Page 1 ICP OPTICAL EMISSION Customer Hardware and Service Guide...
Page 3 Avio 500 Customer Hardware and Service Guide...
Page 4 The information contained in this document is subject to change without notice. Except as specifically set forth in the terms and conditions of sale, PerkinElmer makes no warranty of any kind with regard to this document, including, but not limited to, the implied warranties of merchantability and fitness for a particular purpose.
Page 5: Table Of Contents
Contents Customer Service ..............11 Safety and Regulatory Information .
Page 6 Gases for the Avio 500 ICP ........
Page 7 Contents Spray Chamber ..............89 Nebulizers .
Page 8 Contents Connecting the Cyclonic Spray Chamber ..........155 Setting the Torch Position .
Page 9 Contents Torch Viewing Position Alignment ..........203 Performance Checks .
Page 10 Contents Removing the Argon Tip from the End Cap, N0780546 ........265 Connecting the Nebulizer Argon Tubing (Cross-Flow End Cap, N0780546) .
Page 11 Contents Consumables and Supplies ............313 Chapter 6: Troubleshooting What the Performance Checks Measure .
Page 12 Contents...
Page 13: Customer Service
If you are located within the U.S., call toll free 1-800-762-4000, 8 a.m. to 8 p.m. EST. Your order will be shipped promptly, usually within 24 hours. If you are located outside of the U.S., call your local PerkinElmer sales or service office.
Page 14: Safety And Regulatory Information
The protection provided by this equipment may be impaired if Caution the equipment is used in a manner not specified by PerkinElmer. Attention La protection fournie par cet équipement risque d'être moins efficace si l'équipement fait l'objet d'une utilisation différente de celle...
Page 15: Regulatory Information
Safety and Regulatory Information A caution indicates an operation that could cause instrument damage Caution if precautions are not followed. Attention Une telle mise en garde signale une opération risquant d'endommager l'instrument si les précautions d'usage ne sont pas respectées Regulatory Information Safety compliance Safety information is located in the European Union Declaration of Conformity.
Page 16: Environment
United States (FCC) This instrument is classified as a digital device used exclusively as industrial, commercial, or medical equipment. It is exempt from the technical standards specified in Part 15 of FCC Rules and Regulations, based on Section 15.103 (c). Environment Operating Conditions Explosive Atmosphere...
Page 17: Symbols Used On The Instrument
Safety and Regulatory Information • Temperature +5 °C to +40 °C (+41 °F to +104 °F). • Relative humidity 20% to 80%, without condensation. • Altitude in the range -400 m to 2,000 m (-1,312 ft. to 6,562 ft). Storage conditions: •...
Page 18 This symbol indicates Caution, hot surface. AVERTISSEMENT: La surface est chaude. The following graphic symbols are also found on the instrument: Indicates the OFF position of the main power switch. Indique la position Off de l'interrupteur d'alimentation principal. Indicates the ON position of the main power switch. Indique la position On de l'interrupteur d'alimentation principal.
Page 19: Warning Labels On The Instrument
Safety and Regulatory Information Warning Labels on the Instrument Safety Labels on the Front of the Instrument The warning labels shown below appear in the locations described in the following table and shown in Figure A. For more information on the Emergency Off Switch see EMO Switch on page 105 in this Hardware Guide.
Page 20 Warning Hazard CAUTION: This unit contains protective circuitry. Contact PerkinElmer qualified personnel before performing any AC line tests. Attention: Cet appareil continent un circuit protecteur. Contact le personnel qualifié de PerkinElmer d’effectuer un quelconque controle de circuit en courant alternatif.
Page 21 Safety and Regulatory Information WARNING: To avoid electrical shock, diconnect the power cord before servicing. Débrancher le cordon d'alimentation de l’apparell avant l'entretien afin de prévenir les chocs électriques. WARNING: Equipment needs to be de-energized for 60 seconds to allow safe discharge of capacitors.
Page 22 Safety Labels on the Sides of the Instrument Additional Instructions: To provide adequate space for ventilation, allow at least 15 cm (6 in.) of space between the instrument and the laboratory wall. Do not obstruct the air filters. See Figure D for the location of the filters. Left Side of the Instrument Figure C.
Page 23 Safety and Regulatory Information Right Side of the Instrument Figure D. Location of Warning Labels on the Right Side of the Instrument. Item Warning Hazard CAUTION: Do not restrict air intake or exhaust. ATTENTION: N’obstruez pas l’arrivée ou l’évacuation d’air.
Page 24 Item Description Spray Chamber Compartment Caution: Only use PerkinElmer Flat Plate Torch Glassware Using any other glassware will damage the torch. Attention: N'utiliser que la seringue PerkinElmer Flat Plate Torch Glassware. L'utilisation de toute autre verrerie peut endommager la torche.
