Agilent Technologies 1290 Infinity II 2D-LC Solution Manuals

Manuals and User Guides for Agilent Technologies 1290 Infinity II 2D-LC Solution. We have 2 Agilent Technologies 1290 Infinity II 2D-LC Solution manuals available for free PDF download: User Manual

Agilent Technologies 1290 Infinity II 2D-LC Solution User Manual (395 pages)

Solution for MassHunter TOF and Q-TOF

Brand: Agilent Technologies | Category: Measuring Instruments | Size: 13.82 MB

Table of Contents

5
- Introduction
  10
  - Product Description
    11
  - Features
    12
  - Terms Related to 2D-LC
    14
2 Concepts of 2D-Lc

15
3 Compatibility Matrix

45
- Supported Chromatographic Data Systems
  46
- Supported Drivers
  47
- Supported Operating Systems
  48
- Supported Firmware
  49
- Available Languages
  50
- PC Requirements
  51
- Licensing
  52
4 Installation

53
5 2D-Lc Data Acquisition in Masshunter Workstation 11

103
- LC Data Acquisition in Masshunter Workstation
  104
  - Start the Data Acquisition Software
    104
  - Overview 2D-LC in Masshunter Acquisition 11
    106
  - Instrument Status
    107
  - 2D-LC User Interface
    108
  - Additional Information in the 2D-LC User Interface
    108
  - LC Valves Online Monitor in the 2D-LC User Interface
    114
  - Method Editor Window
    116
  - Sample Run Window
    117
  - Worklist Window
    118
  - Tune Window
    119
  - Instrument Details
    120
  - Use Module List to Obtain Instrument Details
    120
  - Use Instrument Configuration Report to Obtain Instrument Details
    121
  - Log Book in Masshunter Acquisition 11
    123
6 Method Parameters

125
- Method Editor 2D-LC
  
  126
  - 2D LC Operation Mode
    127
- Set the 2D-LC Method Parameters
  
  127
  - Define the 1D Pump Flow
    129
  - Define the 2D Pump Flow
    129
  - Define the 2D Solvent
    130
  - Define the Stoptime
    130
  - Define the Posttime
    132
  - Edit the Sampling Table
    133
  - Define the 2D Gradient
    139
  - Use the Flush Gradient
    147
  - Use Peak Trigger
    148
  - Use the Advanced 2D Pump Settings
    152
- Preview (2D-LC)
  
  154
  - Further Graphical Explanation
    162
- Set up a Peak-Based Experiment Graphically
  
  168
- Setup 2D Gradient Graphically
  
  173
- Setup Second Dimension Gradient with the Graphical User Interface
  
  175
- Additional Information
  
  177
  - Multi-Inject
    177
  - Dynamic Peak Parking
    179
7 Method Development of Active Solvent Modulation (Asm)

185
8 Run the System

192
10 Troubleshooting and Diagnostics

275
- Overview of the Module's Indicators and Test Functions
  
  276
- User Interfaces
  
  277
- Agilent Lab Advisor Software
  
  278
  - Integrated 2D-LC Functions in the Lab Advisor Software
    279
- Lab Advisor Instrument Control
  
  280
- Lab Advisor Service & Diagnostic
  
  286
  - Decluster the 2D-LC Cluster
    286
  - Pump Head Leak Test for the 2D Pump
    287
  - Pump Leak Rate Test for the 2D Pump
    288
  - System Pressure Test for the 2D Pump
    289
  - 2D-LC Capillary Leak Test
    291
  - Replace the Module Firmware
    292
- The Basic Principle of Troubleshooting
  
  294
Table of Contents

296
- Pressure too High
  297
- Pressure too Low
  298
- Peak Area and Peak Height Related
  299
- Retention Time Related
  300
- Missing Signal Linearity
  301
- Drifting Signal
  302
- Signal Noisy
  303
- Recommended Tests to Conclude Troubleshooting
  304
11 Error Information

