page 283 Appendix A Elzone II 5390 Confirm 2439- Could not register file. 2440- Subset not found. 2441- Seek within file failed. 2442- Had header in subset file. 2443- Subset owner denied access. 2444- Not a valid file format. 2445- Subset wrote the wrong amount of data.
Page 284 Elzone II 5390 Confirm Appendix A 2452- Attempt to write MICATTR.DIR in read only mode. File (file name). 2453- Attempt to append MICATTR.DIR in read only mode. File (file name) Cause: The Read-Only attribute is turned on in the application's MICATTR.DIR file (this file exists in each folder containing sample or...
Page 285 Ensure that the analyzer’s ethernet connections are properly connected. Stop and restart the analysis program. If the restarted application can- not establish communications with the analyzer, turn the analyzer off, then back on. If this error persists, contact your Micromeritics service representative. 2461- No instruments are in operation.
Page 286 Elzone II 5390 Confirm Appendix A 2477- Unit n - S/N: nnnn did not properly initialize. Cause A: There were communication problems between the computer and the analyzer. Action A: Check the communication cables and make sure they are connected securely.
Page 287 Appendix A Elzone II 5390 Confirm 2481- Error accessing the sample information file (name). Cause: An unexplained error prevents you from accessing this file. Action: The hard disk drive may be corrupt. Run diagnostics. 2482- File (file name) cannot be opened for writing. It is already in use.
Page 288 Elzone II 5390 Confirm Appendix A 2487- Cannot start report generator. Error code (number). Program will terminate. Cause: An internal processing and/or hardware error has occurred. Action: Contact your service representative if you continue to receive this mes- sage. 2488- File (file name) cannot be opened for editing.
Page 289 Appendix A Elzone II 5390 Confirm 2493- An entry is required for this field. Cause: This field contains an invalid entry. Action: Enter or select an appropriate value. 2494- Value is out of the valid range. Cause: The value you entered in the highlighted field is outside the valid range of values.
Page 290 Elzone II 5390 Confirm Appendix A 2498- The requested change to the Sample’s status is invalid at this time. Cause: A request to change the file’s status (for example, from automatically collected to manually entered data) could not be done.
Page 291 A large number of windows are open and consuming the system resources available to all applications. Action: Close one or more windows on the screen. Contact your Micromeritics service representative if you continue to receive this error message. 2502- Error writing to file (name) during print. Error code: (number).
Page 292 Elzone II 5390 Confirm Appendix A 2506- (sample file) Output device (name) is not installed. Printing cannot be accomplished. Cause: The selected output device is not installed. Action: Install the device using the Control Panel, Printers operation. 2507- Error opening file (name) for printing. Error code: (number).
Page 293 Appendix A Elzone II 5390 Confirm Cause C: An internal processing error occurred. Action C: Contact your service representative. 2511- Print job (name) has been cancelled due to insufficient disk space. Delete unnecessary files and restart the report. Cause: The disk drive does not have enough space for the temporary file required by the Windows Print Manager.
Page 294 Calibration operations should only be done by or under the direction of qualified service personnel. 2516- Warning: Keeping a backup copy of the calibration data is recommended by Micromeritics. Would you like to do so now? Cause: You have performed a calibration operation; a backup copy is recom- mended.
Page 295 Controller debug port error. Cause: An internal processing and/or hardware error has occurred. Action: Contact your Micromeritics service representative if you continue to receive this error message. 2532- The instrument contains a different software version. Do you want to reset it?
Page 296 Elzone II 5390 Confirm Appendix A 2535- The requested directory is not a repository location. Resetting to the default location. Cause: The directory last accessed is no longer available; the application defaults to the default location. Action: Choose an appropriate directory to select a file.
Page 297 Appendix A Elzone II 5390 Confirm 2540- Error getting log file name. Cause: The Confirm application was unable to access (or create) the system log. Action: Contact your Administrator to review user rights and local disk space. 2541- Windows and application user’s rights conflict.
