Thermo Scientific Orion 2117HL User Manual
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Thermo Scientific Orion 2117HL User Manual

High level chloride analyzer
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Thermo Scientific
Orion 2117HL
High Level
Chloride Analyzer
User Guide

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Summary of Contents for Thermo Scientific Orion 2117HL

  • Page 1 Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide...
  • Page 2 ROSS and the COIL trade dress are trademarks of Thermo Fisher Scientific Inc. U.S. patent 6,793,787. AQUAfast, Cahn, ionplus, KNIpHE, No Cal, ORION, perpHect, PerpHecT, PerpHecTion, pHISA, pHuture, Pure Water, Sage, Sensing the Future, SensorLink, ROSS, ROSS Ultra, Sure-Flow, Titrator PLUS and TURBO2 are registered trademarks of Thermo Fisher. 1-888-pHAX-ION, A+, All in One, Aplus, AQUAsnap, AssuredAccuracy, AUTO-BAR, AUTO-CAL, AUTO DISPENSER, Auto-ID, AUTO-LOG, AUTO-READ, AUTO-STIR, Auto-Test, BOD AutoEZ, Cable-Free, CERTI-CAL, CISA, DataCOLLECT, DataPLUS, digital LogR, DirectCal, DuraProbe, Environmental Product Authority, Extra Easy/Extra Value, FAST QC, GAP, GLPcal, GLPcheck, GLPdoc, ISEasy, KAP, LabConnect, LogR, Low Maintenance Triode, Minimum Stir...

  • Page 3: Table Of Contents

    Shutdown .and .Start-Up .Procedure . . . . . . . . . . . . . . . . . . . . . . . . . . . III-35 Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide...
  • Page 4 Pipet . T echniques . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .A-12 Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide...

  • Page 5: Chapter I

    General Information Chapter I This user guide covers the operation, maintenance and troubleshooting for the Thermo Scientific Orion 2117HL high level chloride analyzer, which offers unmatched reliability in analyzing chloride from industrial water and agricultural water applications. Introduction Monitoring the chloride ion content to prevent boiler corrosion or to control chloride levels in RO effluent water applications requires a well designed and maintained system.

  • Page 6: Features And Benefits

    General Information Features and Benefits The Thermo Scientific Orion 2117HL chloride analyzer is ideal for measuring and monitoring the critical chloride levels in industrial water or agricultural water applications. With limited maintenance requirements and no reagent, the 2117HL analyzer can also be used in remote monitoring applications.

  • Page 7: Principles Of Operation

    General Information Principles of Operation The sample enters the Thermo Scientific Orion 2117HL chloride analyzer and passes through the inlet valve, bypass/needle valve, inlet filter, pressure regulator, flow meter and into the restrictor tubing. The sample then passes through the flow cell manifold into the flow cell as air is introduced from the air pump to ensure proper mixing and fast response.
  • Page 8 Therefore, the analyzer is calibrated to determine its actual value. Two standards are used to provide information necessary for the microprocessor to compute the actual slope and E for use during sample analysis. Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide...

  • Page 9: Principles Of Calibration

    Calibration be performed carefully. The calibration procedure used in the Thermo Scientific Orion 2117HL analyzer is a variation of Double Known Addition (DKA) using advanced electrode and flow cell technology. This method has the distinct advantages of being fast, easy and accurate.

  • Page 10: Offline Calibration

    The term “offline calibration” refers only to the fact that a sample from 2117HL analyzer bypass is taken “offline” for laboratory analysis; in fact, no downtime is experienced during the procedure and the analyzer remains online throughout. Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide...

  • Page 11: Fluidics Diagram

    Tube Assembly Flow Meter Calibration Port Flow Cell Reservoir Siphon Tube Pressure Flow Cell Block Regulator Reagent Manifold Diverter Valve Bypass/Needle Valve Inlet Filter Inlet Valve Figure I-3 Fluidics Diagram Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide...

  • Page 12: Glossary

    Calibration Port – Allows introduction of standards to the sample reservoir during calibration. Air Pump – Used to mix the sample during both measurement and calibration as well as provide air to pressurize the reference electrode filling solution bottle. Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide...

