Micromeritics Gemini VII 2390p Manuals

Manuals and User Guides for Micromeritics Gemini VII 2390p. We have 2 Micromeritics Gemini VII 2390p manuals available for free PDF download: Operator's Manual, Installation Instructions And Checklist

Micromeritics Gemini VII 2390p Operator's Manual (426 pages)

Brand: Micromeritics | Category: Measuring Instruments | Size: 20 MB

Section 1

5
- Table of Contents
  5
- General Information
  
  13
  - Introduction
    13
  - Organization of the Operator's Manual
    13
    
    Conventions
    15
  - Equipment Description
    15
    
    Operation
    17
    
    Cryogen
    18
    
    Degasser
    18
    
    Vacuum Pump
    18
  - Software
    19
    
    Report Features
    19
    
    User-Defined Reports
    19
  - Gases
    19
  - Specifications
    20
- User Interface
  
  23
  - Introduction
    23
  - Instrument Components and Connectors
    23
    
    Front Panel
    24
    
    Sample Compartment
    25
    
    Rear Panel
    26
  - Turning the Analyzer on and off
    27
    
    Turning the Analyzer off
    27
    
    Turning the Analyzer on
    27
  - Using the Software
    28
    
    Shortcut Keys
    28
    
    Shortcut Menus
    28
    
    File Name Conventions
    30
    
    File Status and Description
    30
    
    Files
    30
  - Menu Structure
    31
    
    Main Menu Bar
    32
    
    Window Menu
    33
    
    Help Menu
    34
- Operating Procedures
  
  37
  - Introduction
    37
  - Specifying Sample Defaults
    37
    
    Advanced Format
    38
    
    Basic Format
    40
    
    Restricted Format
    41
  - Defining Sample Information Files
    42
    
    Advanced Format
    42
    
    Basic or Restricted Format
    43
    
    Opening Files with a Status of Complete, Analyzing, or Entered
    45
    
    Opening Files with a Status of Preparing, Prepared, or no Analysis
    45
    
    Opening Sample Information Files
    45
  - Defining Parameter Files
    47
    
    Degas Conditions
    48
    
    Analysis Conditions
    49
    
    Adsorptive Properties
    50
    
    Report Options
    51
  - Preparing for Analysis
    52
    
    Cleaning and Labeling Sample Tubes
    53
    
    Determining the Sample Mass
    54
    
    Degassing the Sample
    56
    
    Installing the Sample Tube
    57
    
    Installing the Analysis Dewar
    58
  - Performing an Analysis
    60
    
    Start Analysis
    61
    
    Quickstart Analysis
    62
    
    Blank Analysis
    63
  - Generating Reports
    64
  - Printing Files
    66
  - Listing Files
    67
  - Exporting Isotherm Data
    68
    
    Format of Exported Data
    69
  - Converting Files
    70
  - Generating Graph Overlays
    71
    
    Multiple Sample Overlays
    71
    
    Multiple Graph Overlays
    76
- Software and Setup Modifications
  
  79
- File Menu
  
  111
  - Introduction
    111
  - Common Fields and Buttons - File Menu Options
    111
  - Open
    114
  - Save
    114
  - Save as
    115
    
    Save as (T-Curve or Alpha-S Curve)
    115
  - Save All
    116
  - Close
    116
  - Close All
    116
  - Print
    116
  - List
    116
  - Export
    116
  - Convert
    117
  - Exit
    117
  - Sample Information Files
    118
  - Degas Conditions Files
    120
  - Analysis Conditions Files
    121
  - Adsorptive Properties Files
    127
  - Report Options Files
    128
    
