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Thermo Scientific 43iQTL Manuals
Manuals and User Guides for Thermo Scientific 43iQTL. We have
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Thermo Scientific 43iQTL manual available for free PDF download: Instruction Manual
Thermo Scientific 43iQTL Instruction Manual (290 pages)
Trace Level Sulfur Dioxide Analyzer
Brand:
Thermo Scientific
| Category:
Measuring Instruments
| Size: 19 MB
Table of Contents
Table of Contents
3
Chapter 1 Introduction
9
Iq Series Instrument Platform
10
Figure 1-1. 43Iqtl Front
10
43Iqtl Principle of Operation
11
Figure 1-2. 43Iqtl Flow Schematic
12
Figure 1-3. 43Iqtl Flow Schematic with Zero Span
12
Specifications
13
Table 1-1. 43Iqtl Specifications
13
Table 1-2. 43Iqtl Optional Permeation Oven Specifications
14
Dimensions
15
Figure 1-4. Bench Mount Assembly (Dimensions in Inches [MM])
15
Figure 1-5. Rack Mount Assembly (Dimensions in Inches [MM])
16
Figure 1-6. Rack Mount Requirements
17
Installation and Setup
19
Unpacking and Inspection
19
Cover Removing and Replacing
20
Figure 2-1. Removing the Cover
20
Mounting Options
21
Bench Mount
21
Figure 2-2. Installing Feet
21
Rack Mount
22
Figure 2-3. Removing the Front Panel
22
Figure 2-4. Installing Ears and Handles
23
Setup Procedure
24
Figure 2-5. 43Iqtl Rear Panel
25
Figure 2-6. Atmospheric Dump Bypass Plumbing
25
Startup
26
Figure 2-7. Front Panel and Touchscreen Display
26
Chapter 3 Operation
27
Instrument Display
27
Main Menus and Keypads
31
Numeric Keypad
32
Alphanumeric Keypad
33
Calibration
35
Calibrate Background
37
Calibrate Span Coefficient
38
Zero/Span Schedule
40
Advanced Calibration
42
Manual Calibration
43
Calibration History
48
Data
49
View Data Log (Last Hour)
50
View Data Log (Last 24 Hours)
51
View Data Log (User Defined Time)
52
Advanced Data Setup
54
Data Logging Setup
55
Select Data Logging Variables
56
Streaming Data Setup
57
Select Streaming Variables
58
Settings
59
Health Check
60
Status and Alarms
61
Valve and Pump Resets
72
Predictive Diagnostics
78
Maintenance
79
Preventive Maintenance
80
Change Part
82
Maintenance History
83
Service Tips
84
File Sharing and Support
85
Iq360
86
Measurement Settings
89
Averaging Time
91
Range Mode Selection
93
Range Setting
95
Gas Mode
96
Gas Units
97
Advanced Measurement Settings
98
Communications
104
Wired TCP/DHCP
106
Analog I/O
109
Digital I/O
110
Email Server (SMTP)
111
Bayern Hessen Settings
112
Ethernet Protocol Selection
113
Instrument Settings
114
Display Setup
115
Alarm Setpoints
116
Clock
119
Time Zone
123
Configuration
126
Security Access Levels
127
Change Security to View Only Access
129
Change Full Access Security Password
130
Change Instrument Password
132
Reset Instrument Password
134
USB Drive
135
Firmware Update Via USB Drive
136
Download Data to USB Drive
140
Change USB Password
143
Reset USB Password
145
User Contact Information
146
Update Bootloader
147
Chapter 4 Calibration
149
Equipment Required
149
Zero Air Generation
150
Commercial Heatless Air Dryers
150
Absorbing Column
150
SO 2 Concentration Standard
150
Calibration Gas Generation
150
Cylinder Gas Dilution
151
External Flow Meter(S) and Controller(S)
151
Figure 4-1. Cylinder Gas Dilution System
151
Commercial Precision Dilution Systems
152
Permeation Tube System
152
Commercial Permeation Systems
153
Figure 4-2. Permeation Tube System
153
Calibration
154
Calibration in Dual/Auto Range Mode
156
Zero and Span Check
158
Manual Calibration
159
Adjust Background
160
Adjust Span Coefficient
160
Zero/Span Schedule
162
Next Time
162
Period
162
Zero/Span/Purge Duration Minutes
162
Schedule Averaging Time
163
Background Calibration and Span Calibration
163
Zero/Span Ratio
163
References
163
Chapter 5 Maintenance
165
Safety Precautions
165
Fan Filter Inspection and Cleaning
165
Pump Rebuilding
166
Figure 5-1. Single Stage Pump
166
Figure 5-2. Pump Rebuilding
168
Leak Test
169
Lamp Voltage Check
170
Lamp Voltage Adjustment
170
Chapter 6 Troubleshooting
173
Safety Precautions
173
Troubleshooting Guide
173
Table 6-1. 43Iqtl Troubleshooting Guide
173
Chapter 7 Servicing
181
Safety Precautions
181
Figure 7-1. Properly Grounded Antistatic Wrist Strap
182
Firmware Updates
183
Replacement Parts List
183
Figure 7-2. 43Iqtl Component Layout Top View
184
Figure 7-3. 43Iqtl Component Layout Side View
184
Fuse Replacement
185
Figure 7-4. Replacing the Fuses
185
Filter Replacement
186
Figure 7-5. Start with Top Right Corner of Fan Cover
186
Figure 7-6. Removing the Fan Cover
186
Fan Replacement
187
Figure 7-7. Unplugging the Fan Cable
187
Figure 7-8. Replacing the Fan
188
Measurement Side Removal and Replacing
189
Figure 7-9. Unplugging the Fan Cable
189
Figure 7-10. Unplugging the DMC Cable