Page 25 Safety and Regulatory Information Safety Labels in the Torch Compartment of the Instrument Figure F. Location of warning labels in the torch compartment. Item Description Inside Torch Compartment Warning Label Hot Surface Warning Label-Do Not Defeat Interlocks...
Page 26 Additional Instructions: The instrument has safety interlocks to protect the operator from exposure to radio frequency and ultraviolet radiation. Do not attempt to defeat the safety interlocks. WARNING – DO NOT DEFEAT INTERLOCKS. AVERTISSEMENT: Ne pas desengager les enclenchements de securite. This symbol indicates Caution, hot surface.
Page 27: Using This Guide
Using this Guide Using this Guide This manual is your hardware guide to the Avio 500 instrument. Main topics include: • safety practices • preparing your laboratory • a description of the system • installation • maintenance • troubleshooting •...
Page 28: How This Guide Is Organized
To find out about... 1 Safety Practices Important safety information. 2 Preparing Your Laboratory The preparation of your laboratory needed for the Avio 500 instrument. Environmental, electrical, space, exhaust, gases, and cooling water requirements are reviewed. 3 System Description The components of the instrument, how the Echelle spectrometer works and instrument specifications.
Page 29: Using The Index
A Word on Troubleshooting We recommend that you consult the troubleshooting information included in this manual before you call a PerkinElmer service engineer. The Troubleshooting chapter contains suggestions to help you determine systematically whether instrument problems are due to improper analytical techniques, improper selection...
Page 31 C h a p t e r 1...
Page 33: Chapter 1: Safety Practices
Safety Practices...
Page 34: Introduction
General The protection provided by this equipment may be impaired if Caution the equipment is used in a manner not specified by PerkinElmer. Attention La protection fournie par cet équipement risque d'être moins efficace si l'équipement fait l'objet d'une utilisation différente de celle mentionnée par PerkinElmer.
Page 35: Environmental Conditions
PerkinElmer shall specify any parts which are required to be examined or supplied only by PerkinElmer or agents of PerkinElmer Always wear safety glasses when using the instrument. Safety glasses with side shields will provide an extra margin of safety as well as mechanical protection for your eyes.
Page 36: Handling Of The Instrument
Handling of the Instrument Contact a PerkinElmer service engineer for assistance in installing or evaluating the system after moving. The Avio 500 weighs 163 kg (359 pounds), or 203 kg (447 pounds) with the shipping container. If the instrument needs to be moved please contact PerkinElmer Service.
Page 37: Safety Interlocks
Instrument Safety Practices Safety Interlocks The instrument has safety interlocks to protect the operator from radio frequency (RF) radiation and ultraviolet radiation, and to prevent access to high voltage areas. Do not attempt to defeat the safety interlocks. This would place the operator's safety at risk.
Page 38: Electrical Safety
This section describes some recommended electrical safety practices. Lethal voltages are present at certain areas within the instrument. Installation and internal maintenance of the instrument should only be performed by a PerkinElmer service engineer or similarly Warning authorized and trained person.
Page 39 Instrument Safety Practices Des tensions mortelles sont présentes dans certaines zones de l'instrument. La maintenance interne de l'instrument ne doit être confiée qu'à un responsable technique PerkinElmer ou à une Warning personne disposant des mêmes autorisations et qualifications. Lorsque l'instrument est raccordé à la ligne électrique, l'ouverture de ses capots risque d'exposer des pièces sous tension.
Page 40 Safety Practices Connect the instrument to an AC line power outlet that has a protective ground connection. To ensure satisfactory and safe operation of the instrument, it is essential that the protective ground conductor (the Warning green/yellow lead) of the line power cord is connected to true electrical ground.
Page 41 Instrument Safety Practices Any interruption of the protective conductor (earth ground) inside or outside the instrument or disconnection of the protective conductor terminal is likely to make the instrument dangerous. Intentional Warning interruption is prohibited. Avertissement: Toute interruption du conducteur de protection (mise à...
Page 42: High Temperatures
Safety Practices • Disconnect the instrument from all voltage sources before opening it for any adjustment, replacement, maintenance, or repair. If afterwards, the opened instrument must be operated for further adjustment, maintenance, or repair, this must only be done by a qualified person who is aware of the hazards involved.
Page 43: Waste Disposal Procedures
Instrument Safety Practices Never place the vessel in an enclosed cabinet. Doing so could result in a build-up of hazardous gases, which may result in a serious explosion or fire. Warning Never use a glass drain vessel. A glass drain vessel may break and spill flammable, toxic, or corrosive liquids.
Page 44 Requirements for waste collection reuse, recycling, and recovery programs vary by regulatory authority at your location. Contact your local responsible body (e.g., your laboratory manager) or authorized representative for information regarding applicable disposal regulations. Contact PerkinElmer at the web site listed below for information specific to PerkinElmer products.
