Micromeritics Cirrus AutoChem 2920 Installation Instructions Manual
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Micromeritics Cirrus AutoChem 2920 Installation Instructions Manual

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M
-C
ICROMERITICS
IRRUS
I
NTERFACE
I
I
NSTALLATION
NSTRUCTIONS
292-42805-00
Nov 2016
(Rev C)

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Summary of Contents for Micromeritics Cirrus AutoChem 2920

  • Page 1 ICROMERITICS IRRUS NTERFACE NSTALLATION NSTRUCTIONS 292-42805-00 Nov 2016 (Rev C)
  • Page 2 Copyright The software described in this manual is furnished under a license agreement and may be used or copied only in accordance with the terms of the agreement. ______________________________________________________________________________ Copyright © 2011 - 2016. Micromeritics Instrument Corporation. All rights reserved.

  • Page 3: Contact Us

    --------------- Quotes, Orders, and Customer Satisfaction Customer Service Phone: 1-770-662-3636 Orders@Micromeritics.com --------------- U.S. Instrument Service Department U.S. Service Department Phone: 1-770-662-3666 Service.Helpdesk@Micromeritics.com --------------- Micromeritics Scientific Services Customer Support Portal http://techsupport.micromeritics.com/portal Micromeritics-Cirrus Interface Installation Instructions 292-42805-00 (Rev C) — Nov 2016...

  • Page 4: About This Manual

    The following formats are used throughout this manual: NOTE - Notes contain important information pertinent to the subject matter. CAUTION - Cautions contain information to help prevent actions that may damage the analyzer or components. Micromeritics-Cirrus Interface Installation Instructions 292-42805-00 (Rev C) — Nov 2016...

  • Page 5: Table Of Contents

    Mass Spectrometer to 3Flex 3500 Chemisorption Analyzer Mass Spectrometer to ASAP 2020 Chemisorption Analyzer Pin-Outs for Mass Spec Connectors Software Installation and Operation Preparation Micromeritics Custom Recipe Installation Set Up and Prepare for Operation Power Off the Mass Spectrometer Parts and Accessories Micromeritics-Cirrus Interface Installation Instructions 292-42805-00 (Rev C) —...

  • Page 7: Introduction

    Introduction NTRODUCTION OFTWARE The Micromeritics-Cirrus Interface Software is used with select Micromeritics analyzers integrated with an MKS Cirrus Mass Spectrometer. This software runs within the MKS Process Eye Professional application. The Micromeritics-Cirrus Interface Software will perform the following tasks: Automatically collect data with the Cirrus Mass Spectrometer via trigger signal from the Micro-...

  • Page 8: Hardware Installation

    20 °C. Removing the cover and insulation at the zones will speed the cooling process. The following illustration shows the original plumbing of the TCD/Cold Trap zone. Micromeritics-Cirrus Interface Installation Instructions 292-42805-00 (Rev C) — Nov 2016...
  • Page 9 4. Remove the 1/8 in. tube from the sample exhaust side of the TCD. Disconnect the other end at the hexagonal fitting, which is above the side panel exhaust ports. Micromeritics-Cirrus Interface Installation Instructions 292-42805-00 (Rev C) — Nov 2016...
  • Page 10 Remove the two screws which hold the cover plate to a grooved channel. Remove the cover plate. 7. Remove the screw from the grooved channel. Micromeritics-Cirrus Interface Installation Instructions 292-42805-00 (Rev C) — Nov 2016...
  • Page 11 TEE to the exhaust port of the sample side of the TCD. Note the orientation of the TEE. It will be installed “upside down” so that the counterbore for the original screw head is facing down. Micromeritics-Cirrus Interface Installation Instructions 292-42805-00 (Rev C) — Nov 2016...
  • Page 12 Spectrometer hose from being pulled out of the heated zone. The insulation rings may be used to prevent damage to the Mass Spectrometer hose insulation. 15. Re-attach the side panel cover plate, with the Mass Spectrometer hose passing through into the heated zone. Micromeritics-Cirrus Interface Installation Instructions 292-42805-00 (Rev C) — Nov 2016...
  • Page 13 The tube must be bent so that the metal connectors of the Mass Spec- trometer hose are inside the heated zone. The plumbing should now resemble these photos: Micromeritics-Cirrus Interface Installation Instructions 292-42805-00 (Rev C) — Nov 2016...
  • Page 14 Connect Cables on page 20 for instructions on connecting the cables from the Mass Spectrometer to the analyzer. Micromeritics-Cirrus Interface Installation Instructions 292-42805-00 (Rev C) — Nov 2016...

