Waters Xevo TQ-S Operator's, Overview And Maintenance Manual page 19

Preparing the IntelliStart Fluidics system .................................................. 51
Installing the reservoir bottles.......................................................................... 51
Adjusting the solvent delivery tube positions .................................................. 53
Purging the infusion pump................................................................................ 54
Rebooting the mass spectrometer .................................................................. 55
Leaving the mass spectrometer ready for operation ................................ 56
Emergency shutdown of the mass spectrometer ........................................ 56
3 Changing the Mode of Operation ........................................................ 57
ESI mode .............................................................................................................. 57
Installing the ESI probe .................................................................................... 58
Removing the ESI probe.................................................................................... 62
ESCi mode ............................................................................................................ 62
Optimizing the ESI probe for ESCi operation.................................................. 63
APCI mode ........................................................................................................... 63
Installing the IonSABRE II probe .................................................................... 64
Removing the IonSABRE II probe .................................................................... 67
Combined APPI/APCI source .......................................................................... 67
APPI operation................................................................................................... 67
APCI operation................................................................................................... 68
Dual-mode operation ......................................................................................... 69
The combined APPI/APCI source components ................................................. 70
Installing the combined APPI/APCI source ..................................................... 72
Removing the IonSABRE II probe and combined APPI/APCI source enclosure..
73
NanoFlow ESI source ........................................................................................ 74
Installing the NanoFlow source ........................................................................ 76
Fitting a borosilicate glass capillary (nanovial) ............................................... 78
Positioning the borosilicate glass capillary tip................................................. 81
Restarting a stalled borosilicate glass capillary electrospray ......................... 82
ionKey source ..................................................................................................... 82
Installing the ionKey source ............................................................................. 83
February 28, 2014, 715002212 Rev. C xix