Page 45: Safe Handling Of Gas Cylinders
For Customer Care telephone numbers select "Contact us" on the web page. Products from other manufacturers may also form a part of your PerkinElmer system. These other producers are directly responsible for the collection and processing of their own waste products under the terms of the WEEE Directive.
Page 46: Identification Of Gas Cylinders
Safety Practices If liquid argon or nitrogen is used, the gas cylinder must be fitted with an over- pressure regulator, which will vent the cylinder as necessary to prevent it from becoming a safety hazard. Listed below are some general safety practices for the proper identification, storage, and handling of gas cylinders.
Page 47: Hazardous Chemicals Warnings
Safe Handling of Gas Cylinders Handling Cylinders • If it becomes necessary to move cylinders, do so with a suitable hand truck after ensuring that the container cap is secured and the cylinder properly fastened to the hand truck. • Use only gas-pressure regulators, tubing, and hose connectors approved by an appropriate regulatory agency.
Page 48 Safety Practices Avertissement : certains produits chimiques utilisés avec cet instrument peuvent être dangereux ou le devenir une fois l'analyse terminée. Le responsable (par exemple, le responsable du laboratoire) Warning doit prendre les précautions qui s'imposent afin de veiller à ce que les opérateurs de l'instrument et l'espace environnant ne soient pas exposés à...
Page 49: Safe Use Of Chemical Reagents
Safe Handling of Gas Cylinders Safe Use of Chemical Reagents Give careful attention to the hazards associated with the chemical reagents being used. Refer to the safety data sheets provided by the manufacturer, for example, Material Safety Data Sheets (MSDS) in Warning the USA (for other names, see Reference 5).
Page 50: Sample Preparation
Safety Practices • Store solvents in an approved cabinet (with the appropriate ventilation, as required) away from the instrument. • The responsible body has the responsibility for carrying out appropriate decontamination if hazardous material is spilt on or inside the instrument. Sample Preparation Sample preparation for ICP spectroscopy may require the handling of organic or corrosive solutions.
Page 51: Dissolving Solid Samples In Organics
Sample Preparation Dissolving Solid Samples in Organics • Always work in a fume hood so that flammable and/or toxic solvents do not concentrate in the work area. • Wear protective clothing and gloves. Some solvents are readily absorbed through the skin. When selecting a solvent, consider the following: •...
Page 52: Acid Digestions
Safety Practices • Attempt to dissolve the sample in a dilute acid solution before using concentrated acid. • Add concentrated acid to a sample cautiously. Dissolving a sample in concentrated acid may provoke a vigorous reaction. Acid Digestions Acid digestions, either at atmospheric pressure or at increased pressure, require special care.
Page 53 Sample Preparation Hydrofluoric Acid Hydrofluoric acid (HF) is also used for digestions. It is toxic and extremely corrosive. Hydrofluoric acid will readily burn skin, and if the fumes are inhaled, lung tissue. Burns may not be immediately painful or visible. Contact with eyes could result in blindness.
Page 54: Fusion Mixtures
Safety Practices • Cool the completed digest before transferring it and diluting it. Add water cautiously. Digestions at Elevated Pressure Acid digestions in a pressure digestion apparatus require special care at several points, in addition to the precautions described above. When using high pressure digestion vessels, consult the manufacturer's instructions and recommendations, particularly regarding organic material and possible explosive reactions.
Page 55: Decontamination And Cleaning
Decontamination and Cleaning Before using any cleaning or decontamination methods except those specified by PerkinElmer, users should check with PerkinElmer that the proposed method will not damage the equipment. Decontamination Customers wishing to return instrumentation and/or associated materials to...
Page 56: Cleaning The Instrument
In Canada, call toll free 800-561-4646 and speak to Customer Support. If you are located outside of the United States or Canada, please call your local PerkinElmer sales office for more information. Cleaning the Instrument Exterior surfaces may be cleaned with a soft cloth, dampened with a mild detergent...
Page 57: References
References References 1. Furr, K., ed., CRC Handbook of Laboratory Safety, 5th ed., The Chemical Rubber Co. Press, 2000. 2. National Research Council, Prudent Practices for Handling Hazardous Chemicals in Laboratories, National Academy Press, Washington, D.C., USA, 1981. 3. Compressed Gas Association (USA), "Safe Handling of Compressed Gases in Containers,"...
Page 58 Safety Practices...
Page 59 C h a p t e r 2...
Page 61: Chapter 2: Preparing Your Laboratory
Laboratory Chapter Overview The Avio 500 is a complete system, with the exception of the following items: suitable working area, exhaust vent, gases and regulators, cooling water, and a computer table or bench. The items shown in the following checklist need to be considered when preparing the laboratory for the instrument: •...