  • Page 13: Two Channel Analyzer Configurations

    A pH/ORP module or conductivity module can be added by the operator Configurations to the second channel of the Thermo Scientific Orion 2117HL chloride analyzer for the ultimate flexibility in measurement capabilities. The 2100 series pH/ORP and conductivity analyzers provide accurate and reliable measurements in ultra pure water as well as the harshest industrial environments.

  • Page 14: Analyzer Preparation

    9/16 wrench. These bolts may be discarded. 6. Carefully place the analyzer at a convenient location until proper installation can be completed. Figure II-1 Unpacking the Analyzer Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide II-1...

  • Page 15: Mounting And Plumbing Instructions

    3. Connect a sample line to the inlet of the analyzer, which is 1⁄4 NPT female. It is recommended that a shutoff valve be installed at the sampling point. 4. The analyzer must be mounted and leveled vertically for proper operation. Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide II-2...

  • Page 16: Sample Requirements

    Sample alkalinity – Sample alkalinity should be less than 50 ppm CaCO equivalent. For higher sample alkalinity, contact Technical Support. Sulfite – Sulfite cannot be present in the sample. Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide II-3...

  • Page 17: Electrical Wiring

    Installation and wiring of the analyzer may only be carried out in accordance with applicable local and national codes per this user guide. • Be sure to observe the technical specifications and input ratings. Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide II-4...

  • Page 18: Warning Labels And Locations

    Fuse Holder Power Supply Fuse Type Ground Fuse 115V 250V, 200mA Fast Acting 230V 250V, 100mA Fast Acting Note: Replace the fuse only with a fuse of same rating. Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide II-5...

  • Page 19: Wiring The Analyzer

    Figure II-4. 3. Select and install the appropriate size cable gland or conduit fitting as required. 4. Feed the power cable through the conduit or cable glands as required. Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide II-6...
  • Page 20 Refer to Figure II-3. Refer to the table below for fuse selection. AC Voltage Fuse Rating 115V 200mA, 250V, Fast Acting 230V 100mA, 250V Fast Acting Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide II-7...

  • Page 21: Terminal Assignments

    20 Conductivity drive + 21 Conductivity sense + 22 Conductivity sense - 23 Conductivity drive - 24 Reference electrode 25 Jumper to pin 24 when using preamp Figure II-6 Terminal Assignments Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide II-8...

  • Page 22: Electrode Wiring Assignments

    Connect red wire Conductivity sense - Connect green wire Conductivity drive - Connect blue wire Note: Only reference the wiring configurations that are applicable to your analyzer and electrodes. Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide II-9...

  • Page 23: Installation Of New Electrode Cables

    3. Place the ferrite at the bottom of the analyzer chassis, near its edge. Adjust the ferrite location on the cable so the ferrite is near the top of the cable. Figure II-7 Ferrite Installation Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide II-10...

  • Page 24: Installation Of A New Chloride Electrode

    Installation of a New The Thermo Scientific Orion chloride electrode (Cat. No. 210017) Chloride Electrode must be used in conjunction with the Thermo Scientific Orion reference electrode (Cat. No. 100057). 1. Unpack the chloride electrode (Cat. No. 210017) and carefully remove the protective cap.

  • Page 25: Installation Of A New Reference Electrode

    The electrode should be horizontal with the sidearm pointing up. Gently shake the electrode to allow any trapped air bubbles to rise into the bottle as the electrode fills with solution. Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide II-12...
  • Page 26 11. Insert the reference electrode into its port in the flow cell cap. Refer Figure II-8 for the location. Insert the hollow push pin on the discharge tube of Figure II-10 the air pump here Reference Mounting Clip Clip (on Panel) Bottle Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide II-13...

  • Page 27: Analyzer Operation

    At initial installation, the red LED Indicator indicates that the electrode or probe Orange LED indicates a channel warning needs to be installed and calibrated. Red LED indicates a channel failure Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide III-1...

  • Page 28: Description Of Keypad Icons

    Use in setup and test modes to return to the previous screen or menu Decimal point function Use to set the decimal point position in certain menus with numbers that require a decimal point Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide III-2...

  • Page 29: Use Of The Setup Mode

    If a two channel analyzer is in use, make sure to program both the channel 1 and channel 2 menu options in the setup mode. Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide III-3...
  • Page 30 If password(s) are de-activated: • System enters the setup mode at the last setup menu option used by the operator. • Marquee: Flashes current menu option • Main display: SEL SCrn Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide III-4...

