Waters 717plus Manuals

Waters 717plus Manuals

Manuals and User Guides for Waters 717plus. We have 1 Waters 717plus manual available for free PDF download: Operator's Manual

Waters 717plus Operator's Manual

Waters 717plus Operator's Manual (181 pages)

Autosampler

Brand: Waters | Category: Laboratory Equipment | Size: 2 MB

Table of Contents

Table of Contents
14
Preface
24
Chapter 1 Introduction

27
- Description
  27
- Waters 717Plus Autosampler
  27
  - Features
    28
  - Components and Subsystems
    31
- Waters 717Plus Autosampler Subsystems
  32
Chapter 2 Installation

33
Chapter 3 Startup and Configuration

55
- Powering up the Autosampler
  55
- Power Switch Location
  55
  - Using the Front Panel
    56
- Main Menu
  56
  - Accessing Menus
    57
- Front Panel
  57
- Menu Functions
  57
  - Entering Operating Parameters
    58
- 717Plus Autosampler Menu Flowchart
  58
  - Flushing the Autosampler
    59
  - Calibrating the Seal Pak
    59
    
    Purging the Autosampler
    59
    
    Auto Zeroing the Transducer
    60
- Path to Auto Zero Pressure Page
  61
  - Calibrating the Seal Pak
    62
- Path to Seal Pak Calibration Page
  63
  - Priming the Needle Wash Pump
    64
  - Configuring the Autosampler
    65
    
    Overview of Configuration
    65
- Autosampler Configuration Flowchart
  66
- Configuration Parameters
  67
  - Setting Parameters for LC System Operation
    68
- Setting the Integrator Report Delay
  69
- Setting Terminal Signal Parameters
  70
- Hold Logic
  70
  - Entering Hardware Changes
    72
- Setting IEEE-488 Address
  72
- Configuration Page 3
  73
  - System Verification
    74
- Purge Menu
  74
  - Power down and Storage
    75
    
    Removing Buffered Mobile Phase
    75
    
    Powering down
    75
    
    Storage
    76
Chapter 4 Operating the Autosampler

77
- Overview of Operation
  77
- Overview of Operations
  78
  - Preparing Samples
    79
- Preparing Samples
  80
  - Selecting Sample Vials
    81
  - Selecting a Needle Wash Solvent
    82
- Sample Vial Assembly
  82
- Suggested Needle Wash Solvents
  83
  - Loading the Carousel
    84
- Improper Needle Wash Solvent Location
  84
- Inserting the Carousel
  85
  - Ensuring Reproducibility
    86
    
    Overview of Reproducibility
    86
    
    Performing a Purge
    87
- Purging the Autosampler
  87
- Purge and Compressibility Page
  88
- Autosampler Volume
  88
  - Performing a Compression Check
    89
- Purge Time Examples
  89
- Running a Compressibility Test
  90
  - Running Autosampling
    91
    
    Programming Auto Run
    92
- Overview of Programming
  92
- Edit: Auto Run Screen
  93
  - Programming Step Functions
    96
- Edit: Step Function Screen
  96
  - Using Auto Standards
    98
- Edit: Auto Standards Screen
  99
- Example Auto Standard Run 1
  101
  - Using Auto Addition
    102
- Auto Addition Screen
  104
  - Using Auto Transfer
    106
- Auto Transfer Screen
  108
- Transfer before Step
  111
- Transfer before Vial
  112
  - Programming the Event Output
    113
- Transfer before Injection
  113
  - Starting and Stopping an Auto Run
    114
- Edit: Step Function Screen
  114
  - Monitoring Auto Run Status
    115
- Parameters
  115
  - Making a Stat Run
    116
- Edit Stat Run Screen
  117
- Status: Stat Run
  118
  - Sampling Considerations
    119
    
    Temperature Control
    119
    
    Microbore/Semiprep Injections
    120
- Changing Syringe Configuration
  121
- Entering the Semiprep Configuration
  122
  - Injecting Viscous Samples
    123
- Sample Draw Rate
  123
  - Purging During an Auto Run
    124
- Setting Sample Draw Rate
  124
  - Using Buffered Mobile Phase
    125
- Enabling Auto Purge
  125
- Enabling Purge in Idle
  126
Chapter 5 Maintenance

127
- Defrosting the Heater/Cooler
  127
- Defrost Menu Flowchart
  128
  - Replacing the Syringe
    129
    
    Removing the Syringe
    129
- Syringe Assembly Components
  130
- Positioning the Syringe for Removal
  131
  - Installing the New Syringe
    132
- Installing the Syringe
  133
- Changing Syringe Volume
  134
  - Replacing the Seal Pak
    135
    
    Removing the Injector
    136
    
    Removing the Seal Pak
    137
- Removing the Injector (Shown with Safety Shield Removed)
  137
  - Replacing the Needle
    138
- Bottom View of Injector
  138
- Needle Removal
  138
  - Installing a New Seal Pak
    139
  - Installing the Injector
    139
  - Calibrating the Seal Pak
    140
  - Replacing In-Line Filters
    140
- Locating In-Line Filters
  141
Chapter 6 Troubleshooting

143
- Safety and Handling
  143
- Error Messages
  144
- Error Message Type
  144
  - Informational Error Messages
    145
  - Calibration (CAL) Error Messages
    145
- CAL Error Messages
  145
  - Carousel (CAR) Error Messages
    146
- CAR Error Messages
  146
  - Heater/Cooler (H/C) Error Messages
    147
  - Injector (INJ) Error Messages
    147
- H/C Error Messages
  147
- INJ Error Messages
  147
  - Syringe (SYR) Error Messages
    148
  - Troubleshooting Tables
    148
- SYR Error Messages
  148
- Autosampler Troubleshooting
  148
  - Troubleshooting Procedures
    154
    
    Manual Syringe Purge
    154
    
    Valve Leak Test
    155
- Positioning the Syringe for Manual Purge
  155
- Valve and Motor Operations
  156
  - Manual Transducer Adjustment
    158
- Accessing the Auto Zero Pressure Page
  159
- Adjusting the Transducer
  160
Appendix A Specifications

161
- Operational Specifications
  161
- Mechanical Specifications
  161
- Environmental Specifications
  161
- A-2 Mechanical Specifications
  162
- Communications
  163
- A-5 Communications
  163
Appendix B Spare Parts

164
Appendix C Reproducibility and Solvent Degassing

167
- Factors Affecting Reproducibility
  167
  - Chemical Factors Affecting Reproducibility
    167
  - Instrument Factors Affecting Reproducibility
    168
- Solvent Degassing
  169
  - Theory of Solvent Degassing
    169
  - Solvent Degassing Methods
    170
  - Solvent Degassing Considerations
    171
Appendix D Selecting Sample Vials

173
- Index
  175

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