Page 62: Exhaust Vent Requirements
• Altitude: in the range -400 to 2,000 m (-1,312 to 6,562 feet) The Avio 500 has been designed for indoor use. Do not use the instrument in an area where explosion hazards may exist. Pollution Degree: This product will operate safely in environments that contain nonconductive foreign matter up to Pollution Degree 2 in EN 61010-1.
Page 63 The temperatures of the exhaust gases upon exiting the instrument are about 200 °C (392 °F) at 1500 watts of RF power. The exhaust duct is connected directly to the top of the Avio 500 instrument and it is recommended to use the 4-inch (10.16 cm) I.D. flexible ducting provided to make the final connection to the instrument with stainless steel tubing for the rest of the exhaust ducting.
Page 64: Vent Positions
The venting system for the ICP torch connects directly to the torch compartment chimney located on top of the sample compartment. 4-inch inner diameter tubing is provided with the Avio 500 ICP-OES for making this connection. For proper instrument venting, order PerkinElmer Venting Kit (Part No. N0790188, 110V;...
Page 65 Exhaust Vent Requirements 1. Place exhaust hose over the instrument exhaust connector. 2. Secure the hose clamp around the exhaust hose. Figure 2-1 Location of the Torch Compartment Chimney and Vent. Item Description Top of Instrument Hose Clamp Exhaust Hose...
Page 66: Laboratory Space Requirements
(34.4 in.). Figure 2-2 illustrates the dimensions of the instrument. The instrument 163 kg (359 lb), or 203 kg (447 lbs) with the shipping container. The Avio 500 may be placed on a bench. PerkinElmer has a bench for the Avio 500 (Part No. N8142011).
Page 67 Laboratory Space Requirements Avio 500 Figure 2-2. Outside Dimensions of the Instrument. Item Description 87 cm 34.4 Height in.) 84 cm 33.1 Depth in.) 76 cm (29.9 in.) Length...
Page 68 Preparing Your Laboratory Table 2-1. Avio 500 ICP-OES Cables and Hoses Lengths Part Number Description Length N0810500 Avio 500 Power Cable Assembly 2.4 M (8 Ft) 09290332 Ethernet Cable 4.57M (15 Ft) Instrument to Computer 09290798 USB Cable for Plasma Camera 3M (9.84 Ft)
Page 69: Location
à l'entrée d'eau de l'instrument entre 15 ° C et 25 ° C. Location Typically, the Avio 500 is positioned with the computer and printer on the bench next to the instrument or on an adjacent table. The computer and printer must not be placed on the instrument.
Page 70: Electrical Requirements
être retiré pendant ou après l'installation. • The Avio 500 ICP-OES is equipped with an IEC 309 250 V 16/20 A 2-pole plus protective earth plug (Hubbell® Part No. C320P6SVL, PerkinElmer Part No. 09997530) that inserts into a receptacle (Walther Part No. 410306, PerkinElmer Part No.
Page 71 • The Avio 500 instrument is supplied with a 2.5 m (8 ft.) line power cord that supplies both the spectrometer and the RF Generator. The line power supply point must be within 2.5 meters of the rear of the spectrometer.
Page 72: Handling Of Gas Cylinders And Other Suggested Safety Practices
A PolyScience® WhisperCool™ Recirculating Chiller meets these requirements and is recommended for the instrument. The PolyScience® WhisperCool™ is available through PerkinElmer in the following two configurations: 208-230 V, 50 Hz (Part No. N0772045); 208-230 V, 60 Hz (Part No. N0772046).
Page 73: Gases For The Avio 500 Icp
Gases for the Avio 500 ICP Argon is used as the ICP torch gas with the Avio 500. Nitrogen is recommended for the optical purge gas, although argon can be used as well. The quality criteria for the argon and the nitrogen are shown in Table 2.
Page 74 (0.25-inch Swagelok® connection). For the Avio 500, typical argon consumption would be 10 SLPM argon while the plasma is running in a low-flow condition and 1 SLPM for detector purge at all other times;...
Page 75: Plasma Shear
03030284). The regulator can be used with CGA 580 or CGA 590 fittings. Plasma Shear The Avio 500 uses a shear gas to remove the plasma plume and to keep the heat away from the optics. Either clean air or nitrogen can be used for the shear gas. The shear flow is 25 L/min (1 cubic foot/min) at a minimum of 550 kPa (80 psig).
Page 76 Preparing Your Laboratory...
Page 77 C h a p t e r 3...
Page 79: Chapter 3: System Description
System Description...
Page 80 The Avio 500 Inductively Coupled Plasma Optical Emission Spectrometers (ICP-OES). This chapter introduces you to the Avio 500 Inductively Coupled Plasma Optical Emission Spectrometer (ICP-OES). It includes the following sections. Avio 500 describes the instrument, key instrument features, and different plasma- viewing configurations.
