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Micromeritics Saturn II 5205 DigiSizer Installation Instructions And Checklist

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Saturn II 5205 DigiSizer
Installation Instructions and Checklist
520-42875-02
July 2009

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Summary of Contents for Micromeritics Saturn II 5205 DigiSizer

  • Page 1 Saturn II 5205 DigiSizer Installation Instructions and Checklist 520-42875-02 July 2009...
  • Page 2 Windows is a registered trademark of Microsoft Corporation. Copyright Micromeritics Instrument Corporation, 2009. All rights reserved.

  • Page 3: Table Of Contents

    Table of Contents Introduction ............................1 Conventions............................1 Symbols............................1 Commands............................2 Part 1: Installation Instructions ......................3 Preparing for Installation........................3 Equipment Description........................... 4 Analyzer ............................4 Liquid Sample Handler ........................5 AquaPrep............................6 MasterTech 052..........................6 Completing the Installation Checklist....................7 Documenting Installation ........................
  • Page 4 Table of Contents Sazturn DigiSizer II 5205 Selecting the Voltage ......................29 Turning on the MasterTech (If Used) ..................33 Installing the Ultrasonic Probe ....................34 Installing the Beaker Tray ..................... 35 Installing Sample Transfer Tubing ..................36 Liquid Sample Handler Installation ....................39 Standard Liquid Sample Handler ..................
  • Page 5 Saturn DigiSizer II 5205 Table of Contents Checking the Pumps and Valve ..................... 73 Ultrasonic Probe..........................74 AquaPrep............................75 Performing a Leak Test ......................75 Checking the Flow Rate ......................75 Performing a Bubble Test ...................... 76 Verifying MasterTech Operation ....................77 Preparing the Analysis Liquid......................
  • Page 6 Table of Contents Sazturn DigiSizer II 5205 Jul 09...

  • Page 7: Introduction

    An installation checklist is included following the instructions. Complete each item in the checklist and return the checklist to Micromeritics. In addition to the steps described in this checklist, the Micromeritics Installation Qualification Package for the Saturn DigiSizer 5205 and the Micromeritics Operational Qualification Package for the Saturn DigiSizer 5205 may be completed during installation.

  • Page 8: Commands

    Conventions Saturn DigiSizer II 5205 Commands Menu commands are represented as shown in the following example: Select Unit1 > Rinse > DigiSizer. Which means, select Unit1, then Rinse, then DigiSizer from the main menu. Command buttons in dialog boxes are shown in bold type. For example: Click to close the dialog box.

  • Page 9: Part 1: Installation Instructions

    Saturn DigiSizer II 5205 Preparing for Installation Part 1: Installation Instructions Preparing for Installation Before you begin installation of the Saturn DigiSizer 5205, perform these steps: • Thoroughly review the Preinstallation Checklist, which has been returned from the cus- tomer. The Preinstallation Checklist and Instructions have been written to ensure that the customer site is ready for this installation.

  • Page 10: Equipment Description

    Equipment Description Saturn DigiSizer II 5205 Equipment Description The Saturn DigiSizer 5205 System consists of up to two particle size analyzers, each with a liquid sample handler, an AquaPrep, and one multifunction personal computer. Up to two MasterTech 052 Autosamplers can be installed, allowing automatic analysis of up to 18 samples each.

  • Page 11: Liquid Sample Handler

    Saturn DigiSizer II 5205 Equipment Description Both organic and inorganic particles can be analyzed and measured over a range of 0.06 to 2100 micrometers. The Saturn DigiSizer includes a complete system for circulating the dispersing liquid/sample mixture through the cell and reservoir, as well as to an external waste container.

  • Page 12: Aquaprep

    Equipment Description Saturn DigiSizer II 5205 AquaPrep Tap water varies greatly in its dissolved air content and the presence of debris. This water must be deionized and well filtered before using with the AquaPrep. Filtering the water through (at least) a 1-micron filter will greatly extend the life of the hydrophobic capsule by means of which air is removed.

  • Page 13: Completing The Installation Checklist

    Section 2 of this document contains the Installation Checklist. For each operational verification procedure, fill in the values obtained in the test. When you complete the checklist, fill in the customer information, sign and date, and return the checklist to Micromeritics Service Center as described below.

  • Page 14: Inspecting The Equipment

    Calibration files if instrument calibration data are changed during installation.* *Generally, it is not necessary to change calibration data during installation. If however, you need to change calibration data, the calibration files must be saved and sent to Micromeritics for retention in the instrument history file.

  • Page 15: Setting Up The Digisizer System

    Saturn DigiSizer II 5205 Setting up the DigiSizer System Setting up the DigiSizer System Installing the DigiSizer Space Requirements The Saturn DigiSizer System requires the work space shown below. You must have access to the front, side, and rear panels for installation of the instrument.