    Summary Report
    130
    
    Isotherm Report Options
    132
    
    Bet/Langmuir Surface Area Report Options
    134
    
    Freundlich Report Options
    137
    
    Temkin Isotherm Report Options
    138
    
    T-Plot Report Options
    140
    
    Alpha-S Method
    143
    
    F-Ratio Method
    144
    
    BJH Adsorption/Desorption Report Options
    146
    
    Tabular Report Options
    148
    
    Plot Options
    150
    
    Dollimore-Heal Adsorption/Desorption Report Options
    151
    
    Plot Options
    155
    
    Tabular Report Options
    155
    
    DFT Pore Size Report Options
    156
    
    DFT Surface Energy Report Options
    159
    
    Dubinin Report Options
    159
    
    Tabular Report Options
    160
    
    Transformed Isotherm Plot Options
    161
    
    Pore Volume Options
    162
    
    MP-Method Report Options
    163
    
    Plot Options
    164
    
    Tabular Report Options
    164
    
    Options Report
    165
    
    Sample Log Report
    165
    
    Validation Report
    166
  - Entered or Collected Data File
    167
- Unit Menu
  
  169
  - Introduction
    169
  - Common Fields and Buttons - Unit Menu Options
    170
  - Start Analysis
    170
  - Quickstart Analysis
    173
  - Start Po Measurement
    174
  - Blank Analysis
    175
  - Enable Manual Control
    176
    
    Instrument Schematic Components
    177
    
    System Valves
    178
    
    Instrument Schematic Shortcut Menus
    179
  - Show Instrument Schematic
    180
  - Show Status
    181
  - Show Instrument Log
    183
  - Unit Configuration
    184
  - Diagnostics
    185
  - Calibration
    187
    
    Match Transducers
    188
    
    Zero Pressure
    188
    
    Balance Servo
    189
    
    Reset Pressure Calibration
    189
    
    Sample Servo
    189
    
    Save to File
    190
    
    Load from File
    191
  - Service Test
    191
- Reports Menu
  
  193
  - Introduction
    193
  - Common Fields and Buttons - Reports Menu Options
    194
  - Start Report
    194
  - Close Reports
    195
  - Open Report
    195
  - SPC Report Options
    195
  - Regression Report
    197
  - Control Chart
    199
  - Heat of Adsorption Report
    202
  - Report Features and Shortcuts
    204
    
    Report Header
    205
    
    Report Tool Bar
    206
    
    Report Header Shortcuts
    209
    
    Report Shortcut Menus
    209
    
    Tabular Reports Shortcuts
    210
    
    Graph Shortcuts
    211
    
    Axis Cross-Hair
    215
    
    Other On-Screen Features
    215
    
    Zoom Feature
    215
  - Report Examples
    216
    
    Isotherm Linear Plot
    217
    
    BET Surface Area Report
    218
    
    BET Surface Area Plot
    219
    
    T-Plot
    220
    
    BJH Adsorption Cumulative Pore Volume
    221
    
    BJH Adsorption DV/Dlog(W) Pore Volume
    222
- Options Menu
  
  223
  - Introduction
    223
  - Option Presentation
    223
  - Sample Defaults
    224
    
    Restricted Format
    224
  - Units
    225
  - Graph Grid Lines
    225
  - Service Test Mode
    226
- Troubleshooting and Maintenance
  
  227
  - Introduction
    227
  - Troubleshooting
    227
  - Preventive Maintenance
    230
    
    Recovering from a Power Failure
    230
    
    Cleaning the Analysis Dewar
    231
    
    Cleaning the Analyzer
    231
    
    Lubricating Elevator Drive Assembly
    231
    
    Replacing Port Filter (Frit) and O-Ring
    232
    
    Replacing the Sample Tube O-Ring
    233
    
    Changing or Adding Oil
    234
    
    Inspecting and Changing Vacuum Pump Oil
    234
    
    Inspecting the Oil
    234
    
    Replacing the Alumina in the Oil Vapor Trap
    237
    
    Changing the Vacuum Pump Exhaust Filter
    241
    
    Performing a Leak Test
    242
  - Connecting Gases
    244
    
    Disconnecting the Depleted Bottle
    244
    
    Guidelines for Connecting Gases to the Analyzer
    244
    
    Connecting a Replacement Gas Bottle
    245
    
    Cleaning and Verifying the Gas Line
    248
  - Performing a Blank Analysis for Diagnostic Purposes
    252
  - Performing a Reference Analysis
    254
    