305
- What Are Error Messages
  
  306
- General Error Messages
  
  307
  - Timeout
    307
  - Shutdown
    308
  - Lost CAN Partner
    309
  - Remote Timeout
    309
  - Leak Sensor Open
    310
  - Leak Sensor Short
    310
  - Compensation Sensor Open
    311
  - Compensation Sensor Short
    311
  - Fan Failed
    312
  - Leak
    312
- Module-Specific Error Messages
  
  313
  - Initialization of Valve Failed
    313
  - Valve Switching Failed
    314
  - Valve Tag Violation
    314
  - Position Cluster Partner Missing
    315
  - Pressure Cluster Partner Missing
    315
  - External Valve Falls into Resident Mode
    316
12 Maintenance

317
- Introduction to Maintenance
  318
- Warnings and Cautions
  319
- Overview of Maintenance
  321
- Cleaning the Module
  322
- Correcting Leaks
  323
- Correcting Leaks (G1170A)
  323
  - Replace Valve Heads
    324
- Correcting Leaks (G7116B)
  323
- Replace Valve Heads (G7116B)
  324
- Replace Valve Heads (G1170A)
  327
  - Replacing Parts of the Valve Head
    330
  - Replacing the Fuses of the Infinity Valve Drive
    332
13 Parts for Maintenance

334
- 2D-LC Loops
  335
- 2D-LC Capillaries
  336
- ASM Capillaries
  337
- Pressure Release Kit
  338
- 2D-LC Easy Starter Kit
  339
- Valve Drive Parts
  340
- Valve Driver Parts Infinity II
  341
- Valve Head Parts
  342
- Technical Specifications
  343
- Tools
  343
  - Vale Options Overview (for 2D-LC)
    344
- Obsolete Valve Heads
  347
  - MS Diverter Valve
    348
- Additional Parts for the MS Diverter Valve Setup
  349
  - Valve Options Overview (for G7116B)
    350
  - Additional Heater Devices
    352
- Additional Heater Devices (for G7116B)
  353
  - Accessories and Consumables (for G7116B)
    354
  - Infinitylab Quick Connect and Quick Turn Fittings
    356
- Infinitylab Quick Connect Fittings
  357
- Infinitylab Quick Connect Fitting Replacement Capillaries
  358
- Infinitylab Quick Turn Fitting
  359
  - Capillary Kits
    360
  - Important Customer Web Links
    361
- Theoretical Background
  362
  - Theoretical Basis of 2D-LC
    363
  - Orthogonality
    364
  - Resolution
    365
  - Peak Capacity
    368
    
    As Detector
    371
    
    Successful Mode Combinations
    373
    
    Solvent Elution Modes
    374
    
    Practical Issues
    380
15 Appendix

382
- General
  383
- General Safety Information
  383
- Safety Standards
  383
- Before Applying Power
  384
- Ground the Instrument
  384
- Do Not Modify the Instrument
  385
- Do Not Operate in an Explosive Atmosphere
  385
- Do Not Remove the Instrument Cover
  385
- In Case of Damage
  385
- Solvents
  386
- Safety Symbols
  387
  - Waste Electrical and Electronic Equipment (WEEE) Directive
    389
  - Radio Interference
    390
  - Sound Emission
    391
  - Solvent Information
    392
  - Further Information
    393
  - Agilent Technologies on Internet
    394

Agilent Technologies 1290 Infinity II 2D-LC Solution User Manual (356 pages)

Brand: Agilent Technologies | Category: Laboratory Equipment | Size: 23.38 MB

Table of Contents

6
- Introduction
  10
  - Product Description
    11
  - Features
    13
2 Concepts of 2D-Lc

14
3 Compatibility Matrix

45
- Supported Chromatographic Data Systems
  46
- Supported Drivers
  47
- Supported Operating Systems
  48
- Supported Firmware
  49
- Available Languages
  50
- PC Requirements
  51
4 Installation