  • Page 16: Selecting The Voltage Setting And Installing The Fuses

    Setting up the DigiSizer System Saturn DigiSizer II 5205 Selecting the Voltage Setting and Installing the Fuses The Saturn DigiSizer leaves the factory set for 120 VAC and with the line fuses removed. The correct setting of the universal power entrance must be checked and the appropriate fuses installed before the analyzer can be operated.
  • Page 17 Saturn DigiSizer II 5205 Setting up the DigiSizer System 4. Orient the voltage selector card so that the desired voltage is shown on the side of the card facing you. Voltage setting 5. Slide the voltage selector card into the power connector housing and press until it fits securely.

  • Page 18: Selecting The Computer Line Voltage

    Setting up the DigiSizer System Saturn DigiSizer II 5205 Selecting the Computer Line Voltage The line voltage of the computer must be set to match the input power source (from the wall outlet). The computer operates with either 100-120 VAC or 200-240 VAC at 50 or 60 Hz. Refer to the instruction manual supplied with your computer for instructions on selecting power input.
  • Page 19 Saturn DigiSizer II 5205 Setting up the DigiSizer System Power Cord Connect the power cord to the connector on the rear panel of the DigiSizer and to an appropriate power source. Computer Cables Follow the instructions provided below to connect the monitor, keyboard, printer, and mouse. Refer to the instruction manuals supplied with the computer, video monitor, and printer for voltage requirements for these units.

  • Page 20: Installing The Liquid Sample Handling Unit

    Setting up the DigiSizer System Saturn DigiSizer II 5205 Installing the Liquid Sample Handling Unit A liquid sample handler is required to transfer the sample to the analyzer for analysis. The sample is transferred through the use of tubing. This tubing is installed on the left side of the sample handler and inserted through two ports on the right side of the analyzer.
  • Page 21 Saturn DigiSizer II 5205 Setting up the DigiSizer System 4. Open the front panel of the analyzer. a. The front panel contains a retractable handle; press on the right side to protract the handle. Press here to protract the handle. b.
  • Page 22 Setting up the DigiSizer System Saturn DigiSizer II 5205 7. Unpack the sample cell holder and attach it with the two screws provided. Sample cell holder Attach with the two phillips-head screws provided If the rotation arm is blocking access to the sample cell holder location, do not attempt to move it.
  • Page 23 Saturn DigiSizer II 5205 Setting up the DigiSizer System 10. Slide the liquid sample handler toward the analyzer, guiding the tubing through the ports on the right side of the analyzer. Liquid Sample Handler Tubing Ports 11. Attach the sample transfer tubing to the sample cell holder as shown below. Avoid touching the lens when installing the tubing.

  • Page 24: Installing The Sample Cell

    Setting up the DigiSizer System Saturn DigiSizer II 5205 13. Plug the liquid sample handler’s power cord into an appropriate power source. The liquid sample handler is equipped with universal power input; therefore, voltage selection is unnecessary. Installing the Sample Cell The sample cell should always be kept clean to ensure collection of accurate data.

  • Page 25: Installing The Liquid Sample Handler Tubing

    Saturn DigiSizer II 5205 Setting up the DigiSizer System 3. The sample cell is grooved on the left side and angled slightly on the right, front side. Holding the sample cell by the edges, slide the grooved (left) side of the cell onto the left vertical bar.
  • Page 26 Setting up the DigiSizer System Saturn DigiSizer II 5205 c. Pour approximately 10 liters of water into the rinse container. It may be necessary to add a small amount of surfactant for difficult-to-rinse materials. For example, you may wish to use 0.0005% sodium metaphosphate (W/W) in deionized water. d.
  • Page 27 Saturn DigiSizer II 5205 Setting up the DigiSizer System 7. Place the cap(s) on the container and tighten; ensure that the tubing is resting on the bottom of the rinse and analysis liquid container(s). Analysis Tubing Rinse Tubing Drain Overflow Tubing Tubing Do not allow any of the tubing to form a loop so that flow is restricted;...

  • Page 28: Connecting The Ultrasonic Controller Unit

    Setting up the DigiSizer System Saturn DigiSizer II 5205 Connecting the Ultrasonic Controller Unit Connect the ultrasonic controller unit to the probe as follows: 1. Place the ultrasonic controller unit on top of the liquid sample handler. 2. Connect one end of the 9-pin RS232 M/F straight communication cable to the I/O connector on the rear of the controller unit.

  • Page 29: Installing The Aquaprep

    Saturn DigiSizer II 5205 Setting up the DigiSizer System b. Insert the other end of the ultrasonic probe cable into the connector labeled Probe. Controller Probe 8. Place the control unit power switch in the ON position. The operation of the ultrasonic probe is controlled through the analysis software. Installing the AquaPrep Ideally the AquaPrep should be placed next to the liquid sample handling module of the DigiSizer.