190
Figure 7-11. Unfasten Hardware Front for Measurement Side Removal
190
Figure 7-12. Unfasten Hardware Rear for Measurement Side Removal
191
LCD Module Replacement
192
Figure 7-13. Replacing the LCD Module
192
Figure 7-14. Remove Electrical Cables from LCD
193
I/O Replacement
194
Figure 7-15. I/O Replacement, Arm
194
Figure 7-16. I/O Replacement, Remove Board
194
Figure 7-17. I/O Replacement, Install
195
Figure 7-18. I/O Replacement, Close Arm Alignment
195
Peripherals Support Board and System Controller Board Replacement
196
Figure 7-19. Replacing the Peripherals Support Board
196
DMC Pressure and Flow Board
197
Figure 7-20. Flow Pressure Board, Disconnect DMC Cable
197
Figure 7-21. Flow Pressure Board, Screws
198
Pump Replacement
199
Figure 7-22. Remove Pump, Disconnect and Unfasten
200
Figure 7-23. Pump Removal, Keyway
201
Figure 7-24. Pump Replacing, Unfasten Screws
201
Capillary Cleaning And/Or Replacement
202
Figure 7-25. Remove Capillary, Disconnect and Unfasten
202
Figure 7-26. Capillary Plate, Keyway
203
Figure 7-27. Capillary and O-Ring Replace
203
Capillary O-Ring Replacement
204
Power Supply Replacement
204
Figure 7-28. Removing Power Supply
205
Figure 7-29. Replacing Power Supply
206
Step POL Board Replacement
207
Figure 7-30. Unplug and Unfasten Step POL Board
207
Figure 7-31. Clear Partition Keyway Step POL Board
208
Figure 7-32. Step POL Board 1 Switch Settings
209
Figure 7-33. Optional Step POL Board 2 Switch Settings
209
DMC Optical Bench Removal
210
Optical Bench Assembly Removal
210
Figure 7-34. Removing the DMC Optical Bench Removal from Instrument
211
Optical Bench Assembly Removal
212
Figure 7-35. Removing the Optical Bench Assembly
212
Photomultiplier Tube (PMT) Replacement
214
Figure 7-37. Removing the PMT Assembly
214
Figure 7-38. Removing the PMT Cover
215
Figure 7-39. Replacing the PMT
216
Flasher Pack Replacement
217
Figure 7-40. Removing and Replacing the Flasher Pack
217
Flasher Pack Lamp Replacement
218
Figure 7-41. Replacing the Flasher Pack Lamp
218
Kicker Assembly Replacement
221
Figure 7-44. Removing and Replacing the Kicker Assembly
221
Optional Manifold Replacement
222
Optional DMC Permeation Oven Solenoid Valve Replacement
224
Permeation Oven Replacement
226
Figure 7-51. Finger Push and Release Tubing
227
Permeation Oven Board Replacement
229
Figure 7-53. Replacing the Permeation Oven Board
229
Chapter 8 System Description
231
Optical Bench DMC
233
Flash Lamp Trigger Assembly
233
Flash Lamp
233
Flash Trigger Board
233
Flash Intensity Assembly
233
Photomultiplier Tube
233
Optical Bench DMC Board
233
Bench Heater
234
Permeation Oven (Optional)
234
Common Electronics
234
Figure 8-1. Common System Interconnect Diagram
235
Figure 8-2. 43Iqtl System Interconnect Diagram
236
Power Supply
237
Front Panel
237
I/O and Communication Components
237
System Controller Board
237
Backplane Board
237
Peripherals Support System
238
Fan
238
Step POL Board
238
Sample Pump
238
Solenoid Valve Panel
238
Flow/Pressure DMC
238
Firmware
238
Chapter 9 Optional Equipment
241
Connecting External Devices
241
Communication Board
241
Figure 9-1. I/O Expansion Replacement Boards
241
RS-232/RS-485 Port
242
RS-485 External Accessory Port
242
Figure 9-2. RS-232/RS-485 Port
242
Table 9-1. RS-232/RS-485 Port Terminal Assignment
242
Figure 9-3. RS-485 External Accessory Port
243
Table 9-2. RS-485 External Accessory Port Terminal Assignment
243
Analog I/O Board
244
Analog Voltage Inputs
244
Figure 9-4. Analog Voltage Inputs
244
Table 9-3. Analog Voltage Inputs Assignment
244
Analog Voltage Outputs
245
Figure 9-5. Analog Voltage and Current
245
Analog Output Calibration
246
Table 9-4. Analog Voltage and Current Assignment
246
Analog Output Zero Calibration
247
Analog Output Full Scale Calibration
249
Digital I/O Board
251
Digital Inputs
251
Digital Relay Switches
251
Valve Driver Outputs
251
Figure 9-6. Digital Inputs
251
Table 9-5. Digital Inputs Terminal Assignment
252
Figure 9-7. Digital Relay Switches
253
Table 9-6. Digital Relay Switch Assignment
254
Figure 9-8. Valve Driver Outputs
255
Table 9-7. Valve Driver Outputs Assignment
256
Internal Zero/Span and Sample Valves
257
Internal Permeation Span Source
258
Figure 9-9. Internal Permeation Span Source Flow Diagram
258
Permeation Tube Installation
259
Figure 9-10. Installing Glass Tube Pt 1
259
Computation of Concentrations
262
PTFE Particulate Filter
263
Appendix A Safety, Warranty, and WEEE
265
Safety
265
Safety and Equipment Damage Alerts
265
Warranty
266
WEEE Compliance
268
WEEE Symbol
268
Appendix B Quick Reference
269
List of Figures
269
GNU Lesser General Public License
273
Appendix D Standards for Trace Level Analyzers
285
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