52
5 Method Parameters

87
- Method Parameters Standard Heart-Cutting 2D-LC
  
  88
  - Software Method Setup
    88
  - Set 2D-LC Mode
    89
  - Set Solvents
    96
  - Set Flow
    97
  - Set Solvent Composition Gradient
    98
  - Sampling Table
    100
  - Define Peak Detector Parameter
    102
    
    Method Parameters Multiple Heart-Cutting and High Resolution Sampling 2D-LC
    104
- Method Parameters Multiple Heart-Cutting and High Resolution Sampling
  
  104
  - Software Method Setup
    104
  - Set 2D-LC Mode Multiple Heart-Cutting
    105
  - Set 2D-LC Mode Hires Sampling
    108
  - Set Solvents
    109
  - Set Flow
    110
  - Set Solvent Composition Gradient
    111
  - Set 2D Time Segments (Multiple Heart-Cutting Only)
    113
  - Set Cuts in the Software (Hires Sampling Only)
    115
  - Define Peak Detector Parameter
    118
  - Gradient Preview Functionality
    120
  - Smart Peak Parking
    125
- 2 D-Lc
  
  104
- Method Parameters Comprehensive 2D-LC
  
  127
  - Software Method Setup
    127
  - Set 2D-LC Mode
    128
  - Set Solvents
    129
  - Set Flow
    130
  - Set Solvent Composition Gradient
    131
  - Set 2D Time Segments
    134
  - Define Peak Detector Parameter
    136
  - Gradient Preview Functionality
    137
- Method Development of Active Solvent Modulation (ASM)
  
  141
6 Run the System

146
8 Data Analysis

200
- Data Analysis
  201
- Data Analysis for Heartcutting 2D-LC (LC-LC)
  201
- 2D-LC Viewer
  202
- High-Resolution Sampling - Results
  207
- Quantitation
  211
  - Data Analysis for Comprehensive 2D-LC (Lcxlc)
    219
- Installation
  222
- Overview
  222
- Use Gcimage Software
  223
9 Troubleshooting and Diagnostics

231
- Overview of the Module's Indicators and Test Functions
  232
- User Interfaces
  233
- Agilent Lab Advisor Software
  234
- The Basic Principle of Troubleshooting
  235
- Pressure too High
  238
- Pressure too Low
  239
- Peak Area and Peak Height Related
  240
- Retention Time Related
  241
- Missing Signal Linearity
  242
- Drifting Signal
  243
- Signal Noisy
  244
  - Recommended Tests to Conclude Troubleshooting
    245
10 Error Information

246
- What Are Error Messages
  
  247
- General Error Messages
  
  248
  - Timeout
    248
  - Shutdown
    249
  - Lost CAN Partner
    250
  - Remote Timeout
    250
  - Leak Sensor Open
    251
  - Leak Sensor Short
    251
  - Compensation Sensor Open
    252
  - Compensation Sensor Short
    252
  - Fan Failed
    253
  - Leak
    253
- Module-Specific Error Messages
  
  254
  - Initialization of Valve Failed
    254
  - Valve Switching Failed
    255
  - Valve Tag Violation
    255
  - Position Cluster Partner Missing
    256
  - Pressure Cluster Partner Missing
    256
  - External Valve Falls into Resident Mode
    257
11 Maintenance

258
- Introduction to Maintenance
  259
- Warnings and Cautions
  260
- Overview of Maintenance
  262
- Cleaning the Module
  263
- Correcting Leaks
  264
- Correcting Leaks (G7116B)
  264
- Correcting Leaks (G1170A)
  265
  - Replace Valve Heads
    266
- Replace Valve Heads (G7116B)
  266
- Replace Valve Heads (G1170A)
  269
12 Parts for Maintenance