  • Page 30: Selecting The Input Power

    Setting up the DigiSizer System Saturn DigiSizer II 5205 Selecting the Input Power The AquaPrep leaves the factory set for 120 VAC and with the line fuse removed. The correct setting of the universal power entrance must be checked and the appropriate fuse installed before the AquaPrep can be operated.
  • Page 31 Saturn DigiSizer II 5205 Setting up the DigiSizer System 3. Pull the voltage selector card straight out of the power connector housing. 4. Orient the voltage selector card so that the desired voltage is indicated at the bottom. Orient the indicator pin so that it points upward as shown in the following illustration. Indicator Pin Voltage 5.
  • Page 32 Setting up the DigiSizer System Saturn DigiSizer II 5205 The fuses used in the equipment must be identical in type and rating to that specified. Use of other fuses could result in electrical shock and/or damage to the equipment. b. Insert appropriate fuse(s) for the input power source. Refer to the chart below for the appropriate fuse rating.

  • Page 33: Installing The Aquaprep Tubing

    Saturn DigiSizer II 5205 Setting up the DigiSizer System Installing the AquaPrep Tubing The AquaPrep has inlet and outlet connectors onto which tubing is installed for circulating the water through the AquaPrep for degassing. Tubing Connectors 1. Install the two pieces of tubing (supplied in the accessories kit) into the connectors located on the right side of the front panel.

  • Page 34: Connecting The Power Cord

    Setting up the DigiSizer System Saturn DigiSizer II 5205 Outlet Tubing Inlet Tubing Connecting the Power Cord Insert one end of the power cord into the input power connector on the rear panel of the AquaPrep and the other end into an appropriate power source. Do not turn on the power switch until you are ready to begin operation.

  • Page 35: Installing The Mastertech (Optional)

    Saturn DigiSizer II 5205 Setting up the DigiSizer System Installing the MasterTech (Optional) The MasterTech is an optional device. Skip these instructions if the customer did not purchase a Master Tech. Removing Packing Material From the Unit After removing the MasterTech from the shipping carton, remove all foam packing material from the unit before proceeding with installation.
  • Page 36 Setting up the DigiSizer System Saturn DigiSizer II 5205 b. Remove the fuse block. b. Proceed to Step 6. • If the voltage is incorrect, open the cover and remove the fuse block as described in steps a and b above, then proceed to Step 3. 3.
  • Page 37 Saturn DigiSizer II 5205 Setting up the DigiSizer System 4. Orient the voltage selector card so that the desired voltage is indicated at the bottom. Orient the indicator pin so that it points upward as shown in the following illustration. Indicator Pin Voltage 5.
  • Page 38 Setting up the DigiSizer System Saturn DigiSizer II 5205 7. Insert fuse block into the input power connector (as shown in the following illustration) and snap it into place, then close the cover. Once the fuse block and cover are in place, the position of the indicator pin shows the input power selected.

  • Page 39: Turning On The Mastertech (If Used)

    Saturn DigiSizer II 5205 Setting up the DigiSizer System Turning on the MasterTech (If Used) 1. Make sure the proper operating voltage and fuse are selected and in place. 2. Insert the power cord into the connector on the rear panel of the MasterTech and into an appropriate power source.

  • Page 40: Installing The Ultrasonic Probe

    Setting up the DigiSizer System Saturn DigiSizer II 5205 Installing the Ultrasonic Probe Make sure that no power is supplied to the unit before starting this procedure. 1. Make sure that the power ON/OFF switch on the rear panel of the MasterTech is in the OFF (O) position.

  • Page 41: Installing The Beaker Tray

    Saturn DigiSizer II 5205 Setting up the DigiSizer System Installing the Beaker Tray 1. Place the POWER switch in the ON position. 2. Make sure the arm of the MasterTech is in the LOAD (uppermost) position; the LOAD LED will be illuminated. If the LED is not illuminated, press the ARM AUTO/LOAD switch.

  • Page 42: Installing Sample Transfer Tubing

    Setting up the DigiSizer System Saturn DigiSizer II 5205 Installing Sample Transfer Tubing The MasterTech accessories kit contains two pieces of flexible tubing. One piece of tubing is for installation inside the MasterTech arm. The other piece of tubing is installed inside the liquid sample handler, allowing for connection to the MasterTech.
  • Page 43 Saturn DigiSizer II 5205 Setting up the DigiSizer System Liquid Sample Handler Installation The following steps are common to both liquid sample handlers. 1. Place the MasterTech to the right of the liquid sample handler. 2. If the liquid sample handler contains liquid: a.
  • Page 44 Setting up the DigiSizer System Saturn DigiSizer II 5205 5. Lift off the cover and set aside. Jul 09...