Page 81: Plasma Viewing Configurations
Avio 500 • The Avio 500 is a dual view detector system. The UV detector covers an extended ultraviolet wavelength range from 165 to 403 nm. The VIS detector covers the visible wavelength range from 404 to 782 nm.
Page 82 System Description Figure 3-2. Transfer optics on the Dual View instrument shown in Axial viewing mode. Item Description Item Description Torch Toroidal Mirrors Plasma Entrance Slit Flat Mirror...
Page 83 Avio 500 Figure 3-3. Transfer optics on the Dual View instrument shown in Radial view- ing mode. Item Description Item Description Torch Toroidal Mirrors Plasma Entrance Slit...
Page 84 Major Components The Avio 500 consists of two major components: the spectrometer and the ICP Source. The Avio 500 consists of two detectors. The plasma source is a dual-view (can be viewed either axially or radially) RF generator. The sample introduction system includes a built-in peristaltic pump and a "quick change"...
Page 85 In addition, the sample compartment (part of the ICP Source) contains a Quick- Change Adjustable Torch Module, which can be easily removed in order to replace the torch. The following figure shows the major components of the Avio 500. Figure 3-4.
Page 86: Spectrometer
To separate the orders and create a two-dimensional diffraction pattern, the echelle grating is combined with a cross-dispersing element. In the ultraviolet range, a cross disperser is used. On the Avio 500, a prism is also used in the visible range.
Page 87: Detector Cooling And Purging
Spectrometer The optics are mounted to modules which are secured to the aluminum tub-like enclosure. Nitrogen is used to purge the optical system during operation to remove oxygen and moisture and keep the environment dry. The nitrogen purge also improves sensitivity for elements with wavelengths below 190 nm, particularly aluminum at 167 nm.
Page 88: Icp Source
ICP Source RF Generator The Avio 500 instruments use a 40-MHz free-running solid state RF generator. The RF power from the solid state oscillator is used to ionize the argon in the torch and excite the atoms of the liquid sample so that they emit energy at their atomic wavelength in the form of photons.
Page 89 ICP Source Figure 3-5. Block diagram illustrating the RF Power Control (RFPC) Item Description Item Description AC Power Input Control Feedback Signal 40 MHz RF Power Generator Power Measurement Signal RF Power to Plasma Induction Plates RF Power Control Loop Plasma Microprocessor...
Page 90: Rf Control Electronics
Quick-Change Adjustable Torch Module The Quick-Change Adjustable Torch Module is the quartz torch, injector, spray chamber, and nebulizer/end cap – all in one assembly for the Avio 500 instrument. This module can be quickly removed from the sample compartment. This adjustable mount allows the torch an adjustment of up to 5 mm.
Page 91: Torch
Cross-Flow pneumatic nebulizer is one of the standard configurations. This rugged combination provides the best results for a variety of elements and sample types. Nebulizers PerkinElmer offers these nebulizers for a wide variety of applications: Description/Part No. Uses/Advantages GemTip Cross-Flow...
Page 92 (MEINHARD) dissolved solids (less than 1%). Self- aspirating. Not to be used with solutions containing hydrofluoric acid. PerkinElmer offers two types, Meinhard K1 and K3, which are described below. All require an end cap (Part No. N0680343) for use with the Scott spray chambers.
Page 93 Sample Introduction System Figure 3-6. GemTip Cross-Flow nebulizer and end cap N0780546 (also shown in cross-sectional view).
Page 94 System Description Figure 3-7. GemCone nebulizer and end cap N0680504 (also shown in cross- sectional view).
Page 95: Peristaltic Pump
TubingSaver mode is a feature for extending the life span of pump tubing. Autosampler PerkinElmer offers autosamplers for automated sample handling. These autosamplers consist of a sample table, a sample tray, and a motorized sampling arm with an attached probe. Different sample trays are available for each...
Page 96: System Initialization And Setup
System Description autosampler, covering a variety of sample volumes and total sample capacity requirements. System Initialization and Setup Interlocks Interlocks are designed to ensure operator safety and protect the instrument from damage. The main system interlocks are described below. The following interlocks must be satisfied in order to ignite the plasma. If any of these interlocks is interrupted while the plasma is on, the plasma will automatically be shut down.
Page 97: Hardware Setup And Optimization
System Initialization and Setup Hardware Setup and Optimization The following hardware settings are controlled by the software. • RF Power: Power levels can be adjusted in 1-watt increments. • Plasma and auxiliary argon flow rates: Flow rates can be automated during the analysis with specific flow rates for each element if desired.
Page 98: How The Echelle Spectrometer And Scd Work
ICP emission lines. Random access to data for individual emission lines ensures rapid analysis. The Avio 500 is a dual detector system. The UV detector covers an extended ultraviolet wavelength range from 165 to 403 nm. The VIS detector covers the visible wavelength range from 404 to 782 nm.