277
- 2D-LC Loops
  278
- 2D-LC Capillaries
  279
- ASM Capillaries
  280
- Pressure Release Kit
  281
- 2D-LC Easy Starter Kit
  282
- Valve Drive Parts
  283
- Valve Driver Parts Infinity II
  284
- Valve Head Parts
  285
- Technical Specifications
  286
- Tools
  286
  - Vale Options Overview (for 2D-LC)
    287
- Obsolete Valve Heads
  290
  - MS Diverter Valve
    291
- Additional Parts for the MS Diverter Valve Setup
  292
  - Valve Options Overview (for G7116B)
    293
  - Additional Heater Devices
    295
- Additional Heater Devices (for G7116B)
  296
  - Accessories and Consumables (for G7116B)
    297
  - Infinitylab Quick Connect and Quick Turn Fittings
    299
- Infinitylab Quick Connect Fittings
  300
- Infinitylab Quick Connect Fitting Replacement Capillaries
  301
- Infinitylab Quick Turn Fitting
  302
  - Capillary Kits
    303
  - Important Customer Web Links
    304
- Alternative Ways to Install the System Legacy Stack Configuration
  306
- Agilent 2D-LC Solution with the Selectivity of Mass Selective Detection (MSD)
  311
  - Agilent 2D-LC Solution with an Agilent Single Quadrupole Detector
    312
  - Agilent 2D-LC Solution with High-End MS Detection
    318
- Theoretical Background
  322
  - Theoretical Basis of 2D-LC
    323
  - Orthogonality
    325
  - Resolution
    325
  - Peak Capacity
    328
    
    2Nd Dimension as Detector
    331
    
    Successful Mode Combinations
    333
    
    Solvent Elution Modes
    334
    
    Practical Issues
    340
16 Appendix

342
- General Safety Information
  343
- Safety Standards
  343
- Before Applying Power
  344
- General
  344
- Ground the Instrument
  344
- Do Not Operate in an Explosive Atmosphere
  345
- Do Not Remove the Instrument Cover
  345
- Do Not Modify the Instrument
  346
- In Case of Damage
  346
- Solvents
  347
- Safety Symbols
  348
  - Waste Electrical and Electronic Equipment (WEEE) Directive
    350
  - Radio Interference
    351
  - Sound Emission
    352
  - Solvent Information
    353
  - Further Information
    354
  - Agilent Technologies on Internet
    355

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Agilent Technologies 1290 Infinity II 2D-LC Solution Manuals

Agilent Technologies 1290 Infinity II 2D-LC Solution User Manual (395 pages)

Table of Contents

Table of Contents

2 Concepts of 2D-Lc

3 Compatibility Matrix

4 Installation

5 2D-Lc Data Acquisition in Masshunter Workstation 11

6 Method Parameters

Method Editor 2D-LC

Set the 2D-LC Method Parameters

Preview (2D-LC)

Set up a Peak-Based Experiment Graphically

Setup 2D Gradient Graphically

Setup Second Dimension Gradient with the Graphical User Interface

Additional Information

7 Method Development of Active Solvent Modulation (Asm)

8 Run the System

10 Troubleshooting and Diagnostics

Overview of the Module's Indicators and Test Functions

User Interfaces

Agilent Lab Advisor Software

Lab Advisor Instrument Control

Lab Advisor Service & Diagnostic

The Basic Principle of Troubleshooting

Table of Contents

11 Error Information

What Are Error Messages

General Error Messages

Module-Specific Error Messages

12 Maintenance

13 Parts for Maintenance

15 Appendix

Agilent Technologies 1290 Infinity II 2D-LC Solution User Manual (356 pages)

Table of Contents

Table of Contents

2 Concepts of 2D-Lc

3 Compatibility Matrix

4 Installation

5 Method Parameters

Method Parameters Standard Heart-Cutting 2D-LC

Method Parameters Multiple Heart-Cutting and High Resolution Sampling

2 D-Lc

Method Parameters Comprehensive 2D-LC

Method Development of Active Solvent Modulation (ASM)

6 Run the System

8 Data Analysis

9 Troubleshooting and Diagnostics

10 Error Information

What Are Error Messages

General Error Messages

Module-Specific Error Messages

11 Maintenance

12 Parts for Maintenance

16 Appendix

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