Thermo Scientific ISQ 7000 Manuals

Thermo Scientific ISQ 7000 Manuals

Manuals and User Guides for Thermo Scientific ISQ 7000. We have 1 Thermo Scientific ISQ 7000 manual available for free PDF download: Hardware Manual

Thermo Scientific ISQ 7000 Hardware Manual

Thermo Scientific ISQ 7000 Hardware Manual (442 pages)

Mass Spectrometers

Brand: Thermo Scientific | Category: Measuring Instruments | Size: 21 MB

Table of Contents

Table of Contents
3
About Your System
13
Preface
13
Related Documentation
14
Safety and Special Notices
15
Special Notices
15
System Requirements
15
Safety Symbols and Signal Words
16
Hydrogen Safety Precautions
19
Hydrogen Connection Guidelines
21
Using Hydrogen with ISQ 7000 Mass Spectrometers
21
Properly Storing Hydrogen
23
Purchasing Hydrogen
23
Hydrogen Safety Codes, Standards and References
25
Hazardous Substances Precautions
26
Biological Hazard Warning Note
27
Contacting Us
27
Venting Toxic Gases
27
Chapter 1 Performing Routine Maintenance

29
- Maintenance Schedule
  31
- Maintenance Supplies and Tools
  32
- Configuring the ISQ 7000 Mass Spectrometer
  34
- Powering on the ISQ 7000 Mass Spectrometer
  37
- Powering off the ISQ 7000 Mass Spectrometer
  41
- Replacing a Column
  44
- Replacing a Column in a ISQ 7000 System with no VPI or an AEI Ion Source
  44
- Replacing a Column on a ISQ 7000 System with a VPI and an Extractabrite Ion Source
  55
- Installing the Column in the GC Inlet
  61
- Maintaining the Foreline Pump
  66
- Checking the Oil in the Foreline Pump
  68
- Adding Oil to the Foreline Pump
  68
- Purging Gas from the Oil in the Foreline Pump
  71
- Changing the Oil in a Foreline Pump
  71
- Cleaning the Ion Source Cartridge
  76
- Removing the Ion Source Cartridge
  76
- Removing the Advanced Ion Source Cartridge on a ISQ 7000 System
  92
- Cleaning the Ion Source Components
  95
- Replacing the Ion Source Components
  96
- Reassembling the Advanced EI Ion Source Cartridge
  110
- Maintaining the Calibration Gas Module
  116
- Refilling the Calibrant Reservoir
  117
- Replacing a Dual Filament
  119
- Replacing the Electron Multiplier
  127
- Cleaning Durable Components
  136
- Cleaning Delicate Components
  140
- Cleaning the Filters
  142
- Troubleshooting
  143
- Using Diagnostics
  144
- Running a Diagnostic Tune
  147
- Investigating Communication Issues
  150
- Software Is Not Communicating with the ISQ 7000 System
  150
- Cannot Download Methods to the ISQ 7000 System
  150
- GC Does Not Start or Is Not Ready
  150
- Sample Data Are Not Acquired
  152
- GC Is Not Communicating with the PC
  152
- Autosampler Is Not Communicating with the PC
  152
- Investigating Contamination Issues
  153
- Chemical Noise Is at M/Z 207, 429, 355, 281
  154
- Chemical Noise Is at M/Z 149, 167, 279
  154
- Chemical Noise Is at M/Z 43, 57, 71, 85, 99, Etc
  154
- Spectra Is Showing Solvent Contamination
  154
- Investigating Filament and Lens Control Issues
  156
- Filament Has Burned out
  156
- Filament Does Not Last Long
  156
- Diagnostics Indicate There Is a Problem with Lens Voltages
  156
- Investigating Temperature Issues
  158
- Lens/Source Heater will Not Heat
  159
- Lens/Source Heater Overheats
  159
- Transfer Line will Not Heat
  159
- Transfer Line Overheats
  160
- Investigating Vacuum Issues
  161
- An Air Leak Has Been Detected
  162
- Foreline Pump will Not Power-On
  162
- Foreline Pump Powers On, but the System will Not Pump down
  162
- Turbomolecular Pump will Not Power-On
  162
- Turbomolecular Pump Shuts off While in Use
  163
- Investigating Power Supply Issues
  164
- The ISQ 7000 Instrument will Not Power-On
  164
- Breaker
  164
- Q1 DC Supply Is Outside the Acceptable Range
  164
- Investigating RF/DC Issues
  165
- RF Dip Is Incorrect
  165
- RF/DC System Check Diagnostic Fails
  165
- Investigating Sensitivity Issues
  166
- Poor Sensitivity or Sudden Loss in Sensitivity
  167
- Poor High Mass Response