  • Page 31: Setup Mode Overview

    Set the log interval as hour:minute • Default log interval is 00:00 – logging disabled • Minimum log interval is 1 minute, maximum log interval is 99 hours and 59 minutes Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide III-5...
  • Page 32 AUtO – Brightness will change in response to ambient light source • On – Backlit display is always on • OFF – Backlit display is always off • Default display – AUtO Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide III-6...
  • Page 33 • Default hold time – 30 minutes TADJ Adjust the temperature reading from the ATC probe by ± 5.0 °C: • Default adjustment – 0.0 degrees C Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide III-7...
  • Page 34 (tOUt) outputs: • Select the sensor (SOUt) or temperature (tOUt) output • Scroll the numeric offset value and positive or negative offset value • Default mA offset – 00.0 mA Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide III-8...
  • Page 35 DKA setup menu and during a DKA calibration. ** The standard 2 volume addition is made by adding three increments of standard 2 to the flow cell using the 0.5 mL pipet. Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide III-9...
  • Page 36 HOLD TADJ ALRM mAMP mADJ TEST Press to loop through the menu options Press to select the desired menu option and enter the submenu to customize setup parameters Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide III-10...
  • Page 37 TEST SEL CH2 SEL CH2 SEL CH2 Press to loop through the menu options Press to select the desired menu option and enter the submenu to customize setup parameters Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide III-11...
  • Page 38 Press to accept the calibration password and return to the main setup mode PASS (flashing) SCrn Press to scroll to the next menu Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide III-12...
  • Page 39 (change flashing digit) move through the remaining digits Press to accept the date setting and return to the main setup mode DATE (flashing) SCrn Press to scroll to the next menu Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide III-13...
  • Page 40 Press to accept the time setting and return to the main setup mode TIME (flashing) SCrn Press to scroll to the next menu Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide III-14...
  • Page 41 99 hours and 59 minutes Press to accept the log setting and return to the main setup mode (flashing) SCrn Press to scroll to the next menu Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide III-15...
  • Page 42 TO RESET setup mode RSET (flashing) SCrn Press to scroll to the next menu Warning: Resetting the analyzer will erase all stored information including relay, logs and calibration settings. Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide III-16...
  • Page 43 AUtO, OFF and On settings (flashing) Press to accept the display setting and return to the main setup mode DISP (flashing) SCrn Press to scroll to the next menu Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide III-17...
  • Page 44 Thermo Scientific Orion 2100 Series pH/ORP Analyzer and Conductivity Analyzer User Guide for detailed instructions on the menu option displays) (flashing) SCrn Press to scroll to the next menu Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide III-18...
  • Page 45 MEAS SEL CH1 or SEL CH2 on main display of (flashing) SCrn two channel analyzer Press to scroll to the next menu Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide III-19...
  • Page 46 HOLD TO 22mA WHEN ERROR (flashing) HOLD TO 22mA WHEN ERROR OFF or On Press to scroll between (flashing) OFF and On Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide III-20...
  • Page 47 HOLD SEL CH1 or SEL CH2 on main display of (flashing) SCrn two channel analyzer Press to scroll to the next menu Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide III-21...
  • Page 48 TADJ SEL CH1 or SEL CH2 on main display of (flashing) SCrn two channel analyzer Press to scroll to the next menu Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide III-22...
  • Page 49 SELECT ALARM 2 HIGH rLY2 Press to scroll through OFF, LOW OR OFF OFF, HI or LO HI and LO (flashing) Press to accept the setting and advance to the next screen Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide III-23...
  • Page 50 ALRM SEL CH1 or SEL CH2 on main (flashing) SCrn display of two channel analyzer Press to scroll to the next menu Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide III-24...
  • Page 51 Press to set the values of the remaining digits and press move through the remaining digits Press to accept the setting and advance to the next screen Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide III-25...
  • Page 52 SEL CH1 or SEL CH2 on main (flashing) SCrn display of two channel analyzer Press to scroll to the next menu Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide III-26...
  • Page 53 SELECT TEMP OR SENSOR SOUt or tOUt OUTPUT (flashing) SELECT TEMP OR SENSOR tOUt Press to scroll between OUTPUT (flashing) SOUt or tOUt and select tOUt Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide III-27...
  • Page 54 SEL CH1 or SEL CH2 on main (flashing) SCrn display of two channel analyzer Press to scroll to the next menu Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide III-28...
  • Page 55 TEST SEL CH1 or SEL CH2 on main display of (flashing) SCrn two channel analyzer Press to test the mA outputs (4-20) and relays (rLY) Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide III-29...
  • Page 56 TEST SEL CH1 or SEL CH2 on main display of (flashing) SCrn two channel analyzer Press to test the mA outputs (4-20) and relays (rLY) Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide III-30...
  • Page 57 TEST SEL CH1 or SEL CH2 on main display of (flashing) SCrn two channel analyzer Press to scroll to the next menu Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide III-31...
  • Page 58 SEL CH1 or SEL CH2 on main display of (flashing) SCrn two channel analyzer Press to scroll to the next menu Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide III-32...
  • Page 59 (change flashing digit) Press to set the values of the remaining digits and press move through the remaining digits Press to accept the setting and advance to the next screen Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide III-33...
  • Page 60 SEL CH1 or SEL CH2 on main display of (flashing) SCrn two channel analyzer Press to scroll to the next menu Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide III-34...

