Thermo Scientific Accela Open Autosampler Hardware Manual page 117

Thermo Scientific
Table 33. Repeatability tests with UV-detection (Sheet 2 of 2)
Component
Loop Size
Injection Valve
Cycle Composer Macro
or Cycle (ICC-CE)
Cycle Composer Method Parameter Settings
Table 34 lists the Cycle Composer Method parameter settings for repeatability tests with
UV-detection.
Table 34. Repeatability tests with UV-detection
Parameter
Syringe
Sample Volume
Airgap Volume
Front Volume
Rear Volume
Needle Gap Valve Clean
Fill Speed
Fill Strokes
Stator Wash
Pullup Del
Inject to
Inject Speed
Pre Inj Del
Pst Inj Del
Valve Clean Time Solvent 2
Post Clean Time Solvent 2
Valve Clean Time Solvent 1
Post Clean Time Solvent 1
Specification
• 2 μL (Loop overfill, 7 μL)
• Loop ID: 0.13 mm
• 20 μL (partial loop, 10 μL)
• Loop ID 0.25 mm
VICI/Valco C72VX-1696D-CTC,
bore size 0.25 mm
DLW Standard
Value
100 μL DLW
7/10 μL
3 μL
5 μL
5 μL
3 mm
5 μL
0
0
500 ms
Specified Inj. Valve
5 μL/S
500 ms
500 ms
2 s
2 s
3 s
2 s
6
Standard Chromatographic Tests
Accela Open Autosampler Hardware Manual
Troubleshooting
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