Page 298 Elzone II 5390 Confirm Appendix A 2545- The repository appears to be empty. Check that the directory permissions are correct. Cause: The application was unable to determine the repository structure. Action: Contact your Administrator to review user rights and local disk space.
Page 299 Action C: Exit the application. Turn off the analyzer, then turn it back on. Restart the application. If communication problems persist after all actions have been taken, contact your Micromeritics representative. 539-42822-01 (Rev A) - Nov 2017 A-23...
Page 300 An internal error occurred while read control information was being read from a disk file. Action: The disk on which the application is installed may have failed. Contact your Micromeritics service representative and report the code number given in the message. 4201- No reports selected.
Page 301 Appendix A Elzone II 5390 Confirm 4204- Coarser specification file is not valid. ‘Out of spec.’ column was deleted. Cause: You requested a tabular report with Out of Specification selected as one of the columns. This quantity cannot be computed because the coarse specification file is invalid.
Page 302 Elzone II 5390 Confirm Appendix A 4208- An overlay file is not valid. It was not included in the report Cause: The sample file you selected for overlay does not exist or contains invalid data. Action: From the Report Options dialog, click...
Page 303 Appendix A Elzone II 5390 Confirm 4212- At least one report item must be selected. Press Cancel if you do not want a report. Cause: You failed to select reports in the “Reports to Generate” list box. No output could be produced.
Page 304 Elzone II 5390 Confirm Appendix A 4217- No table entries are within the distribution limit Cause: Truncate to distribution limits is selected on the report editor, but table entries are not within the range of the collected data. Action: Edit the table entries, or deselect Truncate to distribution on the report editor.
Page 305 Appendix A Elzone II 5390 Confirm 6000 Series 6001- DataAcq: Peak width read timed out. Height: (number) 6002- DataAcq: Peak data sequence error. Height: (number) Width: (number) Status: (number) 6003- DataAcq: Current D/A Converter Timed Out. 6004- DataAcq: Test Pulse D/A Converter Timed Out.
Page 306 The sensor for the waste container is not properly installed. Action: Insert the sensor cable and ensure that it is fully seated into the con- nector. If you continue to get this message, contact your Micromeritics Service representatives. 6055- Flow Control: Waste liquid reservoir overflowed. It must be emptied before continuing.
Page 307 Appendix A Elzone II 5390 Confirm 6056- Flow Control: Waste liquid overflow sensor not present. It must be installed before continuing. Cause: The overflow sensor is not properly installed. Action: Contact your Micromeritics Service representative. 6058- Flow Control: Differential pressure out of range. Actual: (number) mmHg...
Page 308 Elzone II 5390 Confirm Appendix A 6080- Data Collection: Measured current out of range. Actual: (number) mA Min: (number) mA Max: (number) mA 6081- Data Collection: Test pulse amplitude out of range. Measured: (number) mA Set: (number) mA 6082- Data Collection: Test pulse frequency out of range. Measured: (number) Hz Set:...
Page 309 Appendix A Elzone II 5390 Confirm Cause C: The electrolyte conductivity is too low for the size orifice in use. Action C: Use an electrolyte with higher conductivity; for example, a solution with a higher concentration of salt. 6092- Data Collection: Particle detection rate of (number) particle per second is excessive.
Page 310 Elzone II 5390 Confirm Appendix A 6093- Data Collection: Cannot measure Orifice Conductivity; Conductivity may be too high. Maximum Conductivity = (number), minimum Orifice Resistance = (number) Cause A: The orifice may be blocked. Action A: Select Unit [n] > Clear Blockages. If this fails, manually clear the blockage;...
Page 311 Appendix A Elzone II 5390 Confirm 6100 Series 6100- Unable to establish the TCP connection with the instrument. Cause: A communications problem between the computer and the analyzer has occurred. Action A: Check the cable connection between the computer and the analyzer.