  • Page 61: Shutdown And Start-Up Procedure

    5. Locate the protective cap from reference electrode kit and place it on the base of the reference electrode to prevent it from drying out. Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide III-35...
  • Page 62 3. Allow the analyzer to stabilize for approximately 1 hour and then recalibrate the system. Refer to Chapter IV, Performing a DKA Calibration. Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide III-36...

  • Page 63: Calibration

    (parts per hundred) in the DKA setup menu and during a DKA calibration. The standard 2 volume addition is made by adding three increments of standard 2 to the flow cell using the 0.5 mL pipet. Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide IV-1...

  • Page 64: Flow Cell Operation

    Measure Level Flow Cell Block Recommendations When the Thermo Scientific Orion 2117HL chloride analyzer is first commissioned, it is advisable to flush out the fluidics system overnight prior to the initial calibration and use. The electronics need not be turned on at this time.

  • Page 65: Rinsing The Flow Cell

    5. Flush the flow cell for 10 to 60 minutes. The sample will drain from the siphon tube into the siphon drain to the waste. 6. Begin a DKA calibration. Refer to Chapter IV, Before Performing a DKA Calibration. Figure IV-2 Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide IV-3...

  • Page 66: Air Regulation

    Air Regulation The Thermo Scientific Orion 2117HL chloride analyzer utilizes pressure, gravity and fluid dynamics as the principal force of operation for the fluidic system. Figure IV-3 Air Pump Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide IV-4...

  • Page 67: Before Performing A Dka Calibration

    Figure IV-4 on the inside of the wall, resulting in errors in precision of calibration. Pipet Dispensing Refer to Figure IV-4. Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide IV-5...

  • Page 68: Performing A Dka Calibration

    Check that the calibration port on the flow CHECK CAL PORT CLOSED FILL cell cap is closed. PUSH DIVERTER VALVE IN FCEL PRESS ENTER Push the diverter valve in. Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide IV-6...
  • Page 69 ADD STD1 Add Std1 Press PRESS ENTER Wait 2 minutes. MEASURING STD1 Actual readings System circulates flashing sample. Minutes will CIRCULATING be counted down on WAIT 2 MINUTES the marquee. Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide IV-7...
  • Page 70 No action necessary. System calculates new Eo and slope and checks for errors. If there is a calibration error, the appropriate error message will be displayed. Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide IV-8...
  • Page 71 System will proceed to measure mode. Actual temperature reading Actual concentration System enters reading measure mode, but will remain on hold until the hold timer expires. Default hold time is 30 minutes. Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide IV-9...

  • Page 72: Calibration Abort Steps

    No operator action needed. Actual temperature reading Actual concentration reading The system will enter the measure mode and remain on hold until the hold timer expires (default hold time is 30 minutes). Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide IV-10...

  • Page 73: Calibration Error Codes

    Perform electrode Press to abort the calibration and cleaning and conditioning, refer to refer to Exit 3. the troubleshooting section and repeat the calibration. Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide IV-11...
  • Page 74 Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide IV-12...

  • Page 75: Calibration .At .Custom .Concentrations .Using .Dka

    For Maximum Accuracy • should be at least twice the normal concentration in the sample • should be about ten times of dC • should not be less than 10 ppb Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide IV-13...

