Micromeritics ASAP 2460 Operator's Manual page 324

Appendix B
6524- Analysis suspended: Time limit exceeded while evacuating sample (servo).
Cause:
Action:
6525- Time limit exceeded while backfilling manifold to (target pressure) with (gas).
Cause A:
Action A:
Cause B:
Action B:
B-44
The maximum time for evacuating the sample through the restricted
valve was exceeded. Possible causes are a leak in the sample tube fit-
ting, a crack in the sample tube, or a poorly degassed sample.
Check the sample tube and the sample tube fitting; ensure that the tube
is securely attached to the port. Verify that the sample is properly
degassed; then resume the analysis.
The maximum time was exceeded before the target pressure point was
reached. The gas regulator may be set too low or turned off.
Set the gas regulator to 15 psig (1.03 bar). Then resume the analysis.
The gas bottle is empty.
Connect a new gas bottle. Then resume the analysis.
ASAP 2460 Operator's Manual
246-42800-01 - Dec 2013