Page 312 Elzone II 5390 Confirm Appendix A 6110- An automatic analysis mode is enabled. The sample defaults may not be edited while this mode is active. Cause: One of the automatic analysis modes is active. Sample defaults cannot be edited while this mode is active.
Page 313 Appendix A Elzone II 5390 Confirm 6114- You chose to use the most recent background but no background is available. Choose Yes to proceed without background data. Cause: You selected Use most recent background on the Data Setup dialog (from the Analysis Conditions dialog) but a background has not been performed on this instrument for the selected orifice tube and liquid.
Page 314 Elzone II 5390 Confirm Appendix A 6118- The entered Minimum Particle Size (number) cannot be measured using the calibration selected in Data Setup. A new calibration spanning the desired size range is recommended. Cause: You selected an orifice tube that has not been calibrated to cover the specified diameter range.
Page 315 Appendix A Elzone II 5390 Confirm 6130- The calculation could not be performed. Cause: You requested a calculated peak height on the orifice tube calibration review screen and the number of reference materials is greater than the number of peaks (see Message 6136).
Page 316 Elzone II 5390 Confirm Appendix A 6133- Calibration failed: Fit tolerances exceeded. 6134- Calibration failed: Error in fit too large. 6136- The automatic calibration could not be performed because the number of ref- erence materials is greater than the number of peaks. All reference materials have been removed from the fit.
Page 317 Appendix A Elzone II 5390 Confirm 6163- The current test is complete. Please save or clear the data before starting a new test or change Ending Conditions to collect more data. Cause: You attempted to begin another test but data for the current test has not been saved or cleared.
Page 318 Elzone II 5390 Confirm Appendix A 6180- Cannot read the background file (file name). Cause: The selected background file is not present or cannot be opened. Action A: Ensure that the path name is correct. Action B: Check directory permissions.
Page 319 Appendix A Elzone II 5390 Confirm 6185- The calibrations could not be updated. The instrument used for the analysis (s/n) is not in operation. Cause: You attempted to update calibration information but the instrument used in the calibration is not the current instrument.
Page 320 Elzone II 5390 Confirm Appendix A 6190- There is no calibration for the orifice (name) on this instrument. Cause: You attempted to update calibration information for an orifice tube that has not been calibrated on this instrument. Action: Calibrate the orifice tube, then update the calibration using the Data push button on the Collected Data dialog.
Page 321 Appendix A Elzone II 5390 Confirm 6200 Series 6200- The file (file name) does not have background data. Cause: You selected a background report for a file that contains no background data. Action: Click on the Collected Data dialog and select a back- Data Setup ground file.
Page 322 Elzone II 5390 Confirm Appendix A 6205- The file (file name) does not have pulse length vs. particle size data. Cause: You requested a pulse length vs. particle size report for a file that does not contain the required data. You may not have collected this data or you may have deleted it.
Page 323 Appendix A Elzone II 5390 Confirm 6214- The noise level or curvature in the blending range is too high. Cause: The data in the blending range are not comparable due to excessive scatter or high curvature for at least one pair of data sets.
Page 324 Elzone II 5390 Confirm Appendix A 6235- The reference material is out of range of the orifice tube and cannot be used in the calibration. Cause: You selected a reference material that is too large or too small for the selected orifice tube.
Page 325 Appendix A Elzone II 5390 Confirm 6244- A negative incremental distribution value was found in the input file (file name). Cause: You attempted to convert an ASCII file, but one of the incremental dis- tribution values in the input file is less than zero.
Page 326 Elzone II 5390 Confirm Appendix A 6260- Full-resolution data cannot be exported because the file (file name) does not have full-resolution data. Cause: You attempted to export full-resolution data using a file that does not contain full-resolution data. Action: Choose Reduced Data as the Export Type in the export dialog box.
Page 327 Elzone II 5390 Confirm Appendix B B. DATA REDUCTION Peak Statistics Four types of statistics are available for reporting: • Weighted • Geometric • Harmonic • Arithmetic The following distributions can be reported for Weighted, Geometric, and Harmonic: • Volume •...