  • Page 76: Span Check Procedure

    Calibration Span Check The Thermo Scientific Orion 2117HL chloride analyzer remains in sample Procedure mode during the entire procedure. 1. Fill flow cell to calibration level (V , approximately 95 mL). 2. Record the concentration displayed when the reading is reasonably stable (C 3.

  • Page 77: Offline Calibration Procedure

    Take a QC sample from the 2117HL TAKE SAMPLE FROM BYPASS DRAIN analyzer bypass for laboratory analysis. PRESS ENTER TO USE METER THEN PRESS CAL TO ENTER LAB Press RESULTS Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide IV-15...
  • Page 78 PRESS ENTER TO ACCEPT OR recalculated the E PRESS EXIT TO ABORT The system will return Press to the measure mode. Only MEASURE should appear as mode. Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide IV-16...

  • Page 79: Analyzer Maintenance

    Analyzer Maintenance Chapter V Maintenance Schedule The Thermo Scientific Orion 2117HL chloride analyzer is designed for simple maintenance. Follow the instructions in this section to ensure proper operation of your analyzer. Recommendations To ensure proper maintenance and good analyzer performance, a service logbook should be kept.

  • Page 80: Monthly Maintenance

    Push the pin down until its PVC base abuts the bottle. Mark and date the level of filling solution in the reservoir. The electrolyte solution will begin to flow into the reference electrode. Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide...
  • Page 81 8. Retighten the hex cap to approximately 75 pound-inch in torque. 9. Turn on the sample flow by turning the inlet valve left. 10. Check for leaks. Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide...

  • Page 82: Yearly .Preventative .Maintenance

    2. Remove the three O-rings from the face of the flow cell manifold. retaining ring 3. Insert the new O-rings on the face of the flow cell manifold. 4. Replace the flow cell manifold assembly. valve stem Figure V-1 Flow Cell Assembly Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide...
  • Page 83 8. Open the inlet valve to start sample flow through the analyzer. restrictor tube assembly Figure V-2 Restrictor Tubing restrictor adapter fitting clamp flow O-ring meter to check valve on flow cell manifold Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide...

  • Page 84: Troubleshooting

    CH1 mA OUTPUT VALUES SENSOR/TEMP CH2 mA OUTPUT VALUES SENSOR/TEMP PRESS ENTER FOR THE DISPLAY TEST PRESS ENTER TO CONTINUE PRESS ENTER TO CONTINUE KEYPAD TEST PRESS ALL KEYS ONE AT A TIME Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide VI-1...
  • Page 85 # # . # c (Temperature) Press Press to display the calibration to scroll temperature and electrode response through the last 12 calibrations Press to proceed to the next menu Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide VI-2...
  • Page 86 Actual description of error code E### Press to scroll through the # - # error list Press to proceed to the next menu Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide VI-3...
  • Page 87 Actual temperature value for logged Concentration and Press to scroll between the measurement mV values for logged measurement log and the data and measurement time display Press to proceed to the next menu Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide VI-4...
  • Page 88 Press to proceed to the next menu Software Revision SOFTWARE REV NUMBER r # . # # r # . # # Press to proceed to the next menu Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide VI-5...
  • Page 89 Output Values mA OUTPUT VALUES SENSOR/ TEMP Current mA output values for sensor and temperature Press to proceed to the next menu Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide VI-6...
  • Page 90 Verify that all of the numeric display PRESS ENTER TO CONTINUE Count pattern segments are functional Count pattern Press to proceed to the next menu Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide VI-7...
  • Page 91 10 seconds No operator action needed The system will enter the measure mode if the keypad test is passed Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide VI-8...

  • Page 92: Slope Problems

    -1001.5 mV to – 998.5 mV + 1000 mV + 998.5 mV to + 1001.5 mV • Background concentration too high for the standards used. • Standards contaminated or incorrectly made – verify calibration with fresh standards. • Standard 1 and standard 2 interchanged – check the volume of the standard added during calibration (add 0.5 mL for standard 1 and add 1.5 mL for standard 2) and repeat the calibration. If using custom standards, verify the values for each standard. • Standard 1 and standard 2 added in wrong sequence – check the sequence of the standards and repeat the calibration. Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide VI-9...
  • Page 93 • Electronics failure – reset the analyzer. Refer to Chapter VI, Resetting the Analyzer. • Improper pipet technique – refer to the Appendix, Pipet Operation and Technique section. • Background concentration too high for the standards used. • Cables interchanged – verify wiring of cable connections to terminal strip. Refer to Chapter II, Wiring the Analyzer. • Check the connection of the cable markers for the corresponding electrode. Cable markers are the white tape at the cap connector on the cable. • “Ref ” for the reference electrode • “Sensing” for the chloride electrode • Sensing electrode coated – clean or replace the sensing electrode. Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide VI-10...

