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Summary of Contents for Thermo Scientific 2210AM
- Page 1 Thermo Scientific Orion 2210AM Ammonia Analyzer UM-271914-001 December 2017 • Revision C •...
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Page 3: Table Of Contents
Contents General Information ..........1 Safety Precautions..........1 Symbols Used in this Manual ......1 Specifications ............. 2 Introduction............. 4 Unpacking the Instrument ........4 General Product Description ......5 Analysis Reaction Principle ........ 7 Installation Environmental Considerations ..... 9 Mounting the Instrument ........ - Page 4 Analyzer Hardware Configuration and Calibration............. 19 Optics Calibration ..........19 Optics Calibration Steps........19 Reaction Cell Temperature Calibration..... 19 Pumps Calibration ..........20 Pumps Calibration Method....... 20 Analog Outputs Calibration ......20 Calibration of the Instrument for Measurement Analysis..............21 Theory of Calibration ........
- Page 5 Warranty Shipments/ Returns/Adjustments ..49 Consumables............ 50 Assistance ............50 Addendum ............51 Analyzer Alarms, Faults and status ....51 2210AM Analyzer Interface to a Sample Conditioner ............52 2210AM Analyzer ONLY ........54 2210AM Measurement ranges ......54 Sample Analysis Data storage......55...
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Page 6: General Information
General Information Safety Precautions EARTH (Ground): This symbol, when noted on the product, identifies the The Thermo Scientific™ Orion™ 2210AM Ammonia Analyzer location of the connection for Protective has been designed with careful attention to safety. It complies Earth (ground). -
Page 7: Specifications
100-240 V AC, 110 W, 50/60 Hz Connections Requirements 3/8 inch OD flexible tubing – Two 0/4-20 mA – Direct or Reverse Drain Tubing Polypropylene or similar material Current Loops Acting (Isolated). Maximum 900 ohm load. Sample Streams General Information Orion 2210AM Ammonia Analyzer... - Page 8 Electrical Data and Control Four SPDT, 2 A @250 V – Relays Programmable RS232 ASCII protocol for data Digital Comms reporting Certifications Safety CE: EN/IEC61010-1, cTUVus CE: EN61326-1 Class A Warranty Warranty 1 Year Orion 2210AM Ammonia Analyzer General Information...
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Page 9: Introduction
This section describes the necessary steps to begin using the across many industries. Orion 2210AM Ammonia Analyzer. Refer to The Orion 2210AM Ammonia Analyzer uses the colorimetric Installation Environmental Considerations for instructions on detection method that relies on specific reagents that are mounting the analyzer, making the plumbing connections, added to the sample to produce a reacted color compound. -
Page 10: General Product Description
Select Services. This user manual provides the information necessary to obtain c. Select Prime Fluidics. the maximum benefits from the Orion 2210AM Ammonia d. Select Prime All. Analyzer. All operating instructions, functional descriptions, Note: This procedure will run automatically and illustrations, and other relevant information are contained in take approximately 10 minutes per cycle. - Page 11 9. STATUS field shows current working status of the instrument. 10. FUNCTIONAL KEYS ASSIGNMENT FIELD shows the functions allotted to the functional keys. 11. FUNCTION KEYS select functions. 12. OPERATIONAL KEYS are meant for operation of the instrument. Introduction Orion 2210AM Ammonia Analyzer...
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Page 12: Analysis Reaction Principle
Fluids Storage Store all reagents and standards in a dark place at room temperature. Calibration Standard Figure 2. Orion 2210AM Ammonia Analyzer NH layout. The calibration standard and corresponding part number, required for this application is determined in the following table based on the concentration range of interest. - Page 13 The ammonia method requires two reagents (for extending the range). The reagent usage depends on the frequency of analysis and the range selected. Based on 1 analyses per 2 hours, the reagents should last approximately 45 days. Introduction Orion 2210AM Ammonia Analyzer...
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Page 14: Installation Environmental Considerations
NEMA 12 and the Fluidics enclosure is a NEMA 4X fiberglass with a clear door window. The Orion 2210AM Ammonia Analyzer should be installed in a well-ventilated location, with ambient temperature between 5°C and 45°C (41°F to 113°F); and relative humidity not to exceed 90% at 40°C. -
Page 15: Plumbing Connections
The ⅜" (9.6 mm) DRAIN MUST BE VENTED TO ATMOSPHERE. The sample drain contains analysis wastes, which include both sample and chemical reagents. Please check with DANGER local authorities concerning proper disposal of waste from this product. 10 | Installation Environmental Considerations Orion 2210AM Ammonia Analyzer... -
Page 16: Installing The Reagents
Note the location of the fuse. Insert the wire into the terminal connector and make sure to tighten the screw. Route signal connections to the back hub, and power connections separately to the front hub. Orion 2210AM Ammonia Analyzer Installation Environmental Considerations... - Page 17 The terminal strip is located at the bottom of the electronics NOTE: cord, loop cord through clip retainer as cabinet (see Figure 9). shown in Figure 8 for proper strain relief. 12 | Installation Environmental Considerations Orion 2210AM Ammonia Analyzer...