Page 328 Appendix B Elzone II 5390 Confirm    x  –    --------------------- -  i     ----------------------------------------------- -   i     x  –    --------------------- - ...
Page 329 Elzone II 5390 Confirm Appendix B Table B-3. Statistics Statistic Formula Mean  Standard deviation Coefficient of variation x/  Standard deviation of transformed size Skewness Kurtosis (coefficient of excess) + [n]  size  –1 + n – [n]  size ...
Page 330 Appendix B Elzone II 5390 Confirm Mass Balance True and Measured Concentration The true concentration is calculated from user input. The mass concentration and dilution factor are entered on the Sample Information dialog and the sample density on the Materials Properties dialog.
Page 331 Elzone II 5390 Confirm Appendix B Fraction of Sample Measured The Fraction of Sample is selected on the Summary report. Measured Concentration ----------------------------------------------------------------- - Fraction Sample Measured True Concentration 539-42822-01 (Rev A) - Nov 2017...
Page 332 Appendix B Elzone II 5390 Confirm Specification/Reference Quantities Out of Spec SampCumFrac = cumulative fraction coarser/finer/passed/retained for class i from sample distribution CoarseSpecCumFrac = cumulative fraction coarser/finer/passed/retained for class i from Coarse Specification distribution interpolated if the bins are of different size. This is always the average of all tests in the named sample file.
Page 333 Elzone II 5390 Confirm Appendix B Difference from Reference SampCumFrac = cumulative fraction coarser/finer/passed/retained for class i from sample distribution RefSpecCumFrac = cumulative fraction coarser/finer/passed/retained for class i from Reference Specification distribution interpolated if the bins are of different size. This is always the average of all the tests in the named sample file.
Page 334 Appendix B Elzone II 5390 Confirm SPC Report Variables Regression Chart The line of best for the Regression Chart is calculated by the usual least squares method . If there is only a single point, or all N points have the same x-value, there can be no line of best fit in the standard form.
Page 335 Elzone II 5390 Confirm Appendix B Cov x y    ------------------------ - CorrelationCoef   Control Chart  -------- - Mean   Mean  – StdDev ------------------------------------- - – StdDev ------------------ - CoefVar Mean  PlusNSig Mean n STdDev ...
Page 336 Appendix B Elzone II 5390 Confirm Log Probability Data Log probability data are a transformation of cumulative mass finer data as a means of determining how well cumulative and differential mass data represent statistical log normal distributions. Since cumulative mass finer data are essentially data indicating the probabilities...
Page 337 Elzone II 5390 Confirm Appendix B Log Probability Interpolation Table X (%) X (%) X (%) 0.20 -2.88 33.00 -0.44 68.08 0.47 0.99 -2.33 34.83 -0.39 69.15 0.50 2.02 -2.05 35.94 -0.36 69.85 0.52 3.01 -1.88 37.07 -0.33 70.88 0.55 4.01...
Page 339 Appendix C Elzone II 5390 Confirm C. FORMAT OF EXPORTED DATA This appendix gives the format for sample files exported in ASCII text. All character strings are delimited with quotation marks; columns are separated with a comma and white space.
Page 340 Elzone II 5390 Confirm Appendix C Date and time quoted strings Number of length class boundaries (following reported for each) integer Particle length floating point Number of particles in class integer Full-Resolution Data Information Conveyed Form File identification quoted string...
Page 341 Appendix C Elzone II 5390 Confirm Particle Shape Data Number of tests (following reported for each test) integer Test: [n] quoted string Date and time quoted strings Number of size classes integer Number of length classes (following reported for each ...
Page 343 This appendix contains a discussion on electrolytes and how to prepare them for analysis. Overview The Elzone II 5390 analyzes samples based on the electrical sensing zone method. This method requires an electrolyte with suitable electrical conductivity and with physico- chemical neutrality toward the sample particles;...