    Analyzing Reference Material
    255
  - Calibrating the System
    256
    
    Zero Pressure
    256
    
    Match Transducers
    257
    
    Sample Servo
    257
    
    Balance Servo
    258
- Forms
  
  263
  - Sample Data Worksheet
    265
- Error Messages
  
  267
  - 2400 Series
    267
  - 2500 Series
    273
  - 4000 Series
    276
  - 6000 Series
    288
- Calculations
  
  295
  - Saturation Pressure
    295
  - Relative Pressure Calculations
    295
  - Quantity Adsorbed Calculations
    296
    
    Free Space
    296
    
    Measured
    296
    
    Calculated
    297
  - Thermal Transpiration Correction
    299
  - BET Surface Area
    300
  - Langmuir Surface Area
    301
  - T-Plot
    302
  - BJH Pore Volume and Area Distribution
    304
    
    Explanation of Terms
    304
    
    Calculations
    305
    
    Compendium of Variables
    312
  - Horvath-Kawazoe
    313
    
    Slit Pore Geometry (Original HK
    313
    
    Cylinder Pore Geometry (Saito/Foley
    314
    
    Sphere Pore Geometry (Cheng/Yang
    315
    
    Cheng/Yang Correction
    316
    
    Interaction Parameter
    317
    
    Additional Calculations
    318
    
    Interaction Parameter Components
    319
  - Dubinin-Radushkevich
    321
  - Dubinin-Astakhov
    323
  - MP-Method
    327
  - Freundlich Isotherm
    329
  - Temkin Isotherm
    329
  - DFT (Density Functional Theory
    330
    
    The Integral Equation of Adsorption
    330
    
    Application to Pore Size Distribution
    331
    
    Application to Surface Energy Distribution
    331
    
    Performing the Deconvolution
    332
    
    Regularization
    332
  - SPC Report Variables
    333
    
    Regression Chart Variables
    333
    
    Control Chart Variables
    334
  - Summary Report
    334
  - References
    336
- Ethernet Configuration
  
  337
  - Configuring the Ethernet Port
    337
    
    Windows 7
    337
    
    Windows Vista
    341
- Analyzing Samples with Total Surface Area of 1.0M2 or Less
  
  343
  - Introduction
    343
  - Using Glass Beads
    343
  - Using Filler Rods
    345
  - Using Glass Beads and Filler Rods
    346
- Dft Models
  
  347
  - Models Based on Statistical Thermodynamics
    347
    
    Theoretical Background
    347
    
    Molecular Simulation Methods
    348
    
    Monte Carlo Method
    348
    
    Density Functional Formulation
    349
    
    Models Included
    353
    
    Non-Local Density Functional Theory with Density-Independent Weights
    353
  - Models Based on Classical Theories
    359
    
    Pore Size
    359
    
    Surface Energy
    359
    
    Kelvin Equation with Halsey Thickness Curve
    360
    
    Models Included
    360
    
    Kelvin Equation with Harkins and Jura Thickness Curve
    361
    
    Kelvin Equation with Broekhoff-De Boer Thickness Curve
    362
  - References
    363
- Index
  
  365
  - Elements Used in this Manual
    377
  - Contact Us
    379
Section 2

381
- 1 About the Smart Vacprep
  
  383
  - Specifications for the Smart Vacprep
    385
  - Set the Voltage for the Smart Vacprep
    386
- 2 About the Software
  
  387
  - Add or Remove a Smart Vacprep
    387
    
    Add a Smart Vacprep Unit
    388
    
    Remove a Smart Vacprep Unit
    388
  - Smart Vacprep Configuration
    389
- 3 Operate the Smart Vacprep
  
  391
  - Backfill the Smart Vacprep Ports
    391
  - Evacuate the Smart Vacprep Ports
    391
  - Quickstart Degas Conditions
    393
    