  • Page 45: Liquid Sample Handler Installation

    Saturn DigiSizer II 5205 Setting up the DigiSizer System Liquid Sample Handler Installation The following steps are common to both liquid sample handlers. After performing these steps, advance to the section applicable to the liquid sample handler you have connected to your analyzer.
  • Page 46 Setting up the DigiSizer System Saturn DigiSizer II 5205 4. Insert the remaining piece of flexible tubing through the hole provided on the base of the sample handler. MasterTech Flexible tubing 5. Guide the tubing through the hole in the front chassis (just below the rinse pump) and connect it to the remaining barbed fitting of the T-connector.

  • Page 47: Low-Volume Liquid Sample Handler

    Saturn DigiSizer II 5205 Setting up the DigiSizer System Low-Volume Liquid Sample Handler 1. Locate the T-fitting of the stainless steel tubing of the drain manifold. T-fitting 2. Use the 7/16- and the 1/2-in. wrenches provided in the accessories kit for this step. Hold the T-fitting secure with the 7/16-in.
  • Page 48 Setting up the DigiSizer System Saturn DigiSizer II 5205 7. Guide the tubing through the hole in the front chassis and connect it to the barbed fitting of the T-connector. Tubing connected to fitting 8. Install the other end of the flexible tubing onto the sample transfer tubing connector on the side chosen in Step 5 of “Installing Sample Transfer Tubing”...

  • Page 49: Connecting Cables

    Saturn DigiSizer II 5205 Setting up the DigiSizer System Connecting Cables 1. Make sure the power switches on the rear panels of the analyzer, liquid sample holder, and MasterTech are in the OFF positions. 2. Insert one end of the serial cable (M/F 9-pin null) into the connector labeled RS-232 Spare on the Liquid Sample Handling Unit.

  • Page 50: Installing The Analysis Program

    Windows operating systems prior to these versions did not have firewalls. To prevent an initialization failure when running the Micromeritics software, you must turn off the firewall option between the computer and the analyzer. (Refer to Technical Bulletin Gen034 for details.) You must also do this for any third-party firewalls that may have been...
  • Page 51 Saturn DigiSizer II 5205 Installing the Analysis Program • Connect the analyzer to the configured port and turn the analyzer on. Install the program as follows: 1. Turn on the analyzer and the liquid sample handler. Insert the Saturn DigiSizer CD into the CD-ROM drive. Select Start >...
  • Page 52 Select the check box just below the Destination Folder group box to add an icon to your desktop; this enables quick access to the analysis program. The DigiSizer icon is added to the Micromeritics folder by default. If you prefer a different folder, enter or select one from the drop-down list.
  • Page 53 Saturn DigiSizer II 5205 Installing the Analysis Program 10. Click Next ; the Analyzer Configuration dialog is displayed. a. In the Step 1 group box: If... Then... you are installing the select the number of analyzers you are installing. analysis program at initial installation: you plan to use the select 0...
  • Page 54 Installing the Analysis Program Saturn DigiSizer II 5205 11. Click Next ; the Ethernet Ports dialog is displayed. 12. Choose one of the following: If ..Then ..the port you configured select the port and proceed to the next step. is listed: the port you plan to use Click...
  • Page 55 Saturn DigiSizer II 5205 Installing the Analysis Program c. When the CD lights ceases to blink, click Next . After the calibration files are installed, you will be prompted to reinsert the original setup CD. 14. Click Next; the Install Complete dialog containing the Readme file is displayed. 15.

  • Page 56: Saturn Digisizer 5205 Confirm Systems

    Determining File Locations When the Micromeritics software is installed, it creates a default directory on the C drive and loads the files into this directory unless you select another location. If the customer wishes to install the files in a different directory, record the location below.

  • Page 57: Installing The Confirm Analysis Program

    Installing the Analysis Program Installing the confirm Analysis Program The installation CD shipped with the analyzer contains the Micromeritics software, which includes both the Micromeritics application and the Administrator Utility software. The person who installs the software must have Windows Administrator rights.
  • Page 58 Browse choose the directory. 10. If you want to run the Micromeritics software from the desktop, select the checkbox just below the Destination Folder group box to add an icon to the desktop. If the box labeled Install this application for All Users is checked (see Step 11 below), an icon is added to the desktop for all users 11.
  • Page 59 Browse 14. Typically, the Seat number should remain as 01. The only time the Seat number should be changed is when the Micromeritics software is installed on multiple computers that share a common repository (directory) for files, perhaps on a network drive. The software uses this number to generate separate logs for each analyzer/computer combination.
  • Page 60 Installing the Analysis Program Saturn DigiSizer II 5205 15. Click Next ; the Analyzer Configuration dialog is displayed. 16. In the Step 1 group box, click the radio button for the number of analyzers to be attached to this computer.In the Step 2 group box, enter the serial number(s) for the analyzer(s) you are attaching to this computer.
  • Page 61 Saturn DigiSizer II 5205 Installing the Analysis Program 17. Click Next ; the Ethernet Ports dialog is displayed. 18. Choose one of the following: If..Then..the port you plan to select the port and proceed to the next step. use is listed: the port you plan to Click...

