Chemical checkout
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pA
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Figure 9. Sample FID checkout chromatogram
Released: March 2004
Press Prep Run to prepare the inlet for splitless injection. When "Ready
for manual inj" appears, inject 1 µL of the checkout sample and press
Start on the GC.
The chromatogram should be similar to
The acceptance criteria are:
•
Area counts for components labeled C14, C15, and C16 are all > 4,000.
•
The area counts ratio calculated as C14/C16 is 1.00 ± 0.05.
MDL (C16, pg/mL) = (436,000 × peak-to-peak noise)/(Area C16) ≤ 4.
•
If these criteria are not met, repeat the test. If after repeated testing the
criteria cannot be met, consult your service and user documentation for
additional information.
2
6850 Series II GC User Information
Figure
4
6
Time (min.)
Verifying Performance
FID checkout
9.
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