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Manuals and User Guides for Thermo Scientific 450iQ. We have
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Thermo Scientific 450iQ manual available for free PDF download: Instruction Manual
Thermo Scientific 450iQ Instruction Manual (306 pages)
Hydrogen Sulfide and Sulfur Dioxide Analyzer
Brand:
Thermo Scientific
| Category:
Measuring Instruments
| Size: 21.79 MB
Table of Contents
Table of Contents
3
Introduction
9
Iq Series Instrument Platform
9
Figure 1-1. 450Iq Front
10
450Iq Principle of Operation
11
Figure 1-2. 450Iq Flow Schematic
12
Figure 1-3. 450Iq Flow Schematic with Zero Span
12
Specifications
13
Table 1-1. 450Iq Specifications
13
Table 1-2. 450Iq Optional Permeation Oven Specifications
14
Dimensions
15
Figure 1-4. Bench Mount Assembly (Dimensions in Inches [MM])
15
Figure 1-5. Rack Mount Assembly (Dimensions in Inches [MM])
16
Figure 1-6. Rack Mount Requirements
17
Installation and Setup
19
Unpacking and Inspection
19
Cover Removing and Replacing
20
Figure 2-1. Removing the Cover
20
Bench Mount
21
Figure 2-2. Installing Feet
21
Mounting Options
21
Figure 2-3. Removing the Front Panel
22
Rack Mount
22
Figure 2-4. Installing Ears and Handles
23
Setup Procedure
24
Figure 2-5. 450Iq Rear Panel
25
Figure 2-6. Atmospheric Dump Bypass Plumbing
25
Figure 2-7. Front Panel and Touchscreen Display
26
Startup
26
Chapter 3 Operation
27
Instrument Display
27
Main Menus and Keypads
31
Numeric Keypad
32
Alphanumeric Keypad
33
Calibration
35
Calibrate Background
36
Calibrate so 2 and CS Background
37
Calibrate Span Coefficients
39
Calibrate so 2 , H
41
Zero/Span Schedule
44
Advanced Calibration
46
Manual Calibration
47
Calibration History
55
Data
56
View Data Log (Last Hour)
57
View Data Log (Last 24 Hours)
58
View Data Log (User Defined Time)
59
Advanced Data Setup
61
Data Logging Setup
62
Select Data Logging Variables
63
Streaming Data Setup
64
Select Streaming Variables
65
Settings
66
Health Check
67
Status and Alarms
68
Valve and Pump Resets
82
Predictive Diagnostics
88
Maintenance
89
Preventive Maintenance
90
Change Part
92
Maintenance History
93
File Sharing and Support
94
Measurement Settings
98
Averaging Time
99
Range Mode Selection
101
Range Settings
103
Gas Mode
106
Gas Units
107
Advanced Measurement Settings
108
Communications
115
Wired TCP/DHCP
117
Serial RS-232/485
119
Analog I/O
120
Digital I/O
121
Email Server (SMTP)
122
Bayern Hessen Settings
123
Ethernet Protocol Selection
124
Instrument Settings
125
Instrument Setpoints
126
Alarm Setpoints
127
Clock
129
Time Zone
133
Display Setup
136
Configuration
138
Security Access Levels
139
Change Security to View Only Access
141
Change Full Access Security Password
142
Change Instrument Password
144
Reset Instrument Password
146
USB Drive
147
Firmware Update Via USB Drive
148
Download Data to USB Drive
152
Change USB Password
155
Reset USB Password
157
User Contact Information
158
Update Bootloader
159
Chapter 4 Calibration
161
Zero Gas Generation
161
Commercial Heatless Air Dryers
161
Absorbing Column
161
Calibration Gas Generation
161
Cylinder Gas Dilution
162
Figure 4-1. Cylinder Gas Dilution System
162
Commercial Precision Dilution Systems
163
Permeation Tube System
163
Figure 4-2. Permeation Tube System
163