  • Page 62: Entering Windows User Accounts

    Entering Windows User Accounts The Windows Administrator for the local computer must create user accounts in Microsoft Windows for all persons who will use the Micromeritics application software. If you need detailed instructions for performing this procedure, refer to Technical Bulletin Gen034.

  • Page 63: Adding Users To Windows User Groups

    The MicDevelopers user group is created to contain users who will be assigned the Devel- oper profile in the Administrator Utility. The Developer profile enables users to develop and enter analysis methods. A Developer has access to all functions of the Micromeritics application.

  • Page 64: Recording User Information

    As described previously, Micromeritics application users are to be assigned to one of the Windows user groups and to one of the two Micromeritics user profiles. The table below lists the Micromeritics application functions that can be performed by users with each profile.
  • Page 65 Saturn DigiSizer II 5205 Installing the Analysis Program Application User Developer Analyst Service** User Name* _________________________________________________ Full Name ___________________________________________________ User Name* _________________________________________________ Full Name ___________________________________________________ User Name* _________________________________________________ Full Name ___________________________________________________ User Name* _________________________________________________ Full Name ___________________________________________________ User Name* _________________________________________________ Full Name ___________________________________________________...
  • Page 66 Installing the Analysis Program Saturn DigiSizer II 5205 Application User Developer Analyst Service** User Name* _________________________________________________ Full Name ___________________________________________________ User Name* _________________________________________________ Full Name ___________________________________________________ User Name* _________________________________________________ Full Name ___________________________________________________ User Name* _________________________________________________ Full Name ___________________________________________________ User Name* _________________________________________________ Full Name ___________________________________________________...

  • Page 67: Setting Up User Profiles In The Administrator Utility

    Setting Up User Profiles in the Administrator Utility Starting the Administrator Utility 1. Select Start > Programs > Micromeritics > AdminUtil for DigiSizer 5205. 2. Enter "cfradministrator" in the User name field. 3. Enter "password" in the Password field, then click The following message displays: Your password has expired.
  • Page 68 Entering Password Configuration Parameters 1. Click the Configuration tab to display the Configuration dialog. 2. The Password parameters you enter in this dialog will apply for all Micromeritics software users. Enter the number of days in which a user’s password will expire in the Expire in field.
  • Page 69 Saturn DigiSizer II 5205 Installing the Analysis Program 7. The Application locked box is checked anytime the application is locked. Click the box to lock or unlock the application. The application locks automatically when the specified number of failed logon attempts is reached. 8.
  • Page 70 Add User dialog. Setting Up a Service User Account A user account should be set up during installation to provide Micromeritics service personnel access to system functions if a service call is required.
  • Page 71 Saturn DigiSizer II 5205 Installing the Analysis Program 2. Click to display the Add User dialog. 3. Enter a Windows User ID to be used by service personnel in the User Name field. 4. Enter in the Full Name field. Service 5.

  • Page 72: Verifying Operation

    Verifying Operation Saturn DigiSizer II 5205 Verifying Operation Installation of the Saturn DigiSizer system is now complete. It is important to perform a series of checkout procedures to verify proper operation. These procedures are designed to assist you in verifying that all installation procedures were performed properly and that the Saturn DigiSizer and its peripheral equipment are working properly.

  • Page 73: Saturn Digisizer

    Saturn DigiSizer II 5205 Verifying Operation Saturn DigiSizer Performing a Leak-Check Procedure 1. Turn on the equipment in this order: a. ultrasonic controller unit b. MasterTech (if installed) - wait until the MasterTech has finished initialization and stopped moving before proceeding to Step 2. c.
  • Page 74 Verifying Operation Saturn DigiSizer II 5205 8. Select Show instrument schematic, then Enable manual control from the Unit menu. MasterTech portion of schematic (shown only if a MasterTech is installed) Circulating Pump 9. Right-click on the circulating pump; choose Set speed. Enter 1500 if you have the standard liquid sampler installed, or 4000 if you have the Low-volume liquid sampler installed, then click 10.

  • Page 75: Moving The Rotation Arm To The Specified Angle

    Saturn DigiSizer II 5205 Verifying Operation Moving the Rotation Arm to the Specified Angle 1. If the Instrument Schematic is not shown on the computer screen, select Unit[n] > Show instrument schematic. 2. Select Unit[n] > Enable manual control. 3. Right-click on the rotation arm symbol and select Move. 4.