Page 344 Elzone II 5390 Confirm Appendix D Wetting and dispersion are highly variable matters associated with the physical chemistry of particle surfaces that can range from tens of square centimeters to hundreds of square meters per gram. Nevertheless, only a few drops of a liquid dispersant or a few grains of a solid one are needed.
Page 345 Appendix D Elzone II 5390 Confirm Modified Organic The dispersant Niaproof 4 (See Table D-1), undiluted, is an acceptable electrolyte for ® especially difficult materials such as Teflon , chocolates, paints, liquid toners, and complex hydraulic and lubricating oils. However, after particles are dispersed in it, they then frequently can be mixed in other liquids, including sometimes, plain water, and analyzed.
Page 346 Elzone II 5390 Confirm Appendix D Preparation of Electrolyte Solutions Choosing the composition of and preparing an electrolyte for frequently used materials are relatively straightforward, while for unknowns it most likely will involve some trial and error. Most often satisfactory electrolytes can be prepared from distilled water or anhy- drous organic liquids using technical grade salts.
Page 347 Appendix D Elzone II 5390 Confirm 2. Clean the lower container: a. Rinse the lower container with a small amount of electrolyte, then replace the upper container. b. Pour electrolyte into the upper container until it is approximately one-half full;...
Page 349 Elzone II 5390 Confirm E. THEORY OF OPERATION The Elzone II 5390 is based on the electrical sensing zone method — also known as the Coulter principle. The sample material is prepared and placed into a beaker containing electrolytic liquid of high electrical conductance in which the particles are suspended. The...
Page 350 Elzone II 5390 Confirm Appendix E 2. At a given concentration, a longer channel length increases the probability that more than one particle (coincidence) will be in the orifice at the same time, thus producing an erroneous signal. The probability of coincidence can be reduced to its original value by diluting particle concentration, but this results in longer analysis times.
Page 351 Appendix F Elzone II 5390 Confirm F. CONCENTRATION ANALYSES Concentration analyses are performed when you need to determine the concentration of particles within your sample. You must have the volumetric pump installed to perform concentration analyses. Standard Analysis Creating the Sample File These instructions are given for the Developer’s (Advanced) format.
Page 352 Elzone II 5390 Confirm Appendix F d. Click Data Setup ; select or enter the following: Full-resolution as the Data Format Logarithmic in Diameter Class range typically for concentration analyses is the same range as specified for diameter range e. Select Volume as the ending condition and enter the volume of electrolyte for the analysis in the adjacent field;...
Page 353 Appendix F Elzone II 5390 Confirm Example: Use a 150-mL beaker filled with 120 mL electrolyte and a sample volume of 2 mL. -------------------- - -------- - Performing the Analysis Install the orifice tube onto the sample port (refer to...
Page 354 Elzone II 5390 Confirm Appendix F Select Unit [n] > Fill System to fill the orifice tube. Adjust and focus the camera if needed (if using the camera). Select Unit [n] > Sample Analysis to display the analysis screen. Click Browse choose the sample file you created.
Page 355 Appendix F Elzone II 5390 Confirm Background-Subtraction Analysis Occasionally, the ratio between contaminates in the electrolyte and particles in a sample can be low and, therefore, difficult to tell the difference between the two. When performing an analysis, the desired ratio between sample particles and contamination (sometimes called signal-to-noise ratio) in the electrolyte is approximately 99:1 in 1 mL of electrolyte.
Page 356 Elzone II 5390 Confirm Appendix F d. Click Data Setup; select or enter the following: Full-resolution as the Data Format Logarithmic in Diameter Class range typically for concentration analyses is the same range as specified for diameter range. e. Enter appropriate values for other fields (size range, stirrer speed, etc.).
Page 357 Appendix F Elzone II 5390 Confirm Performing the Background Analysis Install the orifice tube onto the sample port (refer to Choosing and installing an Orifice tube, page 3-26). Ensure that the appropriate electrolyte is connected to the Supply port. Clean the outside of orifice tube, stirrer, and electrode with filtered electrolyte.