Page 99 How the Echelle Spectrometer and SCD Work passes through the slit, it is collimated by the parabolic mirror and sent to the echelle grating. The echelle grating is a coarse grating with a ruling density of 79 lines/mm. It is precisely ruled with broad flat grooves.
Page 100: Uv Module
The UV module consists of a cross disperser, a camera sphere, a fold flat mirror, a field flattener, and the detector module. On the Avio 500 the overlapping orders from the echelle grating are sent to a Schmidt cross disperser.
Page 101 Light passing through the opening in the center of the optic becomes the visible channel. The Avio 500, the visible light is directed to a VIS detector. Second, the front surface of the Schmidt Cross Disperser is a coarse grating with a ruling density of 374 lines/mm.
Page 102: Visible Module
System Description Third, the surface of the Schmidt Cross Disperser has a small waveform on it. This waveform corrects for the spherical aberrations generated by the camera sphere mirror. By correcting for these spherical aberrations, the UV channel has excellent optical throughput (f/2.5) and excellent resolution (0.006 nm at 200 nm).
Page 103 How the Echelle Spectrometer and SCD Work Figure 3-12. Segmented-array Charge-coupled-device Detector (SCD). The linear subarrays are positioned on the detector at x-y locations that correspond to the locations of the desired emission lines generated by the echelle spectrometer. The figure below shows a representation of the echelle pattern on the detector. The diffraction orders are positioned along the x-axis and the emission lines are positioned along the y-axis.
Page 104 System Description Figure 3-13. Representation of echelle pattern on the detector (every tenth or- der). Item Description Item Description Wavelength Within the Order High High Order Numbers High Wavelength Each linear subarray contains from 8 to 40 pixels. Each pixel is 25µm wide and approximately 100m in height.
Page 105 Electronic Processing of the Signal On the Avio 500 the detector consists of 235 subarrays. The subarray consists of three areas, the photosensitive area, the storage register and the output register (see the following figure). Surrounding this subarray is a “guard band” that prevents excessive charge from blooming onto any other subarray.
Page 106 System Description Item Description Output Register Address Lines Interface Logic Guard Band Output Electronics The next figure shows a cross-section of the detector. Photons strike the photosensitive register and are immediately converted to photoelectrons. These photoelectrons are pulled away from the surface and moved into the storage register where they are stored as an electrical charge.
Page 107: Emo Switch
EMO Switch EMO Switch The Emergency Off (EMO) switch is the illuminated red switch on the front of the instrument. If it is blinking slowly the instrument is in the middle of an ignition cycle. It blinks rapidly after the Emergency Off Switch is depressed. This is an indication that the switch has been depressed and to remind you to push the switch again to release it.
Page 108: Connections To Electrical, Gas, And Cooling Water Supplies
System Description Connections to Electrical, Gas, and Cooling Water Supplies All gas lines supplied with the instrument are 6.5m (20 ft.) long. Ensure Note that the gas connections are located in close range (within 6.5 m) to the instrument. Label reads... Use...
Page 109 Connections to Electrical, Gas, and Cooling Water Supplies Cooling Water O IN Tubing Chiller or cooling Connections (On (Part No. water supply (Red Tie Wrap) the right side or N0770341) the generator side of instrument) O OUT Tubing Chiller or cooling (Part No.
Page 110 System Description Figure 3-17. Electrical, gas, and cooling water connections on the instrument. Item Description Item Description Avio 500 Supply Customer Interface Instrument to 200-230, Single Phase with 20 AMP, IEC309-2 Instrument Coolant Out Chiller Instrument Coolant In Chiller Outlet...
Page 111 Connections to Electrical, Gas, and Cooling Water Supplies Figure 3-18. Ethernet connections Item Description Customer Interface Ethernet...
Page 112: Specifications
System Description Specifications ICP System Specifications Frequency: 40 MHz, free-running Output Power Stability: <0.1% Power Output: 2200 watts, computer-controllable in 1 watt increments. RF generator is located in the left side of the instrument for efficient use of laboratory space. RF Shielding: Meets all FCC requirements for RF emission.
Page 113: Sample Introduction System
Specifications flow automatically within the range of 0 to 2.0 liter/minute in 0.1 liter/minute increments. Nebulizer Argon Flow: Computer-controlled, using a mass flow controller, and is variable between 0.00 and 2.00 liter/minute in 0.01 liter/minute increments. Shear Gas: A compressed-air shear gas (18-25 liters/minute) is used to push the plasma plume out of the optical path, minimizing the impact of self-absorption in the cooler plasma plume.
Page 114: Spectrometer
160 mm echelle grating has 79 lines per mm and a blaze angle of 63.4 degrees. On the Avio 500, the cross disperser for the UV region is a grating (374 lines/mm) with Schmidt correction incorporated into its surface. The Schmidt correction performs aberration correction for the 400 mm radius camera sphere.
