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ACQUITY Refractive Index Detector
Waters ACQUITY Refractive Index Detector Manuals
Manuals and User Guides for Waters ACQUITY Refractive Index Detector. We have
1
Waters ACQUITY Refractive Index Detector manual available for free PDF download: Overview And Maintenance Manual
Waters ACQUITY Refractive Index Detector Overview And Maintenance Manual (98 pages)
Brand:
Waters
| Category:
Laboratory Equipment
| Size: 1.21 MB
Table of Contents
Copyright Notice
3
Trademarks
3
Customer Comments
3
Contacting Waters
4
Safety Considerations
4
High Voltage Hazard
5
FCC Radiation Emissions Notice
5
Electrical Power Safety Notice
5
Safety Hazard Symbol Notice
5
Equipment Misuse Notice
5
Safety Advisories
6
Operating this Instrument
6
Applicable Symbols
6
Audience and Purpose
7
Intended Use of the ACQUITY Refractive Index Detector
7
Calibrating
7
Quality-Control
7
ISM Classification
8
ISM Classification: ISM Group 1 Class B
8
EC Authorized Representative
8
Table of Contents
9
1 The ACQUITY Refractive Index Detector
13
Location of the Refractive Index Detector in an Example System
15
Operating Principles
15
Optical Refraction
15
Differential Refractometry
20
Common Refractive Index Detection Problems
23
Environmental Factors
23
Inhomogeneities in Solution
23
Range and Attenuation
24
Features
24
Fluid Path Components
25
Flow Path
25
Purge Mode
27
Recycle Mode
29
Countercurrent Heat Exchanger
30
Flow Cell
30
Purge Valve
30
Pressure Relief Valve
30
Recycle Valve
31
Insulated Sample Inlet Tubing
31
Optics
32
Selecting the Appropriate Sampling Rate
33
Filtering Noise
34
Polarity
35
Temperature Control
36
2 Preparing the Detector
37
Stacking the Modules
38
Installing the Leak Sensor
39
Installation Recommendations for Fittings
41
Connecting a Column or Second Detector
42
Connecting to Waste
43
Making the Recycle Connection
44
Installing the Multi-Detector Drip Tray
45
Making the Ethernet Connection
45
Making Signal Connections
45
Connecting to the Electricity Source
48
Typical Solvent Problems
49
Selecting a Solvent
49
Solvent Quality
49
Preparation Checklist
50
Water
50
Buffers
50
Tetrahydrofuran (THF)
51
Refractive Indices of Common Solvents
51
Solvent Degassing
52
Gas Solubility
52
Solvent Degassing Methods
53
Solvent Degassing Considerations
54
3 Using the Detector
57
Starting the Detector
58
Monitoring Detector Leds
59
About the Detector Control Panel
60
Resolving Leak Sensor Errors
63
Shutting down the Detector
66
Removing Buffered Mobile Phase
67
4 Maintenance Procedures
69
Maintaining the Detector
70
Contacting Waters Technical Service
70
Maintenance Schedule
71
Configuring Maintenance Warnings
72
Spare Parts
72
Troubleshooting with Connections INSIGHT
72
Safety and Handling
74
Replacing the Leak Sensor
75
Decontaminating the Fluid Path
77
Cleaning the Refractive Index Detector's Exterior
79
A Safety Advisories
81
Warning Symbols
81
Task-Specific Hazard Warnings
81
Specific Warnings
82
Caution Advisory
84
Warnings that Apply to All Waters Instruments and Devices
85
Electrical and Handling Symbols
90
Electrical Symbols
90
Handling Symbols
91
Physical Specifications
93
B Specifications
94
Environmental Specifications
94
Electrical Specifications
94
Input/Output Specifications
95
Performance Specifications
95
Wetted Materials of Construction
97
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