Table 8-1: Activity Matrix For Epa Calibration Equipment And Supplies; Table 8-2: Activity Matrix For Calibration Procedure - Teledyne 200E Instruction Manual

EPA Protocol Calibration
Table 8-1:
Equipment/
Supplies
Recorder Compatible with output signal
of analyzer; min chart width of
150 mm (6 in) is recommended
Sample line Constructed of PTFE, glass or
and manifold stainless steel
Calibration Meets guidelines and Section
equipment 2.3.2 of Q. A. Handbook
Working Traceable to NIST-SRM. Meets
standard NO limits in traceability protocol for
cylinder gas accuracy and stability.
Section 2.0.7 of Q. A. Handbook
Recording Develop standard forms
forms
Audit Cannot be the same as used for
equipment calibration
Table 8-2:
Equipment/
Supplies
Calibration Sec. 2.0.7, Q.A. Handbook
gases
Dilution gas Zero air, free of contaminants;
2
TAD and Sec. 2.0.7, Subsec.
7.1, Q.A. Handbook
Multi-point t < 2 minutes P
R
calibration > 2.75 ppm/min
(GPT)
Use calibration procedure in Q.A
Handbook; also CFR
Converter efficiency > 96%
128
Activity Matrix for EPA Calibration Equipment and Supplies
Acceptance Limits
Activity Matrix for Calibration Procedure
Acceptance Limits
R
1
Model 200E Instruction Manual
Frequency And Method
Of Measurement
Check upon receipt
Check upon receipt
See Section 2.3.9 of Q.
A. Handbook
Analyzed against NIST-
SRM; see protocol in
Section 2.0.7, Q.A.
Handbook
N/A
System must be
checked out against
known standards
Frequency And Method
Of Measurement
Assayed against an
NIST-SRM quarterly,
Sec. 2.0.7
(Q.A. Handbook)
2
See TAD
Method: Section 7.2 of
this manual)
1
CFR Title 40 ,
Appendix F
Action If Requirements
Are Not Met
Return equipment to
supplier
Return equipment to
supplier
Return equipment/
supplies to supplier or
take corrective action
Obtain new working
standard and check for
traceability
Revise forms as
appropriate
Locate problem and
correct or return to
supplier
Action If Requirements
Are Not Met
Working gas standard is
unstable, and/or
measurement method is
out of control; take
corrective action such as
obtaining new calibration
gas
Return to supplier or take
appropriate action with
generation system
Adjust flow conditions
and/or reaction cell
volume to meet
suggested limits
Repeat the calibration
Replace or service the
converter
044100102 Rev A