Page 358 Elzone II 5390 Confirm Appendix F 10. Enter your password, then click and start the analysis. 11. After the analysis is finished, save the background data. Performing the Sample Analysis Now that you have established a background, you can perform your sample analysis and have the background subtracted from the analysis.
Page 359 Appendix G Elzone II 5390 G. CAMERA OPTION This appendix contains installation and operating instructions for the camera used with the Elzone II analyzer. The camera option kit includes the following: • Camera assembly • Light assembly • USB cable...
Page 360 Elzone II 5390 Appendix G Installation This section will explain how to install the: • camera assembly • light assembly • camera software Camera Assembly If your Elzone was ordered with a camera option installed, advance to Light Assembly and continue with installation of the light assembly.
Page 361 Appendix G Elzone II 5390 With a Phillips-head screwdriver, secure the assembly into position using the four captive screws on the assembly. Tighten these screws securely. Using a Phillips-head screwdriver, unscrew the retaining screws on the rear panel; then remove the panel.
Page 362 Elzone II 5390 Appendix G Locate the camera assembly cord you inserted earlier. Plug the cord into its USB connector. The guide should be facing upward and the connector slot downward. USB guide Slot for connector USB connector Replace the rear panel, then connect the USB cable to the connector labeled Camera USB on the rear panel of the analyzer.
Page 363 Appendix G Elzone II 5390 Light Assembly Remove the external electrode and the stirrer for easy access to the connector for the orifice light cable. Connect the orifice light cable to the connector inside the top panel of the sample compartment.
Page 364 Elzone II 5390 Appendix G Camera Software Be sure to close all programs before installing the camera software. Your computer will restart automatically after software installation. If the camera software was not installed with the Elzone software, insert the Elzone installation CD and browse to the Camera folder then launch the camera Setup program.
Page 365 Appendix G Elzone II 5390 Operation This section will explain how to: • start and use the software • adjust the orifice light • focus the image Before starting the camera software, perform the following steps: Reinstall the external electrode and the stirrer.
Page 366 Elzone II 5390 Appendix G Adjusting the Orifice Light Be sure the sample stand is raised (as instructed earlier at the beginning of the Operation section) and the camera software is operating. Close the right door of the sample compartment (the one containing the reflector).
Page 367 Appendix G Elzone II 5390 Focusing the Image Follow these guidelines to obtain a clear image of the orifice on the computer screen: • Make sure the orifice is aligned with the camera lens. • Be sure the orifice tube is not too close to the beaker. There should be approximately 1/2 to 1 inch (12.7 to 25.4 mm) between the orifice tube and the...
Page 368 Elzone II 5390 Appendix G Turn the focal ring fully clockwise (to the right), then slowly turn it counterclockwise (to the left) until a clear image displays on the computer screen. Adjusts the image right to left. Focal Ring Adjusts the image up and down.
Page 369 Elzone II 5390 Confirm Appendix H H. OPTIMUM PERFORMANCE FOR STRAY PARTICLE COUNT AND NOISE Some Elzone users have applications which require minimum stray or particle counts, or are prone to their appearance. These unexpected pulses, counted as particles, can result from: •...
Page 370 Appendix H Elzone II 5390 Confirm Vibration and Acoustic Noise Vibration and acoustic noise produce electrical signals much like those produced by a microphone. This usually results from the combination of a small orifice in the sample tube and a viscous electrolyte solution. As the size of the orifice decreases, the voltage drop across the orifice during operation increases.
Page 371 Elzone II 5390 Confirm Appendix H An option to optimize instrument settings to your electrolyte (current/gain settings) has been included in the software and is located on the second view of the Analysis dialog. Refer to Optimizing Instrument Settings, page 3-31for step-by-step instructions.
