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7
Run a Sequence
Prepare the Samples
100
Prepare 1:2 serial dilutions of the 100 ng/mL 5975 MSD
1
Sample (P/N 05970-60045 or P/N 5074-3025 Japan only ) in
hexane to make a 50 ng/mL and a 25 ng/mL method
calibration sample.
2
Prepare 1:2 serial dilutions of the 10 ng/mL 5975 MSD
Sample (P/N 05970-60045 or P/N 5074-3025 Japan only ) in
hexane to make a 5 ng/mL and 2.5 ng/mL method
calibration sample.
Fill the vials with approximately 500 µL of each standard
3
(2.5, 5, 10, 25, and 50 ng/mL).
If you are not using an ALS skip the remaining steps.
4
Place the sample vials in increasing order of concentration
into positions 1 through 5 of the GC sample tray.
Fill a solvent wash vial with isooctane and place it in
5
injector turret location A for solvent wash mode A, B.
6
Place an empty waste vial in turret location B specified for
solvent wash mode A, B.
Agilent G1701EA MSD Productivity ChemStation Familiarization Guide
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