- Page 18 RELAY contacts are rated at: 250 V, 2 A AC 500 W (non-inductive load). All inputs (except IN 6 & 7) must be connected to POTENTIAL FREE contacts. Figure 10. Communication ports Orion 2210AM Ammonia Analyzer Installation Environmental Considerations...
- Page 19 Common contact relay 2 Normally closed contact relay 3 Normally open contact relay 3 Common contact relay 3 Normally closed contact relay 4 Normally open contact relay 4 Common contact relay 4 14 | Installation Environmental Considerations Orion 2210AM Ammonia Analyzer...
- Page 20 These connectors are the Ethernet and USB A ports. (See Figure 10). For connecting to them, use the communication conduit hub port on the right side of the instrument for wire entry. Orion 2210AM Ammonia Analyzer Installation Environmental Considerations...
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Page 21: Startup And Operation
Startup and Operation Each Orion 2210AM Ammonia Analyzer gets thoroughly It is highly recommended to allow the wet-tested and calibrated at the factory, so the system is Orion 2210AM Ammonia Analyzer to ready to begin analyzing sample streams. The results of this... -
Page 22: In Auto-Calibration Mode
It is highly recommended to allow the previously stored calibration and will flash the “CHK CAL” NOTES: Orion 2210AM Ammonia Analyzer to message in the Info section of the LCD screen. complete its measurement cycle rather The “CHK CAL” message can be cleared by resetting the fault than using the STOP key. -
Page 23: Sample Analysis And Validation
The default setup for the analyzer uses the sample as the cleaning solution. A cleaning cycle can be performed by pressing: ➔ ➔ ➔ STOP MENU MEASUREMENT CLEAN This cycle helps maintain clean reaction cell. 18 | Startup and Operation Orion 2210AM Ammonia Analyzer... -
Page 24: Analyzer Hardware Configuration And Calibration
In order to get consistent and repeatable measurements, the method is setup such that the reaction cell in the Orion 2210AM Ammonia Analyzer is heated to a specific set point (30°C). A heater element located on the back plate of the reaction cell controls the temperature. -
Page 25: Pumps Calibration
90 seconds. The Orion 2210AM Ammonia Analyzer relies on a PID The sequence starts with a priming step to allow fluid to purge (Proportional, Integral, Derivative) algorithm setting to control the air from the tubing. -
Page 26: Calibration Of The Instrument For Measurement Analysis
Intercept = Concentration (Low) – [Slope X Absorbance (Low)]. This is used along with the slope for single point calibration. Two methods of calibration are provided in the Orion 2210AM The calibration data is available for editing. From the MAIN Ammonia Analyzer. -
Page 27: Theory Of Measurement
MENU SETUP (+) ANALYSIS PARAMETERS MODE The Orion 2210AM Ammonia Analyzer is designed to provide Manual Restart Mode on-line process measurements, and has two modes of operation. The mode is always displayed at the bottom right, i.e., below the Info field and above the status field of the This mode allows you to START the measurements manually. -
Page 28: Measurement Cycle
LED source. During this stage in the cycle, the info field (if enabled) shows The Orion 2210AM Ammonia Analyzer follows a sequence of the test optics progress bar which times out at a maximum steps or events for performing the analysis cycle. They are: period of 90 seconds. - Page 29 To edit the reagent volume, from the MAIN MENU follow the sequence: ➔ ➔ ➔ MAIN MENU SETUP METHOD (+) to go to page 2 ➔ STIR TIME (1, 2) 24 | Calibration of the Instrument for Measurement Analysis Orion 2210AM Ammonia Analyzer...
- Page 30 The Orion 2210AM Ammonia Analyzer product stores If the pump is not assigned to a reagent, it measurement and calibration results for up to 365 days. The...
