Exercise 2. Prepare The Samples For The Analyses - Agilent Technologies 6100 Series Familiarization Manual

Exercise 2. Prepare the samples for the analyses

In the exercises in the next chapters, you analyze a mixture of four
sulfonamide compounds. The Electrospray LC Demo Sample (p/n
59987-20033), contains five ampoules with 100 ng/μL each of these
compounds:
• sulfamethizole (M+H)
• sulfamethazine (M+H)
• sulfachloropyridazine (M+H)
• sulfadimethoxine (M+H)
Sulfamethizole
To perform the analyses in the following chapters, you must first prepare the
sample at various dilutions. The final concentrations will be 1, 5 and 10 ng/μL.
You will also prepare a solvent blank.
Agilent 6100 Series Quadrupole LC/MS Systems Familiarization Guide
+
= 271
+
Sulfamethazine
Exercise 2. Prepare the samples for the analyses
= 279
+
= 285
+
= 311.
Sulfachloropyridazine
Prepare for the Analysis
Sulfadimethoxine
1
13