Page 372 Appendix H Elzone II 5390 Confirm Pump/Fan Off During Data Collection The vacuum pump used to drive the electrolyte flow and the fan used to cool the elec- tronics of the Elzone produce internal vibrations which may be detected when using low- conductivity electrolytes of high viscosity with small orifice tubes.
Page 373 Elzone II 5390 Confirm Appendix H Location The Elzone uses vibration-absorbing feet to reduce the effects of vibrations in the lab bench, but whenever working with noise-sensitive applications, extra effort should be taken to reduce the vibrations in the vicinity of the Elzone. For example, a sieve shaker may sit on the same bench with the Elzone.
Page 375 Elzone 5390 II Confirm Index INDEX Asterisk background list, 5-31 Add archive location command, orifice tube field, 4-13 Add Archive Location dialog, Autoscale, 4-32 Add Log Entry, 4-10, 4-41 graph shortcut menu, 6-27 Add Orifice Tube dialog, 4-13 in Control Chart reports, 6-16 Adding selecting options,...
Page 376 Index Elzone II 5390 Confirm peak statistics, calculations, Regression report, defining the Y-axis, 6-16 Calibrate recalculating archived results, 6-17 orifice tube, 5-23 selecting statistics, 6-18 Calibration command, 5-3, 5-49 Control chart report command, Calibration report, 4-41 Control Chart Sample Selection dialog,...
Page 377 Elzone 5390 II Confirm Index Differential flow rate, 4-16 4200 Series, A-24 Differential pressure, 4-16 6100 Series, A-35 Dilution factor, 6200 Series, A-45 Directories, Ethernet connector, adding, Exit command, 4-72 editing labels for, Exiting the analysis program, 2-7, 4-72 Directory Export orifice tube calibration, 5-30...
Page 378 Index Elzone II 5390 Confirm Format selecting information to display, 5-44 data, choosing for sample file, 4-20 Instrument schematic, 5-36 exported data, component shortcut menu, 5-37 Front panel, description, description of components on, 5-37 Full-resolution data, 4-20 displaying, 5-42 exporting, 4-64,...
Page 379 Elzone 5390 II Confirm Index opening, adding and deleting from list, 4-13 printing contents, 3-38, 4-59 calibrating, 5-23 Measure conductivity, 5-16 calibration report, 4-41 before each test, 4-15 chanigng, 5-19 Menu checking before analysis, shortcut, choosing, 3-26 structure, 2-13 cleaning, Messages clearing blockages, 5-22...
Page 380 Index Elzone II 5390 Confirm logging in, 4-71 Reference Sample dialog, 4-26 service tests, Regressioin Report Options dialog, 6-11 Peak Regression report, 6-11 valley depth, 4-28 calculations, Peaks, Summary report, 4-37 recalculaing SPC values, 6-12 Performance, optimum, selecting X- and Y-Axes variables,...
Page 381 Elzone 5390 II Confirm Index importing, 3-40 exporting, 3-41, 4-64 listing file statistics, 4-62 importing, 3-40, 4-63 listing statistics, 2-7, 3-39 listing statistics, 3-39 opening, opening, 4-49 printing contents, 3-38, 4-59 printing contents, 3-38, 4-59 Reports revert to previous version, exporting automatically after analysis, 5-7, 5-15 saving,...
Page 382 Index Elzone II 5390 Confirm Smoothing, 4-20 Software Tables, editing, 4-33 camera, installing, Tabular reports using, editing options, 4-33 version, 5-47 shortcut menu, 6-26 Sparkle display, Temperature, environment, SPC Calculations dialog, Template SPC Percentile Options dialog, 6-10 creating, SPC report...
Page 383 Elzone 5390 II Confirm Index Units Selections dialog, Units, selecting, Update file list command, User levels, User parameters, specifying, 7-4, Vacuum pump, 5-39 tubing, Valve air, 5-38 appearance when closed, 5-38 appearance when open, 5-38 fill, 5-38 sample, 5-39 servo, 5-40 Valves on instrument schematic,...

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