Pre-Calibration
164
Calibration in Single Range Mode
166
Calibration
166
Set so 2 and CS Backgrounds to Zero
166
Calibrate so
166
Calibrate so
167
Calibrate CS
168
Calibrate H S
169
Calibration in Dual Range and Auto Range Mode
170
Set so
170
And CS
170
Zero and Span Check
171
Calibrate High so 2 , H S, and CS
171
Manual Calibration
172
Adjust so
173
Adjust Span Coefficient
174
Zero/Span Schedule
175
Next Time
175
Period
175
Zero/Span/Purge Duration Minutes
175
Schedule Averaging Time
176
Zero/Span Ratio
176
Chapter 5 Maintenance
177
Safety Precautions
177
Fan Filter Inspection and Cleaning
177
Pump Rebuilding
178
Figure 5-1. Single Stage Pump
178
Figure 5-2. Pump Rebuilding
180
Leak Test
181
Lamp Voltage Check
182
Lamp Voltage Adjustment
182
Chapter 6 Troubleshooting
185
Safety Precautions
185
Troubleshooting Guide
185
Table 6-1. 450Iq Troubleshooting Guide
185
Chapter 7 Servicing
195
Safety Precautions
195
Figure 7-1. Properly Grounded Antistatic Wrist Strap
196
Firmware Updates
197
Replacement Parts List
197
Figure 7-2. 450Iq Component Layout Top View
198
Figure 7-3. 450Iq Component Layout Side View
198
Fuse Replacement
199
Figure 7-4. Replacing the Fuses
199
Filter Replacement
200
Figure 7-5. Start with Top Right Corner of Fan Cover
200
Figure 7-6. Removing the Fan Cover
200
Fan Replacement
201
Figure 7-7. Unplugging the Fan Cable
201
Figure 7-8. Replacing the Fan
202
Measurement Side Removal and Replacing
203
Figure 7-9. Unplugging the Fan Cable
203
Figure 7-10. Unplugging the DMC Cable
204
Figure 7-11. Unfasten Hardware Front for Measurement Side Removal
204
Figure 7-12. Unfasten Hardware Rear for Measurement Side Removal
205
LCD Module Replacement
206
Figure 7-13. Replacing the LCD Module
206
Figure 7-14. Remove Electrical Cables from LCD
207
I/O Replacement
208
Figure 7-15. I/O Replacement, Arm
208
Figure 7-16. I/O Replacement, Remove Board
208
Figure 7-17. I/O Replacement, Install
209
Figure 7-18. I/O Replacement, Close Arm Alignment
209
Peripherals Support Board and System Controller Board Replacement
210
Figure 7-19. Replacing the Peripherals Support Board
210
DMC Pressure and Flow Board
211
Figure 7-20. Flow Pressure Board, Disconnect DMC Cable
211
Figure 7-21. Flow Pressure Board, Screws
212
Pump Replacement
213
Figure 7-22. Remove Pump, Disconnect and Unfasten
214
Figure 7-23. Pump Removal, Keyway
215
Figure 7-24. Pump Replacing, Unfasten Screws
215
Capillary Cleaning And/Or Replacement
216
Figure 7-25. Remove Capillary, Disconnect and Unfasten
216
Figure 7-26. Capillary Plate, Keyway
217
Figure 7-27. Capillary and O-Ring Replace
217
Capillary O-Ring Replacement
218
Power Supply Replacement
218
Figure 7-28. Removing Power Supply
219
Figure 7-29. Replacing Power Supply
220
Step POL Board Replacement
221
Figure 7-30. Unplug and Unfasten Step POL Board
221
Figure 7-31. Clear Partition Keyway Step POL Board
222
Figure 7-32. Step POL Board 1 Switch Settings
223
Figure 7-33. Optional Step POL Board 2 Switch Settings
223
DMC Optical Bench Removal
224
Optical Bench Assembly Removal
224
Figure 7-34. Removing the DMC Optical Bench Removal from Instrument
225
Figure 7-35. Removing the Optical Bench Assembly
226
Photomultiplier Tube (PMT) Replacement
228
Figure 7-37. Removing the PMT Assembly
228
Figure 7-38. Removing the PMT Cover