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Page 31: Menu Overview
Allows configuration of the daylight saving for USA, Europe Display Parameters Menu and custom settings. When daylight saving is enabled, the Allows configuration of display-related parameters. system will correct the time based on the settings shown below the selection. 26 | Menu Overview Orion 2210AM Ammonia Analyzer... -
Page 32: Measurement Menu
(factory password required), printing options, instrument label, Review / Reset Alarms and to view instrument setup details. Allows user to review and selectively reset the faults and alarms triggered during the latest Analysis/Calibration/ Validation/Cleaning cycle performed. Orion 2210AM Ammonia Analyzer Menu Overview... -
Page 33: System Administration Menu
PLEASE NOTE THE (-) SIGN. Allows technician to print the system configuration, analysis parameters and method parameters. Also allows technician to enable/disable online printing. See Terms Definition Section for the default analyzer parameters listing printouts. 28 | Menu Overview Orion 2210AM Ammonia Analyzer... -
Page 34: Diagnostics Menu
LED. Any new setting of the gain or of the intensity of the LED will override any previous optics calibration setting. CONSULT FACTORY before overriding any setting. Orion 2210AM Ammonia Analyzer Menu Overview... -
Page 35: User Interface Tree
Validation Parameters Cleaner Parameters Calibration Parameters (+) Press + sign to go to next page Method (+) Page 3 Date & Time Daylight Saving Recovery After Power Failure Ethernet Parameters RS232 Parameters Language 30 | Menu Overview Orion 2210AM Ammonia Analyzer... - Page 36 Prime Reagent (1, 2) Prime Sample Priming Volume (+/-) Press (+) to go to page 2 New Reagents Blank Diagnostics Pumps and Stirrer Inputs Status Relays Analog Outputs LED & Detector Control ** Consult Factory first Orion 2210AM Ammonia Analyzer Menu Overview...
- Page 37 Blank Measurement (+) Page 2 Reagents 1, 2 and (+) Press + sign to go to next page Stir Time (+) Page 3 Cell Wash Flow rate Reagent1 and 2 flow rate 32 | Menu Overview Orion 2210AM Ammonia Analyzer...
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Page 38: Terms Definition
Enabled, Disabled of the current cycle performing. Selectable precision to show the analysis XXXX.X, XXX.XX, XX.XXX, X.XXX, XXXXX, Results Decimal Point result. Auto Large Fonts Screen To display the result with large fonts. Enabled, Disabled Orion 2210AM Ammonia Analyzer Terms Definition... - Page 39 Depends on the inner diameter of the The rate at which the reagent is pumped Reagent1 and 2 Flow Rate pump tubing. It is derived from the to wash the cell. calibration of pumps. 34 | Terms Definition Orion 2210AM Ammonia Analyzer...
- Page 40 Reaction Temperature PID temperature control. Enable, Disable Control Reaction Temperature The temperature set point. 0 to 60 Wavelength The LED wavelength. Allows the blank measurement in the Blank Measurement Disable, Before Reagent1, Reagent2 analysis cycle. Orion 2210AM Ammonia Analyzer Terms Definition...
- Page 41 Reset All Alarms? shown below this option. Displays the calibration results for the Reset All Faults? None selected data range. REVIEW CALIBRATION RESULTS Displays the calibration results for the Display None selected data range. 36 | Terms Definition Orion 2210AM Ammonia Analyzer...
- Page 42 Password of the new user entered. are allowed Measure Permission Measurement permission for the new user. Enabled, Disabled Calibrate Permission Calibration permission for the new user. Enabled, Disabled Validate Permission Validation permission for the new user. Enabled, Disabled Orion 2210AM Ammonia Analyzer Terms Definition...
- Page 43 To check the functionality of pumps. ON, OFF Pump3, Pump4 Stirrer To check the functionality of stirrer. ON, OFF RELAYS Relay1, Relay2, To check the functionality of relays. ON, OFF Relay3, Relay4 38 | Terms Definition Orion 2210AM Ammonia Analyzer...
- Page 44 LED & ADC Select LED To test the functionality of LED. 3, None Intensity Intensity of the LED. 0% to 100% Optics Amplifier gain Changing the gain of the amplifier. 0 to 255 Orion 2210AM Ammonia Analyzer Terms Definition...
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Page 45: Maintenance Schedule
Press (+) to go to next page and ENTER (+) upon next menu entry. the value of the reagent blank offset which is detailed on the form that comes with the new reagents kit. 40 | Maintenance Schedule Orion 2210AM Ammonia Analyzer... -
Page 46: Cleaning The Reaction Cell
Make sure that the stir bar is clean and moving freely, as needed. all tubing is secured and in good condition. The reaction cell assembly can swing NOTE: down to allow better access. Undo both thumb screws and swing down. Orion 2210AM Ammonia Analyzer Maintenance Schedule... -
Page 47: Cleaning The Sample Flow Chamber
Disconnect and empty out the reagents bottles and flush the lines using FLUIDICS PRIME menu. Release the pressure on the peristaltic pump tubing. Use the Table 3 to diagnose and correct analyzer problems. 42 | Maintenance Schedule Orion 2210AM Ammonia Analyzer... - Page 48 Problem with memory allocation. Insufficient Try again after some duration or after Do not try to repeatedly view the graph. memory in the system performing one more measurement cycle. or system is busy. Orion 2210AM Ammonia Analyzer Maintenance Schedule...