  • Page 15: Autochem 2920 (Serial Numbers 701 And Above)

    2. Loosen the screws that retain the plastic hose clamps, remove the side panel cover plate, and remove the hard plastic center cap shown in the following illustration. Save the screws for later. Micromeritics-Cirrus Interface Installation Instructions 292-42805-00 (Rev C) — Nov 2016...
  • Page 16 If the tube is too long, either coil or zig-zag the tube to use the excess length. With the covers and insulation removed, the Mass Spectrometer TEE connection block may be accessed. 3. Remove the plug from the left side of the TEE. Micromeritics-Cirrus Interface Installation Instructions 292-42805-00 (Rev C) — Nov 2016...
  • Page 17 TEE. Nuts and ferrules are included in the kit. The tube must be bent so that the metal connectors of the Mass Spectrometer hose are inside the heated zone. Micromeritics-Cirrus Interface Installation Instructions 292-42805-00 (Rev C) — Nov 2016...
  • Page 18 Hardware Installation The plumbing should now resemble these photos: Micromeritics-Cirrus Interface Installation Instructions 292-42805-00 (Rev C) — Nov 2016...
  • Page 19 Connect Cables on page 20 for instructions on connecting the cables from the Mass Spectrometer to the analyzer. Micromeritics-Cirrus Interface Installation Instructions 292-42805-00 (Rev C) — Nov 2016...

  • Page 20: Autochem Hp 2950

    Save the nuts for later. 4. Remove the side panel cover plate. Discard the insulation rings and the cover plate. Save the screws for later. Micromeritics-Cirrus Interface Installation Instructions 292-42805-00 (Rev C) — Nov 2016...
  • Page 21 7. Mount the retaining ring onto the threaded stud located on the rear of the Mass Spectrometer port plate. Secure with the locking nut (part number 004-28205-00, nylon locking nut, 6-32). Do not tighten the nut completely. Micromeritics-Cirrus Interface Installation Instructions 292-42805-00 (Rev C) — Nov 2016...
  • Page 22 12. Insert the 1/4 in. tube at the end of the Mass Spectrometer hose into the reducing union. 13. Use a 9/16 in. wrench to tighten the nut on the reducing union. 14. Re-install the rear panel and the analyzer top panel. Micromeritics-Cirrus Interface Installation Instructions 292-42805-00 (Rev C) — Nov 2016...

  • Page 23: 3Flex 3500 Chemisorption

    MKS Cirrus to 3Flex Accessories Kit (part number 350-33031-00) and the 9/16 in. nut to secure the connection. Connect Cables on page 20 for instructions on connecting the cables from the Mass Spectrometer to the analyzer. Micromeritics-Cirrus Interface Installation Instructions 292-42805-00 (Rev C) — Nov 2016...

  • Page 24: Asap 2020 Chemisorption

    4. Bend the stainless steel tubing so that it does not interfere with the operation of the analyzer. 5. Insert the Mass Spectrometer capillary hose fitting into the reducing union on the stainless steel tube. Micromeritics-Cirrus Interface Installation Instructions 292-42805-00 (Rev C) — Nov 2016...
  • Page 25 6. Use a 9/16 in. wrench to tighten the nut on the reducing union. Connect Cables on the next page for instructions on connecting the cables from the Mass Spectrometer to the analyzer. Micromeritics-Cirrus Interface Installation Instructions 292-42805-00 (Rev C) — Nov 2016...

  • Page 26: Connect Cables

    Cirrus to their appropriate connections. Tighten the retaining screws. 4. On the side panel of the AutoChem, attach the 15-pin and 25-pin connectors labeled AutoChem to their appropriate connections. Tighten the retaining screws. Micromeritics-Cirrus Interface Installation Instructions 292-42805-00 (Rev C) — Nov 2016...

  • Page 27: Mass Spectrometer To 3Flex 3500 Chemisorption Analyzer

    Tighten the retaining screws. 3. On the back panel of the analyzer, attach the 25-pin connector of the straight-thru cable to its appropriate connection. Tighten the retaining screws. Micromeritics-Cirrus Interface Installation Instructions 292-42805-00 (Rev C) — Nov 2016...

  • Page 28: Mass Spectrometer To Asap 2020 Chemisorption Analyzer

    3. Connect and tighten the 9-pin male connector to the Valve/Fan port on the analyzer front. 4. Connect and tighten the extension cable (P/N 003-20656-03) to the 25-pin connector on the interface cable (P/N 202-60815-00). Micromeritics-Cirrus Interface Installation Instructions 292-42805-00 (Rev C) — Nov 2016...
  • Page 29 6. Plug one end of the power cord into the connector on the rear panel of the Mass Spectrometer and the other end into an appropriate power source. Refer to the Cirrus 2 Hardware Manual for electrical specifications. Micromeritics-Cirrus Interface Installation Instructions 292-42805-00 (Rev C) — Nov 2016...