  • Page 94: Troubleshooting .Matrix

    Refer to Chapter II. Inlet filter clogged Replace or clean the filter. Restrictor tubing crimped Replace the restrictor tubing. Refer to or clogged Chapter II. Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide VI-11...
  • Page 95 Inlet filter just replaced Flush the analyzer for one hour. Refer to Chapter IV. If an offline calibration was performed, verify accuracy of alternate method value. Refer to Chapter IV. Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide VI-12...
  • Page 96 Electronics failure Try resetting the analyzer. Refer to Chapter VI or consult Technical Support. Default Battery failure Consult Technical Support. Reset the analyzer. Refer to Chapter VI. Electronics failure Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide VI-13...

  • Page 97: Error/Event Codes

    INVALID SLOPE Invalid slope obtained during calibration Check electrodes, electrode cables and connectors for defects or shorts. Replace electrodes, if necessary. Recalibrate using new standards in the correct calibration sequence. Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide VI-14...
  • Page 98 2 E134 CH2 TOUT mA UNDER RANGE Measured temperature value below Tout Verify user selectable Tout low limit value in setup mode low limit value on channel 2 Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide VI-15...
  • Page 99 Replace electrode, if needed. E126 CH2 BAD OFFSET Last calibration produced a bad Eo offset Recalibrate the analyzer using fresh standards. Check electrode on channel 2 connections. Replace electrode, if needed. Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide VI-16...

  • Page 100: Resetting The Analyzer

    The operator will need set the analyzer to original to re-enter the setup mode to factory setup continue programming the setup values. parameters. Press to return to the setup mode. Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide VI-17...

  • Page 101: Serial Number And Software Revision

    Hard Reset A hard reset should be performed if the analyzer becomes unresponsive or the status indicators are flashing. Perform the following sequence: • Carefully open the front cover of the electronics case (loosen the four corner screws). • Press the small button located on the raised portion of the PCB to reset the electronics. • Close the front cover of the electronics case and tighten the screws. System settings and calibrations are preserved and analyzer returns to the measure mode. The actual value for concentration and temperature will be displayed if the electrodes are properly installed. If the system does not reset, contact Technical Support at 1-800-225-1480 for assistance. Serial Number and In the event you require technical assistance, please have the serial number Software Revision available when calling for assistance along with the software version. • The analyzer serial number is located on the underside of the electronics enclosure or if panel mounted then on the backside of the electronics enclosure. • The software revision is accessed through the diagnostics mode. Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide VI-18...

  • Page 102: Service And Repair

    Service Kit to Expand With in-house resources at a premium, many organizations require Standard Warranty immediate access to manufacturer expertise. Purchase a service kit within ninety days of the initial product purchase date to eliminate the costly effects of down time. • Provides a contracted, cost-effective means to enhance level of support offered during the product warranty period. • Provides priority access to the manufacturer’s technical experts at Thermo Scientific Orion Support Call Center. • Provides a service kit to expedite on-site repairs in conjunction with telephone consultation with Thermo Scientific Orion product experts. The service kit includes: • Power supply • Front panel display • Air pump • Electrode cables Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide VI-19...
  • Page 103 Remedial Service This is a one-day service engineer on-site visit to your facility for remedial service events at standard response time. Consider this plan an excellent uplift to one of the aforementioned programs. Preventive Maintenance All precision-made scientific equipment requires preventive maintenance Programs and calibration checks to perform at their maximum effectiveness. Consider a fixed-fee preventive maintenance contract to have one of our experts perform the following tasks: • Sampling check • Full validation test • Visual check for worn, loose or damaged parts • Replacement of consumables (additional charge for consumables) • Diagnostic check to verify all operating parameters are within the factory specifications • Check analyzer electrodes, flows and pressures • Clean and replace any wearable items Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide VI-20...