  • Page 76: Fire The Laser

    Verifying Operation Saturn DigiSizer II 5205 Fire the Laser This procedure can be performed with or without the analysis cell in place; no water is required. 1. If the Instrument Schematic is not shown on the computer screen, select Unit[n] > Show instrument schematic.

  • Page 77: Liquid Sample Handling Unit

    Saturn DigiSizer II 5205 Verifying Operation Liquid Sample Handling Unit Recording Application Version 1. Select Unit[n] > Unit Configuration to display the Unit Configuration dialaog. Sample Handler Application Version 2. Record the liquid sample handler application version number in the checklist. Jul 09...

  • Page 78: Checking Temperature Of Fluid

    Verifying Operation Saturn DigiSizer II 5205 Checking Temperature of Fluid 1. If the Instrument Schematic is not shown on the computer screen, select Unit[n] > Show instrument schematic. 2. Select Unit[n] > Enable manual control. Temperature 3. Circulate cold water through the system. 4.

  • Page 79: Checking The Pumps And Valve

    Saturn DigiSizer II 5205 Verifying Operation Checking the Pumps and Valve While performing the steps below, observe the symbols in the instrument schematic. A component’s symbol will change when the state of the component changes. 1. With the instrument schematic displayed, select Unit[n] > Enable manual control. Rinse Pump Analysis Pump Circulating pump...

  • Page 80: Ultrasonic Probe

    Verifying Operation Saturn DigiSizer II 5205 Ultrasonic Probe 1. With manual control enabled, right-click the Ultrasonic Probe symbol on the instrument schematic screen, then select Probe on. Ultrasonic Probe 2. Right-click the Ultrasonic Probe symbol, then select Probe off. 3. Right-click on the Ultrasonic Probe symbol, then select Set probe intensity. 4.

  • Page 81: Aquaprep

    Saturn DigiSizer II 5205 Verifying Operation AquaPrep Performing a Leak Test The AquaPrep works only with water; do not use any other liquid. Do not use water that contains a detergent or wetting solution. 1. Make sure the AquaPrep tubing is properly installed in a plastic container of deionized water.

  • Page 82: Performing A Bubble Test

    Verifying Operation Saturn DigiSizer II 5205 6. When the level reaches 1 liter, stop the timer and turn off the unit. 7. The elapsed time must be within 20 to 60 seconds. Performing a Bubble Test 1. Fill the small beaker supplied with the unit with water. 2.

  • Page 83: Verifying Mastertech Operation

    Saturn DigiSizer II 5205 Verifying Operation 5. Turn off the unit. You may hear the solenoid valve click as it opens to vent air back into the filter cartridge. 6. Turn the unit back on. You should again see a fast stream of bubbles, which tapers off after a few seconds.
  • Page 84 Verifying Operation Saturn DigiSizer II 5205 8. Select Unit [n] > Enable manual control. If the instrument schematic is not displayed, select Show instrument schematic. MasterTech Arm MasterTech Arm MasterTech Pump Pop-Up Menu 9. Ensure that the Arm AUTO/LOAD switch on the front panel of the MasterTech is in the AUTO position.
  • Page 85 Saturn DigiSizer II 5205 Verifying Operation e. Select Stirrer Speed Fast. f. Select Stirrer Off. g. Select Move Arm Up. h. Select Move To Beaker and enter the beaker position; note that the display is updated to reflect the position of the beaker tray. The picture on the screen will reflect whether or not a beaker is present.

  • Page 86: Preparing The Analysis Liquid

    Verifying Operation Saturn DigiSizer II 5205 Preparing the Analysis Liquid Water that has been freed of dissolved air (degassed water) is recommended for use as the analysis liquid. Water is easily and most efficiently degassed by using the AquaPrep degasser as described below.

  • Page 87: Rinsing The Sample Cell

    Saturn DigiSizer II 5205 Verifying Operation 4. Place the On/Off switch (on the rear panel) in the ON position (O); the power indicator should illuminate. Be sure to turn off the AquaPrep when water is not being deaerated. Failure to have water circulating may damage the unit.

  • Page 88: Creating A Sample Information File

    Verifying Operation Saturn DigiSizer II 5205 5. Select Report after measurement and choose Screen as the destination. 6. Click a progress dialog is displayed, then the background measurement is displayed. Next; If this background is unsatisfactory, you can measure another one by clicking Repeat. Refer to Appendix I of the Saturn DigiSizer 5205 Operator’s Manual for guidelines on determining an appropriate background.
  • Page 89 Saturn DigiSizer II 5205 Verifying Operation 3. When the file is copied in the Service directory, it is Read-Only. To remove the Read- Only attribute, select the file from the Microsoft Explorer, right click to display the shortcut menu, select Properties, and click the Read-Only box to remove the check mark and the attribute.
  • Page 90 Verifying Operation Saturn DigiSizer II 5205 4. Select Yes to create the file. The Sample Information File dialog is displayed, with the name of the file you created in the Sample field. 5. Select .The Open Sample Information dialog displays. Replace All 6.
  • Page 91 Saturn DigiSizer II 5205 Verifying Operation 7. Select MRMXXXX.SMP (where XXXX = the serial number of the unit) from the Files list, then click This copies the analysis conditions from the file in the C:\5205\Service directory into your sample file so you do not have to enter the analysis conditions individually. 8.