  167
- Poor Sensitivity in CI Mode
  167
- Investigating Stability Issues
  169
- Mass Assignment Is Unstable
  169
- Signal Response Is Unstable or Shows Unexpected Drop-Out
  169
- Investigating Tuning Issues
  170
- Tune Is Interrupted
  171
- Cannot Find Calibration Gas Peaks
  171
- Cannot Perform Detector Gain Calibration
  171
- Cannot Calibrate Resolution
  171
- Cannot Perform Mass Calibration
  172
- An Air Leak Has Been Detected
  172
- Contacting Technical Support
  173
- Advanced Maintenance
  175
- Replacing Components of the Analyzer
  176
- Analyzer Tray
  177
- Ion Guide
  195
- Ion Guide Clamp
  198
- Attach the Wire Connecting the Quadrupole Entrance Lens to the Source Interface Board by Screwing in the Terminal with a Slotted Screwdriver
  199
- Ion Guide Wire Set
  200
- Quadrupole
  201
- Quadrupole Wire Set
  203
- Once the Components Are Correctly Attached to the Analyzer Tray, Follow the Instructions in "Replacing the Analyzer Tray" on Page
  205
- Quadrupole Entrance Lens
  206
- Exit Endcap
  209
- Entrance Endcap
  210
- Replacing Components of the Ion Source
  213
- Ion Source Block
  214
- Source-Repeller Thumbscrews
  222
- Thumbscrew-Repeller Spacers
  224
- Insulating Spacers
  226
- Repeller Plate
  229
- Lens/Source Heater
  232
- Lens Heater Block
  234
- Lens Heater Block Grounding Strap
  238
- Lens Plate and Springs
  239
- Source to Ion Guide Spacer
  240
- Ion Source Cartridge
  244
- Replacing Components of the Source Exchange Tool
  246
- Replacing Components of the Vacuum Interlock
  250
- Shut down Your System by Following the Steps in on Page
  251
- Shutting down the ISQ 7000 System
  251
- On Page
  264
- Replacing Components of the Manifold
  265
- Manifold Door Hinge
  266
- Front Manifold Plate
  271
- Back Manifold Plate
  277
- Source Retainer Magnets, Magnet Yoke, Source Insertion Guide, Source Magnets and Front Manifold O-Ring
  280
- Vent Valve Knob and O-Ring
  282
- Delivery Tubes
  283
- Replacing Components of the Electron Multiplier
  285
- Electron Multiplier Plate
  286
- Large Feedthroughs
  291
- Anode Feedthrough
  293
- Upgrading the ISQ 7000 System Software
  297
- Updating the Firmware on the Instrument
  297
- Upgrading Software on the Computer
  298
- System Requirements
  299
- Installing the Software Set
  300
- Replacing the Covers of the ISQ 7000 Mass Spectrometer
  303
- Top Cover Panel
  304
- Left Side Panel
  305
- Right Side Panel
  306
- Top Manifold Cover
  308
- Replacing the Chassis Feet
  309
- Replacing Components of the Front Door
  311
- Front Door Hinges and Supports
  312
- Front Door Latch
  315
- Replacing the Boards in the ISQ 7000 Mass Spectrometer
  320
- RF Board and Rod Driver Board
  321
- RF Board/Rod Driver Board Kit
  326
- 4- Pin Feedthrough
  329
- Lens Driver Board
  335
- 20-Pin Feedthrough
  338
- PC Communication Board, Controller Interface Board, and Support
  346
- Bracket
  346
- Distribution Board
  351
- Source Interface Board and Heat Shield
  362
- Electrometer Board Cable
  364
- Electrometer Board and Shield
  371
- Replacing the Power Supplies
  374
- Power Supply System
  375
- Dynode and Multiplier Power Supply
  377
- Replacing the Calibration Gas Components
  381
- Calibration Gas Module
  382
- Calibrant Reservoir Kit
  391
- Gas Mixing Chamber
  392
- Transfer Line
  393
- Replacing Fans and Filters
  397
- Intake Filters and RF Shields
  398
- Chassis Cooling Fan
  399
Chapter 4 Upgrade Equipment

401
- Advanced EI Ion Source
  402
- Dust Filters
  408
- CI Reagent Gas Flow Module
  409
- CI Ion Volume
  416
- EI/CI Ion Volume
  417
- Ion Gauge
  418
- Convectron Gauge and Foreline Adapter with Hose
  422
- Turbomolecular Pumps
  424
- Installing a Standard Capacity Turbomolecular Pump
  424
- Installing an Extended Capacity Turbomolecular Pump
  429
- Probe Controllers
  434

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