Page 115 C h a p t e r 4...
Page 117: Chapter 4: Installation
Installation Contact a PerkinElmer service engineer for assistance in installing or evaluating the system after moving. The Avio 500 weighs weighs 163 kg (359 pounds). If the instrument needs to be moved please contact PerkinElmer Service. A PerkinElmer Service Representative should install your system for the first time or help you in moving the system.
Page 118: Installation Summary
Installation Installation Summary The installation of the system is divided into the following steps: • Moving the Instrument • Connecting the Gases and Cooling Water • Connecting the System Components • Installing the Quick-Change Torch Module • Installing the Torch Module •...
Page 119: Moving The Instrument
Moving the Instrument Caution f moving the Avio 500 will subject the instrument to any freezing temperatures you must contact a PerkinElmer service engineer to assist you in the move. The PerkinElmer service engineer will flush all traces of cooling water from the RF generator to prevent freezing of RF generator components.
Page 120: Connecting The Gases And Cooling Water
Installation Connecting the Gases and Cooling Water After the instrument has been moved into its position, it can be connected to the various services in the laboratory. Connecting the Gases All gas hose connections use 1/4 inch Swagelok fittings. Note Use two wrenches when making Swagelok connections.
Page 121 Connecting the Gases and Cooling Water Figure 4-1. Pneumatic, water, shear gas, and cooling connections. Item Description Item Description Ar Supply Out (water Hose with White Tie Wrap) Air/ N 2 Shear Gas Supply Cooling Water N 2 Supply In (water Hose with Red Tie Wrap)
Page 122 Installation Connecting the Argon Supply Make sure that the required purity of the argon gas is 99.996% pure Caution otherwise the detector will be damaged. Use the following procedure to connect the argon supply. Gas delivery lines from the argon tank must be contaminant-free and not made of Caution plastic, although PTFE lines are acceptable.
Page 123: Connecting The Polyscience Chiller
An air hose with 1/4-in. Swagelok fittings at each end is supplied in the hose kit that is shipped with the instrument. A second air hose is included with the PerkinElmer Air Dryer Filter in the Installation kit (Part No. N0770432). The following procedure describes how to connect the PerkinElmer air compressor, filter and regulator.
Page 124 Installation The PolyScience is available through PerkinElmer in the following two configurations: 208/230V, 60 Hz 220/240V, 50 Hz Connecting the Chiller to the Instrument Teflon tape (PTFE tape) should be used for all pipe-thread Note (NPT) fittings. Use of Teflon tape can prevent leaks.
Page 125 Connecting the Gases and Cooling Water Remote Chiller Connections The chiller can be turned on or off via the software. Your service engineer will connect the Remote Cable (Part No. N0770175) from the chiller to the instrument so that the chiller can be operated remotely. See the following figure for the location of the cable connections.
Page 126 Installation Figure 4-2. Remote chiller connections on the instrument. Item Description Item Description Avio 500 Instrument to 200-230, Single Phase with 20 AMP, IEC309-2 Remote Cable (Part No. N0770175) Chiller to Ethernet Connection Instrument Coolant Out Chiller Outlet Instrument Coolant In...
Page 127 Connecting the Gases and Cooling Water Figure 4-3. Ethernet Connections. Item Description Customer Interface Connections at the 5 and 7 Position...
Page 128: Filling The Polyscience Chiller
Initiating the software will have no effect on the chiller if the chiller is already on. If the Avio 500 Spectrometer is in Sleep or Standby mode and the instrument is still ignited, the chiller will remain on. If the instrument is not ignited in Sleep or Standby mode the chiller will turn itself off.
Page 129: Starting Up The Polyscience Chiller
Connecting the Gases and Cooling Water Figure 4-4. Filling the chiller. Item Description Reservoir Plug Detail Starting Up the PolyScience Chiller ® Check the following before starting up the PolyScience WhisperCool Chiller: • All plumbing connections are tight. • The chiller reservoir is full. •...
Page 130: Connecting The System Components
Note compromise instrument communication. • The Avio 500 is equipped with an IEC 309 250 V 16/20A 2 pole plus protective earth plug (PerkinElmer Part No. 09997530) that inserts into an equivalent IEC 309 series receptacle (see Section 2, Electrical Requirements).
Page 131 Connecting the System Components Caution Risk of damage to the instrument. Make sure that signals from accessories connected to the instrument connector do not exceed: Vmax = 30 V AC, Imax = 0.5 A AC Vmax = 30 V DC, Imax = 2 A DC Attention Risque d'endommagement de l'instrument.
Page 132 Installation Figure 4-5. System Component Connections Item Description Item Description Avio 500 Connection from Computer to Printer Autosampler Connection from Computer to Autosampler Computer Connection from Computer to USB/Ethernet Printer Connection from Autosampler to Customer Interface...