  • Page 104: Customer Service

    Further information on compliance with these directives, the recyclers in your country, and information on Thermo Scientific Orion products that may assist the detection of substances subject to the RoHS Directive are available at www.thermo.

  • Page 105: Declaration Of Conformity

    ISO 9001:2008 by QMI, listed as File #001911. Patrick Chiu Place and Date of Issue: Senior Quality Engineer, Beverly, MA Regulatory Compliance July 30, 2009 Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide VII-2...

  • Page 106: Terms And Conditions

    Returning Goods Permission to return Thermo Scientific Orion products must be obtained prior to return. Contact us within 30 days of receipt of goods for a return authorization number. Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide VII-3...
  • Page 107 Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide VII-4...
  • Page 108 Customer Service Warranty Thermo Scientific Orion process products are warranted to be free from defects in material and workmanship for a period of 12 months from date of installation or 18 months from date of shipment, whichever is earlier, when used under normal operating conditions and in accordance...

  • Page 109: Appendix

    Appendix Mounting Dimensions 26” 17” 8.5” Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide...

  • Page 110: Ise Default Values

    Volume of standard 1 added during calibration = 0.50 mL Concentration of standard 2 added during calibration = 2.96 % Volume of standard 2 added during calibration = 1.50 mL Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide...

  • Page 111: Specifications

    Temperature Measurement Range -10 to 120 °C Resolution 0.1 °C Relative Accuracy ± 0.5 °C Failure Detection Manual compensation ATC Probe 30 K thermistor LED Status Indicator Green Yellow Warning Failure Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide...
  • Page 112 Offline Calibration Offline Calibration Points 1 point Pre-programmed Standard Values Custom Calibration Programmable for concentration and volume Operator Input DKA, operator programmable, offline Inputs (Potentiometric) Ion Input Chloride Reference Input Reference Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide...
  • Page 113 Software Features Self-test and Diagnostics Real Time Clock Password Protection Reset Function Programmable Alarms High, low, error, calibration/offline Measurement, Active Signal noise, temperature Calibration Sensor response, drift, E , slope, temperature Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide...
  • Page 114 Altitude Sea level to 2000 M Shock and Vibration Vibration, Shipping/Handling 0 to 60 Hz @ 1 G Load Shock, Drop Test in Packaging 36” on all sides and corners Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide...

  • Page 115: Ordering Information

    Automatic temperature compensation (ATC) probe with ground (30 kΩ) 2001XT Automatic temperature compensation (ATC) probe with ground (30 kΩ) and 10 meter extension cable 21003M (2) x 3 meter extension cables for 210017 and 100057 electrodes Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide...
  • Page 116 2120XP and 2120XPEN analyzers 21GRBT Replacement bottle for 2100 series grab sampler 21GRPA Air pump replacement kit for 2100 series grab sampler 21GRFK Fittings kit for 2100 series grab sampler Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide...
  • Page 117 (2100PA), (1) regulator assembly (2100RG), (2) electrode cable with gland assemblies for sensing and reference electrodes, (1) power supply assembly (2100PS) and (1) fuse kit assembly (2100FK115 and 2100FK230) Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide...

  • Page 118: Recommended .Consumables .For .Annual .Operation

    Calibration Kit – includes carrying case, 0.5 mL pipet (204847-001), box of pipet tips (204846-001), wash bottle, (5) x 2 oz bottle of 29,600 ppm high level chloride standard (211740HL) Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide A-10...

  • Page 119: Pipet Operation

    Press the shelf hanger firmly into place on a shelf, counter top or pipet stand. To use, hang the grippy finger rest on the shelf hanger. Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide A-11...

  • Page 120: Pipet Techniques

    This action will empty the tip. 4. Release the push button to the ready position. If necessary, change the tip and continue pipeting. Thermo Scientific Orion 2117HL High Level Chloride Analyzer User Guide A-12...
  • Page 122 Process Water Instruments North America 9 0 0 1 : 2 0 0 8 166 Cummings Center Beverly, MA 01915 USA Toll Free: 1-800-225-1480 Tel: 1-978-232-6000 Dom. Fax: 1-978-232-6015 Int’l Fax: 978-232-6031 Europe P.O. Box 254, 3860 AG Nijkerk Wallerstraat 125K, 3862 CN Nijkerk, Netherlands Tel: (31) 033-2463887 Fax: (31) 033-2460832...

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