  • Page 92: Confirm Systems

    Verifying Operation Saturn DigiSizer II 5205 Confirm Systems Creating a Service Directory To create a subdirectory: 1. Select Options > Add Archive Location. 2. Select MICService in the Category field. 3. Enter Service <current date> in the Sub-category field. 4. Click Creating a Sample File for confirm systems These instructions are for confirm systems only.

  • Page 93: Performing A Reference Material Test

    7. When the analysis has finished and reports are printed, remove the reports from the printer. The Combined Report will state whether the analysis passed (results were within specifications) or failed (results were not within specification). 8. Include the printed results in the installation documentation sent to Micromeritics. Jul 09...

  • Page 94: Part 2: Installation Checklist

    Checklist Description Saturn DigiSizer II 5205 Part 2: Installation Checklist Checklist Description The tables in the checklist contain the columns described below Column Description/Action Procedure Perform the procedure described in this column. Evaluation Code Circle an evaluation code for each procedure according to the following criteria: P = Pass Indicates that this procedure has been successfully completed without...

  • Page 95: Preparing For Installation

    Saturn DigiSizer II 5205 Preparing for Installation Preparing for Installation Evaluation Initial/ Procedure Code Date Review the Preinstallation Instructions and Checklist and ensure that the F N/A laboratory is prepared for installation. Ensure that the required personnel are available. F N/A Ensure that all equipment has been unpacked and verified using the F N/A packing list.

  • Page 96: Installing The Mastertech (If Used)

    Installing the MasterTech (if used) Saturn DigiSizer II 5205 Installing the MasterTech (if used) Evaluation Code Initial Procedure (circle one) /Date Remove packing material. P N F N/A Select voltage. P N F N/A Insert fuse(s). P N F N/A Turn on the MasterTech.

  • Page 97: Installing The Analysis Program (Confirm Software Only)

    Saturn DigiSizer II 5205 Installing the Analysis Program (Confirm Software Only) Installing the Analysis Program (Confirm Software Only) Evaluation Code Initial Procedure (circle one) /Date Determine file locations. P N F N/A Install the 5205 confirm software P N F N/A Add application users to Windows user groups.

  • Page 98: Verifying Digisizer System Components

    Verifying DigiSizer System Components Saturn DigiSizer II 5205 Verifying DigiSizer System Components Evaluation Code Initial Procedure (circle one) /Date Enter service test mode. P N F N/A Leak check the DigiSizer. P N F N/A Move rotation arm to the specified angle. P N F N/A Fire laser.

  • Page 99: Verifying The Mastertech (If Used)

    Saturn DigiSizer II 5205 Verifying the MasterTech (if used) Verifying the MasterTech (if used) Evaluation Code Initial Procedure (circle one) /Date Test ultrasonic probe AUTO/ON switch. P N F N/A Initialize MasterTech. Ensure that the tray rotates until beaker position P N F N/A one is reached.

  • Page 100: Performing Reference Material Test

    Performing Reference Material Test Saturn DigiSizer II 5205 Performing Reference Material Test Evaluation Code Initial Procedure (circle one) /Date Record reference material lot number:______________________ P N F N/A Perform a reference material analysis. P N F N/A Record expected results of the reference material analysis (listed in P N F N/A the reference material instructions booklet): Volumetric arithmetic mean equivalent spherical diameter = _________...
  • Page 101 Saturn DigiSizer II 5205 Performing Reference Material Test Evaluation Code Initial Procedure (circle one) /Date Record the actual results of the analysis: Volumetric arithmetic mean equivalent spherical diameter = _________ P N F N/A Volume median equivalent spherical diameter = __________ P N F N/A 90 Cumulative volume % finer than __________ P N F N/A...

  • Page 102: Exceptions

    Exceptions Saturn DigiSizer II 5205 Exceptions Procedures categorized as Fail should be explained below. Initial/ Procedure Comments Date Jul 09...

  • Page 103: Signatures

    Saturn DigiSizer II 5205 Signatures Signatures Installer Name: Signed: (please print) Position: Date: Company: Field Service Report (FSR Number): Customer Representative Name: Signed: (please print) Position: Date: Company: Field Service Report (FSR Number): Jul 09...

