Flow Cell Operation - Thermo Scientific Orion 2117HL User Manual

Calibration

Flow Cell Operation

Recommendations
Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide
The sample reservoir in the flow cell, as shown in Figure IV-1, has two
sample volumes: a normal operation volume of 20 mL and a highly
accurate and individually calibrated flow cell volume of approximately
95 mL. The lower volume results in fast system response while online, and
the higher volume ensures accuracy in calibration.
Figure IV-1
Calibration Level
Measure Level
When the Thermo Scientific Orion 2117HL chloride analyzer is first
commissioned, it is advisable to flush out the fluidics system overnight
prior to the initial calibration and use. The electronics need not be turned
on at this time. Refer to Chapter IV, Rinsing the Flow Cell.
• For accurate volume displacement install the chloride sensing
electrode, reference electrode and ATC probe in their respective flow
cell cap ports. Refer to Chapter II, Installation of a New Chloride
Electrode, Chapter II, Installation of the ATC probe and Chapter II,
Installation of a New Reference Electrode.
• Close the calibration port.
• When rinsing the flow cell before a standard calibration, be sure to
rinse off the inside of the reservoir lid with deionized water to prevent
buildup of chloride contamination along the lid.
• To ensure that the analyzer achieves stability and minimizes interference
during calibration, the operator should minimize activity on the system
during calibration.
Flow Cell Block
Calibration Port
IV-2