Table Of Contents - PerkinElmer AAnalyst 700 User Manual

Table of Contents

Table Of Contents5
Safety And Regulatory Information9
Safety Practices And Conventions11
Correct Use Of The Instrument12
Electrical Safety13
Operating Conditions15
Laboratory Hygiene16
Laboratory Ventilation16
Safe Handling Of Chemicals17
Waste Disposal18
Contents Of Waste Containers18
Disposing Of Defective Lamps18
Uv Radiation19
High Temperatures20
Burner System20
Graphite Furnace20
Quartz Tube Atomizer Cell20
Handling Compressed Gases21
Summary Of Gas Hazards21
Identifying Cylinders21
Storing Cylinders22
Handling Cylinders23
Safety Practices For Flame Atomization24
Safety Interlocks24
Safe Use Of Burner Gases24
Air Supply25
Nitrous Oxide25
Acetylene26
Safe Operation Of The Flame27
The Drain System28
Flashbacks28
Hazards With Flame Atomization29
Safety Practices For Electrothermal Atomization30
Inert Gas30
Safety Checks30
Hazards With Electrothermal Atomization31
Safety Practices For Fias And Mercury Hydride Systems32
Hazards With Fias And Mercury Hydride Systems33
References For Laboratory Safety Practice34
Regulatory Information35
Electrical Protection35
Iec 1010 Compliance35
Installation Category35
Electromagnetic Compatibility (Emc)36
Symbols Used On The Instrument37
Warning Markings At The Front Of The Spectrometer38
Warning Markings On The Instrument38
Warning Markings On The Rear Panel40
Warning Markings On The Deuterium Lamp Cover43
Spectrometer Installation45
Before You Install The Spectrometer47
When The Spectrometer Arrives47
Before The Service Engineer Arrives47
When The Service Engineer Arrives47
Moving And Reinstalling The Spectrometer48
Preparing The Spectrometer To Be Moved48
Moving The Spectrometer49
Reinstalling The Spectrometer50
Connecting The Burner Gases51
What You Need To Provide51
What Is Provided With The Spectrometer51
To Connect The Gases52
Air52
Connecting The Furnace Gases54
To Connect Argon (Or Nitrogen) Only55
Connecting Argon (Or Nitrogen) Only56
To Connect Both Argon And A Special Gas57
Connecting Argon (Or Nitrogen) And A Special Gas58
To Connect The Drain System To The Burner59
To Install The Furnace Autosampler59
Connecting Cooling Sources60
Installing The Cooling System60
Connecting And Disconnecting The Water Hoses60
Connecting The Cooling System61
Filling The Cooling System62
Connecting External Cooling Sources63
Connecting The Main Water Supply63
Connecting Cooling Water Hoses65
Electrical Connections66
Summary66
Preparing The System For Analyses69
Switching On The System71
Required Pressures For The Burner Gases73
Required Pressures For The Furnace Gases74
Installing Lamps75
Lamp Compartment75
Installing And Connecting Lamps76
Lamp Holders In The Lamp Compartment76
Edls77
Removing Lamps78
Tips For Installing Lamps78
Installing Sample Trays79
To Shut Down The Flame System80
To Shut Down The Furnace System80
Shutting Down The System80
To Shut Down The Spectrometer81
Emergency Shutdown82
Spectrometer: System Maintenance83
Perkinelmer Service85
If The Spectrometer System Does Not Function Correctly85
Troubleshooting85
Maintenance Checklist86
General Preventative Maintenance Procedures86
Spectrometer, Maintenance Checklist86
Spectrometer Maintenance Procedures87
Cleaning The Windows Of The Optical System87
Maintaining The Electrical Components89
Parts That May Be Serviced By The User89
Resetting The Automatic Circuit Breaker90
Changing The Fuses90
Automatic Circuit Breaker And Fuses On The Rear Panel91
Changing The Air Filters92
Replacing The Deuterium Lamp93
Location Of Deuterium Lamp Inside The Spectrometer93
Deuterium Lamp Cover And Bracket Assembly94
Maintaining The Acetylene Supply96
Chapter 5 Parts And Supplies97
Parts Provided99
Obtaining Supplies, Replacement Parts, And Accessories100
What Is Listed In This Section100
Laboratory Requirements101
Introduction103
Bench And Location Requirements104
Fume Ventilation104
Space Requirements For The Spectrometer System105
Computer And Printer105
Accessories105
Electrical Requirements108
Gas Supply Requirements109
Specifications And Requirements Of The Burner Gases110
Acetylene Supply112
Nitrous Oxide Supply113
Furnace Gases114
Special Gas114
Specifications And Requirements Of The Furnace Gases115
Cooling The Spectrometer System116
Cooling System116
External Cooling116
Requirements For The Cooling Water Supply116
Lamps118
System Description119
The Aanalyst 700 Spectrometer System121
Concept121
Features Of The Aanalyst 700 System121
System Components122
System Control122
The Optical System124
Optical System125
Switches And Connectors On The Spectrometer126
Operational On/Off Switches126
Switches And Ports On The Front Panel126
Accessory Ports127
Electrical Connectors And Controls On The Rear Panel128
Electrical Connectors And Switches On The Rear Panel129
The Gas And Cooling Connectors130
Gas And Cooling Connectors On The Rear Panel131
Technical Data132
Chapter 8 Translations Of Warnings135
Index187