- Page 49 If the temperature is not able to reach the Try a different set point temperature. Temperature above set set point and is above the set point. Call a service agent. point. 44 | Maintenance Schedule Orion 2210AM Ammonia Analyzer...
- Page 50 Measured temperature differs widely from set May be due to the connectors or the Check for thermistor and heater temperature. Please check thermistor or heater malfunctioning. connections, and calibrate if necessary. for hardware malfunction. Orion 2210AM Ammonia Analyzer Maintenance Schedule...
- Page 51 Reagents High Range (For ranges above 10mg/L Ammonia) 2210AM001 Ammonia 1 mg/L Standard solution 2210AM005 Ammonia 5 mg/L Standard solution 2210AM025 Ammonia 25 mg/L Standard solution 2210AM250 Ammonia 250 mg/L Standard solution 2210CL Cleaning solution 46 | Maintenance Schedule Orion 2210AM Ammonia Analyzer...
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Page 52: Standby And On-Demand Modes
Orion 2210AM Ammonia Analyzer. CAUTION stand-by. The Orion 2210AM Ammonia Analyzer is equipped with two modes of operations: OPTIONAL MENU setting: 1. AUTO RESTART mode (default) 2. MANUAL mode (Please consult factory before modifying default setup). -
Page 53: Factory Setup Recommendations When Operating In "On-Demand" Mode
OFF position. When stopped, the unit will switch automatically to stand-by after one hour. In stand-by mode, the system will execute the necessary house-keeping to maintain a ready state. 48 | Standby and On-Demand Modes Orion 2210AM Ammonia Analyzer... -
Page 54: Customer Services
OR IN CONJUNCTION WITH THE SALE OR USE OF THIS ICES-003. PRODUCT. The Thermo Scientific Orion 2210AM Ammonia Analyzer is The customer’s sole and exclusive remedy is the return of CE and cTUVus certified, which includes testing to EMC and defective components or sub assemblies to Thermo Fisher US and Canadian standards. -
Page 55: Consumables
In Europe, the Middle East and Africa, contact your local authorized dealer. For the most current contact information, visit www.thermofisher.com/water. For the latest application and technical resources for Thermo Scientific Orion products, visit www.thermofisher.com/water. 50 | Customer Services Orion 2210AM Ammonia Analyzer... -
Page 56: Addendum
The RESULT READY signal can operate in two timing modes: ACTIVE TIME: 060 sec (default setting) The signal is activated at the end of the sample measurement cycle and reset after the specified time. The limit is 900 sec. Orion 2210AM Ammonia Analyzer Addendum... -
Page 57: 2210Am Analyzer Interface To A Sample Conditioner
In most cases the sample conditioner continuously provides sample to the analyzer for periodic sample analysis by the 2210AM at a frequency specified by the user. For those cases where the sample conditioner system is kept in stand by until the analyzer signals a request for fresh... - Page 58 FILTER, SIZE IS BASED ON SAMPLE PROCESS LINE SYSTEM CONDITION, SET FLOW RATE BETWEEN : 50 TO 500 ML/MIN SAMPLE RETURN Figure 14. Using WASH IN PROCESS signal from the 2210AM with an external sample conditioner system. Orion 2210AM Ammonia Analyzer Addendum...
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Page 59: 2210Am Analyzer Only
2210AM Analyzer ONLY The UNIVERSAL 2210AM Ammonia analyzer has a specific programmed method for executing the wash and sample capture; the method starts with a PRE-WASH sequence. The... -
Page 60: Sample Analysis Data Storage
REAGENT 2 PUMP VENT REACTION CELL TO CELL TO DRAIN SUCTION VALVE 1 VALVE 2 Mounted on Back plate SAMPLE RETURN TO PROCESS FILTERED SAMPLE IN TO DRAIN Figure 15. 2210AM Universal Ammonia Analyzer fluidics plumbing diagram. Orion 2210AM Ammonia Analyzer Addendum... - Page 61 Water Analysis Instruments North America Germany India Japan Toll Free: 1-800-225-1480 Tel: (49) 6184-90-6000 Tel: (91) 22-4157-8800 Tel: (81) 045-453-9175 Tel: 1-978-232-6000 info.water.uk@thermofisher.com wai.asia@thermofisher.com wai.asia@thermofisher.com info.water@thermofisher.com China Singapore Australia Tel: (86) 21-68654588 Tel: (65) 6778-6876 Tel: (613) 9757-4300 wai.asia@thermofisher.com wai.asia@thermofisher.com In Australia: (1300) 735-295 InfoWaterAU@thermofisher.com Find out more at...