    Load Quickstart Degas Conditions into a Sample File
    394
  - Start Smart Vacprep Degas
    395
  - Show Smart Vacprep Dashboard
    397
  - Show Smart Vacprep Log
    398
  - Show Smart Vacprep Schematic
    399
    
    Smart Vacprep Schematic Shortcut Menus
    400
  - Show Smart Vacprep Status
    401
- 4 Smart Vacprep Calibration
  
  403
  - Smart Vacprep Pressure Offset
    403
  - Smart Vacprep Servo Valve Calibration
    404
- 5 Smart Vacprep Diagnostics
  
  405
- 6 Maintenance and Troubleshooting
  
  416
  - Replace the Vacuum Pump Exhaust Filter
    417
- 7 Parts and Accessories for the Smart Vacprep
  
  419
- 8 Error Messages
  
  421
- Index Index
  
  426

Micromeritics Gemini VII 2390p Installation Instructions And Checklist (113 pages)

SURFACE AREA ANALYZER

Brand: Micromeritics | Category: Measuring Instruments | Size: 5 MB

Warranty
3
Corporate Profile
4
Contact Us
5
About this Manual
6
General Safety
7
Table of Contents
10
1 Installation Overview

13
- Prepare for Installation
  13
- Safe Servicing
  14
- Power
  15
- Parts and Accessories
  15
2 Equipment Installation

17
- Vacuum Pump
  18
- Connect Ethernet Cable
  19
- Connect the Power Cord
  20
  - Apply Power to the Analyzer
    20
- Connect Optional Smart Vacprep to Analyzer
  21
3 Keypad Only Installations

23
- Operational Verification
  26
  - Clean and Verify the Gas Line
    26
  - Reference Analysis
    27
- Keypad and Keyboard Functions
  29
- RS-232 Operation
  31
- Communications
  32
- Data Results
  36
- Adsorptive Line Test
  38
- Helium Line Test
  40
4 Software Installation

43
- Start the Application
  51
5 Analyzer Preparation

53
- Unit Configuration
  53
- Unit Selection
  53
6 Gas Connections

55
7 Operational Verification

63
- Measure Saturation Pressure
  64
- Perform a Reference Material Analysis
  65
  - Clean and Label Sample Tubes
    67
  - Create Sample Files
    70
  - Determine the Sample Mass
    72
  - Degas Samples
    73
  - Sample Tube Installation
    74
  - Dewar Precautions
    76
- Fill and Install the Dewar
  77
- 21CFR11 Environments
  79
  - Overview
    79
    
    User Permissions
    80
  - Software Installation in 21CFR11 Environments
    83
    
    Uninstall Software in 21CFR11 Environments
    93
    
    Maintaining Confirm Users and Groups
    94
9 Installation Checklists

99
- Exceptions
  106
- Signatures
  107
- Final Documentation
  107
10 Worksheets

109
- Users and Groups Worksheet for 21CFR11
  110
- Sample Data Worksheet for Gas Adsorption
  111

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Micromeritics Gemini VII 2390p Manuals

Micromeritics Gemini VII 2390p Operator's Manual (426 pages)

Table of Contents

Section 1

General Information

User Interface

Operating Procedures

Software and Setup Modifications

File Menu

Unit Menu

Reports Menu

Options Menu

Troubleshooting and Maintenance

Forms

Error Messages

Calculations

Ethernet Configuration

Analyzing Samples with Total Surface Area of 1.0M2 or Less

Dft Models

Index

Section 2

1 About the Smart Vacprep

2 About the Software

3 Operate the Smart Vacprep

4 Smart Vacprep Calibration

5 Smart Vacprep Diagnostics

6 Maintenance and Troubleshooting

7 Parts and Accessories for the Smart Vacprep

8 Error Messages

Index Index

Micromeritics Gemini VII 2390p Installation Instructions And Checklist (113 pages)

Table of Contents

1 Installation Overview

2 Equipment Installation

3 Keypad Only Installations

4 Software Installation

5 Analyzer Preparation

6 Gas Connections

7 Operational Verification

9 Installation Checklists

10 Worksheets

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