Waters Autospec Premier Operator's Manual page 18

Acquiring analog data ................................................................................... 4-14
5 Calibrating the instrument .................................................................. 5-1
Overview ............................................................................................................. 5-1
Calibration files ................................................................................................. 5-2
Calibrating the instrument for SIR experiments ...................................... 5-2
Calibrating the instrument for MIKES and NRMS experiments .......... 5-5
Calibrating the instrument for scanning experiments ............................ 5-5
Manually correcting a calibration ................................................................ 5-7
Editing the calibration parameters .............................................................. 5-9
Saving a calibration ....................................................................................... 5-12
Applying the calibration ............................................................................... 5-12
Associating a calibration file with an experiment .................................. 5-13
6 Inlets and probes .................................................................................... 6-1
The GC interface ............................................................................................... 6-2
Installing the GC column ................................................................................ 6-3
Required materials .......................................................................................... 6-3
The solids sample introduction probe ......................................................... 6-4
Making the probe cooling water connections ................................................. 6-5
Fitting the probe tip to the probe
Loading sample into the sample cup .............................................................. 6-6
Fitting the sample cup to the probe tip
Removing the sample cup from the probe tip
Inserting the solids sample introduction probe in the ion source
Removing the probe from the ion source
Ramping the probe temperature ................................................................. 6-14
The Probe Control dialog box's Options tab ................................................. 6-14
The Probe Control dialog box's Ramps tab................................................... 6-16
The Probe Control dialog box's Control tab.................................................. 6-18
4 Table of Contents
..................................................................... 6-6
............................................................ 6-8
.................................................. 6-9
....................................................... 6-13
.................. 6-9