229
Figure 7-39. Replacing the PMT
229
Flasher Pack Replacement
230
Figure 7-40. Removing and Replacing the Flasher Pack
230
Flasher Pack Lamp Replacement
231
Figure 7-41. Replacing the Flasher Pack Lamp
231
Kicker Assembly Replacement
234
Figure 7-44. Removing and Replacing the Kicker Assembly
234
Optional Manifold Replacement
235
Figure 7-46. Replacing the Manifold Pt 2
236
Figure 7-47. Replacing the Manifold Pt 3
236
Scrubber Replacement
237
Figure 7-48. Removing and Replacing the Scrubber
237
Optional DMC Permeation Oven Solenoid Valve Replacement
238
Mode Valve Replacement
240
Converter DMC Replacement
242
Figure 7-53. Converter DMC Assembly Remove
242
Converter Assembly Board Replacement
243
Figure 7-54. Replacing the Converter Assembly Board
243
Converter Cartridge Heater Replacement
244
Figure 7-55. Converter Assembly Replace Heater
245
Optional Permeation Oven Replacement
246
Figure 7-57. Finger Push and Release Tubing
247
Optional Permeation Oven Board Replacement
249
Figure 7-59. Replacing the Permeation Oven Board
249
Chapter 8 System Description
251
Optical Bench DMC
253
Flash Lamp Trigger Assembly
253
Flash Lamp
253
Flash Trigger Board
253
Flash Intensity Assembly
253
Photomultiplier Tube
253
Bench Heater
254
SO2 Scrubber (Optional)
254
Converter
254
Permeation Oven (Optional)
254
Common Electronics
254
Figure 8-1. Common System Interconnect Diagram
255
Figure 8-2. 450Iq System Interconnect Diagram
256
Power Supply
257
Front Panel
257
I/O and Communication Components
257
System Controller Board
257
Backplane Board
257
Peripherals Support System
258
Fan
258
Step POL Board
258
Sample Pump
258
Flow/Pressure DMC
258
Firmware
258
Chapter 9 Optional Equipment
261
Connecting External Devices
261
Communication Board
261
Figure 9-1. I/O Expansion Replacement Boards
261
RS-232/RS-485 Port
262
RS-485 External Accessory Port
262
Figure 9-2. RS-232/RS-485 Port
262
Table 9-1. RS-232/RS-485 Port Terminal Assignment
262
Figure 9-3. RS-485 External Accessory Port
263
Table 9-2. RS-485 External Accessory Port Terminal Assignment
263
Analog I/O Board
264
Analog Voltage Inputs
264
Figure 9-4. Analog Voltage Inputs
264
Table 9-3. Analog Voltage Inputs Assignment
264
Analog Voltage Outputs
265
Figure 9-5. Analog Voltage and Current
265
Table 9-4. Analog Voltage and Current Assignment
266
Analog Output Zero Calibration
267
Analog Output Full Scale Calibration
269
Digital I/O Board
271
Digital Inputs
271
Digital Relay Switches
271
Valve Driver Outputs
271
Figure 9-6. Digital Inputs
271
Table 9-5. Digital Inputs Terminal Assignment
272
Figure 9-7. Digital Relay Switches
273
Table 9-6. Digital Relay Switch Assignment
274
Figure 9-8. Valve Driver Outputs
275
Table 9-7. Valve Driver Outputs Assignment
276
Internal Zero/Span and Sample Valves
277
Internal Permeation Span Source
278
Figure 9-9. Internal Permeation Span Source Flow Diagram
278
Permeation Tube Installation
279
Figure 9-10. Installing Glass Tube Pt 1
279
Computation of Concentrations
282
PTFE Particulate Filter
283
Appendix A Safety, Warranty, and WEEE
285
Safety
285
Safety and Equipment Damage Alerts
285
Warranty
286
WEEE Compliance
288
WEEE Symbol
288
Appendix B Quick Reference
289
GNU Lesser General Public License
293
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