  • Page 104: Final Documentation

    Service Support Center in Norcross, Georgia, USA. After completing the installation process, representatives of Micromeritics who install instruments are required to send the documents listed below to Micromeritics for inclusion in the customer's instrument history.

  • Page 105: Appendix A: Attaching Multiple Analyzers To One Computer

    Saturn DigiSizer II 5205 Appendix A Appendix A: Attaching Multiple Analyzers to One Computer You can install up to two Saturn DigiSizer analyzers to one computer, allowing for high sample throughput. Each analyzer can also have a MasterTech autosampler attached. The MasterTech allows you to queue up to 18 samples for analysis.
  • Page 106 Appendix A Saturn DigiSizer II 5205 Installing Analyzers with Default Configurations These instructions are for installing a second analyzer with a default configuration to a computer that already has an analyzer (Unit #1) installed. Connect the ethernet switch (refer to the manufacturer’s manual for instructions). Exit the analysis program (if operating) and turn the installed analyzer (Unit #1) off.
  • Page 107 Saturn DigiSizer II 5205 Appendix A 16. Enter 2 for the final configuration of this unit (first line) 17. Enter 102 as the new IP address for Unit #2 (fourth field of second line). 18. Record the IP address and subnet mask on the Saturn DigiSizer Configuration form (the last page of this appendix).
  • Page 108 Appendix A Saturn DigiSizer II 5205 28. Select Add an analyzer and click Next ; the Ethernet Introduction dialog is displayed. This screen outlines the steps that should be completed before installing the software. 29. Make sure the steps are completed, then click .
  • Page 109 Saturn DigiSizer II 5205 Appendix A 31. Click Next ; the Calibration File installation dialog is displayed. 32. Ensure that the CD-ROM drive is shown as the source location; if not, click Browse select the correct drive. 33. Click Finish to install the calibration files;...
  • Page 110 Appendix A Saturn DigiSizer II 5205 Moving an Existing Configured Analyzer to Another Computer Use the instructions in this section if you have a configured analyzer that you wish to move to a different computer that already has an analyzer and the analysis program installed. Review the Saturn DigiSizer Configuration forms for both the current and destination computers.
  • Page 111 Saturn DigiSizer II 5205 Appendix A Select Move an analyzer from one PC to another PC and click Next ; the Ethernet Introduction dialog is displayed. This screen outlines the steps that should be completed before installing the software Make sure the steps are completed, then click Select Source PC, then click ;...
  • Page 112 Appendix A Saturn DigiSizer II 5205 10. From the drop-down list in the Step 1 group box, select the analyzer that is to be moved from this computer. 11. Click Browse in the Step 2 group box to select a location for storing the calibration and status files associated with the source computer.
  • Page 113 Saturn DigiSizer II 5205 Appendix A 19. Click Exit to close the dialog. 20. Remove the CD-ROM from the computer and store in a safe place. 21. Use Windows Explorer to edit the application file (either WIN5205.ini for standard software or cfr5205.ini for confirm software): a.
  • Page 114 Appendix A Saturn DigiSizer II 5205 A-10 Jul 09...

  • Page 115: Appendix B: Saturn Digisizer Configuration Management

    Saturn DigiSizer 5205 Appendix B Appendix B: Saturn DigiSizer Configuration Management Serial Unit Number Number IP Address Subnet Mask Date Jul 09...
  • Page 116 Appendix B Saturn DigiSizer 5205 Jul 09...
  • Page 117 Saturn DigiSizer II 5205 Appendix C Appendix C: Selecting the Voltage and Installing Fuses with Other Input Power Configuration On some instruments, the input power connector has a removable cover instead of the hinged cover desribed in this document. If this type of configuration is used on the instrument being installed, follow the instructions below.
  • Page 118 Appendix C Saturn DigiSizer II 5205 Pull the voltage selector card straight out of the power connector housing. Orient the voltage selector card so that the desired voltage is indicated at the bottom. Orient the indicator pin so that it points upward as shown in the following illustration. Indicator Pin Voltage Insert the voltage selector card into the power connector housing with the edge containing...
  • Page 119 Saturn DigiSizer II 5205 Appendix C Fuse the input power line according to local safety practices. The input power connector can be used with either a single-fuse arrangement or a double-fuse arrangement, as shown in the following illustration. Fuse Fuse Block Retaining Screw Jumper Bar Fuses...
  • Page 120 Appendix C Saturn DigiSizer II 5205 c. Insert the appropriate fuse(s) for the input power source. Refer to the chart below for the appropriate fuse ratings for the DigiSizer, AquaPrep and MasterTech. Instrument Power Source Fuse Saturn DigiSizer 5205 100-115 VAC 3 AG, 1.5 Amp Slow-Blow 200-240 VAC 5 x 20 mm, 1.25 Amp Slow-Blow...

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