  • Page 30: Pin-Outs For Mass Spec Connectors

    All other pins in the 15-pin connector are floating (not connected). Connect the metal shell of the connector to the chassis ground and cable shield to maintain shielding of the signals. Micromeritics-Cirrus Interface Installation Instructions 292-42805-00 (Rev C) — Nov 2016...
  • Page 31 Opto-coupled inputs Maximum reverse voltage = 3 v Nominal forward voltage = 1.3 v at 10 mA Minimum current required to be recognized by the 2950 analyzer = 1 mA Micromeritics-Cirrus Interface Installation Instructions 292-42805-00 (Rev C) — Nov 2016...
  • Page 32 Opto output 3 emitter Opto output 4 collector Opto output 4 emitter Opto input 1 anode (+) Opto input 1 cathode (-) Opto input 2 anode (+) Opto input 2 cathode (-) Micromeritics-Cirrus Interface Installation Instructions 292-42805-00 (Rev C) — Nov 2016...
  • Page 33 D cable with male connector pins on both ends to directly connect to a MKS Cirrus Mass Spectrometer. Pin 6. Normally open contact of the 3Flex relay Pin 10. The common pole of the 3Flex relay. Other pins are not used. Micromeritics-Cirrus Interface Installation Instructions 292-42805-00 (Rev C) — Nov 2016...

  • Page 34: Software Installation And Operation Preparation

    USTOM ECIPE NSTALLATION 1. Insert the Micromeritics Custom Recipe installation media into the media drive. 2. Go to Start > All Programs > MKS RGA Applications > Tools > User Setup. 3. The Setup Wizard displays. Click Next. 4. On the Install Recipes window, click Have Disk.
  • Page 35 5. On the Select a Drive Location window, click the down arrow to the right of the text field, select Browse, then click OK. 6. Navigate to the Micromeritics/MKS/Software directory on the installation disk. Select the Micromeritics Install V[n].lst file, then click Open.
  • Page 36 Micromeritics Custom Recipe Installation 8. On the Hardware Setup window, ensure the Skip Hardware Auto-Detection option is selec- ted, then click Next. 9. Verify the Setup Wizard has enough information to complete the installation, then click Finish. 10. On the Recipe Installation History window, click Close.
  • Page 37 Software Installation and Operation Preparation 13. On the Instrument Access window, click to complete installation. 14. Go to Start > All Programs > MKS RGA Applications > Process Eye Professional. Micromeritics-Cirrus Interface Installation Instructions 292-42805-00 (Rev C) — Nov 2016...

  • Page 38: Set Up And Prepare For Operation

    F5 to display the Recipe Control menu. To install from the Windows Explorer display, minimize the Process Eye Professional window, then navigate to C:\Micromeritics\MKS\Microsoft Silverlight. After installation is complete, maximize the Process Eye Professional window and press F5 to display the Recipe Control menu.
  • Page 39 Whether or not the capillary needs to be heated depends on the application and the nature of the gases being sampled. The Cirrus is designed to allow the capillary heater to be run continuously. Micromeritics-Cirrus Interface Installation Instructions 292-42805-00 (Rev C) — Nov 2016...

  • Page 40: Power Off The Mass Spectrometer

    The pumps will stop and the vent valve will open after a few minutes. 5. Wait 5 minutes for the system to cool further and come to a full stop. Micromeritics-Cirrus Interface Installation Instructions 292-42805-00 (Rev C) — Nov 2016...

  • Page 41: Parts And Accessories

    004-28310-01 Wrench, 7/64 Allen, for 6-32 socket head screws 004-54113-00 Software, MKS Cirrus Mass Spectrometer 292-20805-00 Micro-Cirrus Interface User Guide 292-42804-00 Micro-Cirrus Interface Installation Instructions 292-42805-00 Cable, Mass Spectrometer 292-60805-00 Micromeritics-Cirrus Interface Installation Instructions 292-42805-00 (Rev C) — Nov 2016...
  • Page 42 Ferrule, Rear, 1/4 in. Nylon (qty. 2) 004-25104-00 Ferrule, Front, 1/4 in. Peek (qty. 2) 004-25139-00 Software, MKS Cirrus Mass Spectrometer 292-20805-00 Micro-Cirrus Interface User Guide 292-42804-00 Micro-Cirrus Interface Installation Instructions 292-42805-00 Micromeritics-Cirrus Interface Installation Instructions 292-42805-00 (Rev C) — Nov 2016...
  • Page 43 Swaging nut, 1/16 in. 004-25541-00 Ferrule, 1/16-in. 004-25541-01 Cable, chemisorption port to mass spectrometer interface 202-60815-00 Software, MKS Cirrus Mass Spectrometer 292-20805-00 Micro-Cirrus Interface User Guide 292-42804-00 Micro-Cirrus Interface Installation Instructions 292-42805-00 Micromeritics-Cirrus Interface Installation Instructions 292-42805-00 (Rev C) — Nov 2016...

This manual is also suitable for:

Cirrus autochem hp 2950

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