Table of Contents
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About This Manual.................................................................................................................................xi
Overview ...................................................................................................................................xi
Conventions Used in This Manual..........................................................................................xiii
Instrument Markings and Symbols .........................................................................................xvi
Using Hydrogen .....................................................................................................................xvii
Using the Hydrogen Sensor .....................................................................................xviii
Chapter 1
Preventive Maintenance.................................................................................................................... 21
Suggested Maintenance Schedule ............................................................................................ 22
Chapter 2
Maintaining a Split/Splitless Injector ............................................................................................... 25
Split/Splitless Injector .............................................................................................................. 26
Split/Splitless Injector Maintenance ........................................................................................ 28
When replacing the septum......................................................................................... 28
When cleaning or replacing the liner .......................................................................... 28
If the glass liner breaks inside the injector.................................................................. 29
When replacing the split line tubing ........................................................................... 29
Chapter 3
Maintaining a Large Volume Splitless Injector ............................................................................... 53
Large Volume Splitless Injector............................................................................................... 54
Large Volume Splitless Injector Maintenance......................................................................... 56
When replacing the septum......................................................................................... 56
When cleaning or replacing the liner .......................................................................... 56
If the glass liner breaks inside the injector.................................................................. 57
When replacing the split line tubing ........................................................................... 57
Chapter 4
Maintaining a Cold On-Column Injector for Standard Automatic Injections ............................... 79
Automated Operation Cold On-Column Injector..................................................................... 80
Cold On-Column Injector Maintenance................................................................................... 82
Replace the O-ring ...................................................................................................... 82
Possible leaks in the rotary valve................................................................................ 82
Chapter 5
Maintaining a Cold On-Column Injector Direct Narrow-Bore ........................................................ 97
Automated Operation Cold On-Column Injector..................................................................... 98
Maintenance and Troubleshooting Manual
Contents
v
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Chapters
Table of Contents
Troubleshooting
