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Xevo TQ-GC
Waters Xevo TQ-GC Manuals
Manuals and User Guides for Waters Xevo TQ-GC. We have
1
Waters Xevo TQ-GC manual available for free PDF download: Overview And Maintenance Manual
Waters Xevo TQ-GC Overview And Maintenance Manual (137 pages)
Brand:
Waters
| Category:
Laboratory Equipment
| Size: 7 MB
Table of Contents
General Information
2
Trademarks
2
Customer Comments
3
Manufacturing Information
3
Safety Considerations
4
Considerations Specific to the Device
4
Safety Hazard Symbol Notice
6
Equipment Misuse Notice
6
Safety Advisories
6
Operating the Device
6
Applicable Symbols
7
Audience and Purpose
8
Intended Use of the Xevo TQ-GC
8
Quality Control
8
EMC Considerations
8
FCC Radiation Emissions Notice
9
Canada Spectrum Management Emissions Notice
9
ISM Classification: ISM Group 1 Class a
9
EMC Emissions
9
Table of Contents
10
1 Waters Xevo TQ-GC Overview
15
Intellistart Technology
16
Waters Xevo TQ-GC
17
Software and Data System
17
Ionization Techniques
18
Electron Ionization (EI) Mode
18
Chemical Ionization (CI) Mode (Optional)
18
Xevo TQ-GC Operation
18
Ionization Source
20
The Inner Source Assembly
22
The Mounting Flange
25
The Outer Source Assembly
25
Gas Requirements
27
Sample Inlets
28
GC Interface
28
Reference Sample Inlet
30
MS Operating Modes
30
MS Scanning Mode
30
SIR Mode
31
MS1 Scanning Mode
31
MS/MS Operating Modes
31
Product (Daughter) Ion Spectrum
31
Precursor (Parent) Ion Spectrum
32
MRM Mode
33
PICS Mode
33
Vacuum System
34
Rear Panel
34
2 Preparing the Mass Spectrometer for Operation
36
Preparing to Start the Mass Spectrometer
36
Starting the Mass Spectrometer
36
Verifying the Instrument's State of Readiness
38
Monitoring the Mass Spectrometer Leds
38
Power LED
38
Status LED
39
Tuning and Calibration Information
39
Configuring the GC Autosampler
39
Rebooting the Mass Spectrometer
39
Leaving the Mass Spectrometer Ready for Operation
40
Emergency Shutdown of the Mass Spectrometer
40
3 Changing the Mode of Operation
42
Changing the Inner Source Assembly from EI to CI Operation
42
Changing the Inner Source Assembly from CI to EI Operation
46
4 Maintenance Procedures
51
Maintenance Schedule
51
Spare Parts
53
Safety and Handling
53
Preparing the Instrument for Working on the Source
54
Using Masslynx Software to Prepare the Instrument for Working on the Inner and Outer Sources
54
Preparing the GC Oven for Working on the Capillary Column
55
Removing and Refitting the Source Components
55
Removing the Inner Source Assembly from the Instrument
56
Removing the Mounting Flange Assembly from the Instrument
58
Removing the Outer Source Assembly from the Instrument
59
Fitting the Outer Source Assembly to the Instrument
62
Fitting the Mounting Flange Assembly to the Instrument
63
Fitting the Inner Source Assembly to the Instrument
64
Cleaning the Inner Source Components
65
Disassembling the Inner Source for Cleaning
66
Cleaning the Repeller and the Ionization Chamber
69
Assembling the Inner Source after Cleaning
70
Replacing the Inner Source Assembly Filament
73
Replacing the Filament
73
Cleaning the Outer Source Assembly's Lenses
77
Removing the PCB Holder Assembly from the Lens Holder
78
Removing the Lenses and the Spacers from the Lens Holder
81
Cleaning the Lenses
84
Fitting the Lenses and the Spacers into the Lens Holder
86
Fitting the PCB Holder Assembly to the Lens Holder
90
Replacing the Reference Gas Ampule
93
Working on the GC Column
94
Precautions and Recommendations for Working on the Column
97
Cleaning the Instrument Case
98
Replacing the Gas Cylinders
98
Maintaining the Rotary Backing Pump Oil
98
Gas-Ballasting the Rotary Backing Pump
101
Replacing the Rotary Backing Pump's Demister Element
101
Replacing the Instrument's Fuses
101
5 Best Practices for Efficient Operation
102
GC Injector and Inlet
102
Air Leaks
102
Contaminated Sample Ampule and Reference Gas Line
103
Contaminated Source Components
103
Air in the CI Gas Inlet Line
104
Repelling Magnets on the Outer Source
104
6 Troubleshooting the Xevo TQ-GC
105
System Troubleshooting
105
Component Hardware Troubleshooting
105
No Ion Beam
105
Unstable or Low-Intensity Ion Beam
106
Poor Sensitivity with EI Source
107
Poor Sensitivity with CI Source
107
Poor Analyzer Vacuum
108
Poor Source Vacuum
109
Failure of Rotary Pump Fuse
109
Poor Resolution
109
High Noise Levels in MRM Analyses
110
A Safety Advisories
111
Warning Symbols
111
Specific Warnings
112
Notices
114
Bottles Prohibited Symbol
114
Required Protection
114
Warnings that Apply to All Waters Instruments and Devices
114
Warnings that Address the Replacement of Fuses
119
Electrical Symbols
120
Handling Symbols
121
B External Connections
123
External Wiring and Vacuum Connections
123
Connecting the Rotary Backing Pump
124
Making the Electrical Connections to the Rotary Backing Pump
127
About the Waters Hydrogen Control Box
128
Connecting to the Workstation
130
Connecting the Workstation to the Power Source
131
I/O Signal Connectors
131
Making I/O Signal Connections
133
Connecting to the Power Supply
136
C Stopping the GC Instrument Manually
137
Stopping the GC Instrument Manually Following a Sample-List Abort
137
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