Micromeritics ASAP 2460 Operator's Manual page 323

Accelerated surface area and porosimetry system
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ASAP 2460 Operator's Manual
Action A:
Cause B:
Action B:
6522-
Time limit exceeded while evacuating manifold.
Cause A:
Action A:
Cause B:
Action B:
Cause C:
Action C:
6523-
Analysis suspended: Time limit exceeded while evacuating sample
(unrestricted).
Cause:
Action:
246-42800-01 - Dec 2013
Set the analysis gas regulator to 15 psig (1.0 bar). Then resume the
analysis.
The analysis gas bottle is empty.
Connect a new analysis gas bottle. Then resume the analysis.
Maximum manifold evacuation time was exceeded before the vacuum
set point was achieved. Vacuum pump may be turned off.
Turn on vacuum pump switch. Then restart the analysis.
The vacuum pump oil level is low.
Check the vacuum pump oil level and add more oil if necessary. Then
restart the analysis.
The manifold is contaminated or leaking.
Correct the problem. Refer to Appendix D,
LYZER FOR
LEAKS.
The maximum time for evacuating the sample through the unrestricted
valve was exceeded.
Check the sample tube and the sample tube fitting; ensure that the tube
is securely attached to the port. Verify that the sample is properly
degassed; then restart the analysis.
Appendix B
TESTING THE ANA-
B-43

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