Analytical Operation; Method Optimisation; Running The Icap - Thermo Scientific iCAP 6000 Series User Manual

Using the iCAP

Analytical Operation

Analytical
Operation
Method
Optimisation
Running the
4-2
iCAP User Guide
The iCAP 6000 will require optimisation that is dependent on the
sample being analysed and the method requirements.
It is important that the method development verifies the data produced
by the method.
It is also important that a suitable quality control regime is established
that verifies the continuing validity of data.
Training courses are available through a local Thermo Scientific Sales
Office; contact details are available on www.thermo.com.
The following parameters can all affect the data obtained and should be
optimised. Usually a default setting will give data that is satisfactory,
but may not be optimal for the analysis requirements.
Nebuliser Gas flow
Plasma viewing height
RF Power
Pump speed
Auxiliary gas flow
Coolant gas
Integration times
Once the iCAP has been on and the optics have been purged for a
sufficient time using argon or nitrogen, you can begin to use your
iCAP
instrument for analysis.
Note: Gas pressures, details of power supplies and water chillers, etc.
can be found on the Pre-Installation guide on your supplementary CD.
It is critical to the instrument's operation that these specifications are
followed.
Thermo Fisher Scientific