Agilent Technologies 6850 Series II User Information page 63

2.
3.
4.
Table 18. FID Checkout Conditions (Method FIDCKO)
Column and sample
Type
Sample
Injection volume
Inlets
Temperature
Inlet pressure
Split/splitless
Mode
Purge flow
Purge time
PTV
Mode
Inlet temperature
Initial time
Rate 1
Final temp 1
Final time 1
Rate 2
Final temp 2
Final time 2
Purge time
Purge flow
Detector
Temperature
H
2
Air flow
Makeup flow (N
Lit offset
Released: March 2004
Enter the parameter values listed in
Define the column.
Save the method. We suggest using the name FIDCKO.
flow
)
2
6850 Series II GC User Information
Table
HP-1, 30 m × 0.32 mm × 0.25 µm part number 19091Z–413E
FID/TCD checkout 18710-60170
1 µL
250°C Purged packed and split/splitless
Oven Track (cool on-column)
40°C PTV (see below)
25 psi (constant pressure, helium)
Splitless
60 mL/min
0.75 min
Splitless
40°C
0.1 min
720°C/min
350°C
2 min
100°C/min
250°C
0 min
0.75 min
60 mL/min
300°C
30 mL/min
400 mL/min
25 mL/min
Should be < 20 pA
Verifying Performance
18.
FID checkout
page 63 of 256