Waters Xevo TQ MS Operator's, Overview And Maintenance Manual page 163

Hide thumbs Also See for Xevo TQ MS:
Table of Contents

Advertisement

Probe inlet connector
3.
Fit the UNF coupling to the new capillary.
4.
Use the needle-nose pliers to slide a new ferrule onto the capillary.
5.
Insert the capillary in the PEEK union, and ensure that it is fully seated.
6.
Screw the UNF coupling into the PEEK union, finger-tight only.
7.
Gently tug on the capillary, testing to ensure that it stays in place.
8.
Use the 7-mm wrench to tighten the locknut against the PEEK union.
Warning:
goggles when performing the leak test.
9.
Perform a leak test by attaching the free end of the PEEK tubing to an
LC pump and pumping 50:50 acetonitrile/water through it at 1 mL/min.
If leakage occurs, disassemble and remake the connection, and
repeat the leak test.
If the backpressure on the LC pump is high, replace the capillary,
and repeat the leak test.
10. When no leakage occurs and the backpressure on the LC pump is
normal, disconnect the PEEK tubing from the LC pump.
11. Remove the probe inlet connector and PEEK tubing from the PEEK union.
12. Remove the probe heater (see
page
166,
step 2
PEEK tubing
To avoid high-pressure liquid jet spray, wear safety
"Replacing the APCI probe heater" on
through
step
4).
February 11, 2013, 71500130002 Rev. D
Replacing the APCI probe sample capillary
TP02671
163

Advertisement

Table of Contents
loading

Table of Contents