Page 133: Connecting The Usb Cable For The Plasmacamtm
Connecting the System Components Connecting the USB Cable for the PlasmaCam To be able to view the plasma from the ICP Syngistix software you need to attach the USB cable (Part No. 09290798) from the USB connection located on the lower left side of the instrument to the USB connection on your computer.
Page 134: Installing The Quick-Change Adjustable Torch Module
The Quick-Change Adjustable Torch Module is shipped pre-assembled as one unit. It includes the torch, spray chamber, injector, and nebulizer. Installing the Quick-Change Adjustable Torch Module Only use PerkinElmer Flat Plate Torch Glassware . Using any other Caution glassware will damage the torch.
Page 135 Installing the Quick-Change Adjustable Torch Module Figure 4-7 Replacing the torch. Item Description Item Description Torch Glass (Part No. N0790131) Spacer (Part No. N0791125) Torch Cutout O-Ring Color Code Blue (Part No. N0791334)
Page 136 Installation Item Description Item Description Knurled Nut (Part No. N0776027) Cassette (Part No. N0810214) Washer (Part No. N0776028) Stripe on Torch O-Ring (Part No. 09902223) After Index Mark on Torch Holder removing the torch the lower O-ring may move out of position. Make sure to push the lower O-ring all the way down on the ledge it rests on before you return the torch glassware.
Page 137 Installing the Quick-Change Adjustable Torch Module...
Page 138 Installation Figure 4-8 Torch Assembly. Item Description Item Description Knurled Nut (Part No. N0776027) O-Ring (Part No. 09902207) Injector 2mm Alumina (Part No. Cyclonic Injector Adapter (Part N0791183) No. N0790143) O-Ring Color Coded Blue (Part No. Scott Injector Adapter (Part No. N0791333) N0790143) Lock Collar (Part No.
Page 139 Installing the Quick-Change Adjustable Torch Module 1. Open the torch compartment door. 2. Take the torch cassette body and insert the o-ring, and then the PEEK sleeve (spacer) into it. Ensure that the hole on the PEEK sleeve lines up with the top hole on the torch cassette body.
Page 140 Installation 4. Make sure the holes between the PEEK sleeve and the torch cassette body line up when fully inserted. The holes must line up and be empty, and the PEEK sleeve should not be visible. You can use a small flashlight to determine that the holes are visible once the color is pushed in all the way.
Page 141 Installing the Quick-Change Adjustable Torch Module Figure 4-11 Incorrect and Correct Position of the Peek Sleeve Item Description Incorrect positioning of the top of the PEEK sleeve. There is not enough room for additional pieces to be installed and even if all pieces are forced together, the torch glassware will not be air tight and the plasma will not ignite or will be unstable.
Page 142 Installation hen installing the Torch Module in the next steps, do so carefully so you will avoid breaking the torch and risking possible injury. Warning Avertissement: Lors de l'installation du module de la flamme dans les prochaines étapes, faire avec soin afin que vous éviter de casser la torche et un risque de blessure possible.
Page 143 Installing the Quick-Change Adjustable Torch Module Once the knurled nut is tightened the torch glassware should be tight. It should not Note be possible to twist it easily. If it is not tight, o-ring #5 in Figure 4-7 on page 133 is probably not fully seated in the torch body.
Page 144 Installation 11. Line up the black line on the torch cassette body with the pin on the instrument. Figure 4-14 Lining up the black line with the locking pin Item Description Sample Compartment Black Locking Pin Black Line for Alignment...
Page 145 Installing the Quick-Change Adjustable Torch Module 12. From the bottom of the sample compartment carefully insert the torch cassette. Figure 4-15 Inserting the torch Item Description Item Description Torch Compartment Plasma induction plates Torch Injector...
Page 146 Installation Wear gloves when you handle the torch glassware. Caution Attention Portez des gants lorsque vous manipulez la verrerie de la torche. 13. Push the torch up carefully through the flat induction plates until the torch cassette body is fully inserted. Figure 4-16 Inserting the torch Item...
Page 147 Installing the Quick-Change Adjustable Torch Module 14. As you push the torch into position make sure that the slot on the torch is facing the radial purge window. Figure 4-17 Location of slot on torch Item Description Torch Slot Radial purge window...
Page 148 Installation 15. Once the torch cassette is in the proper position go back to the sample compartment and push in the black locking pin. This will lock the torch cassette into position Figure 4-18 Location of locking nut Item Description Sample compartment Black locking pin 16.
Page 149 Installing the Quick-Change Adjustable Torch Module Figure 4-19 Installing the torch into the sample compartment. Item Description Item Description Inside of the Torch Compartment Ignitor Contact Plastic Air Vent Tube Ignitor Cable...
Page 150: Connecting The Scott Spray Chamber
Installation Item Description Item Description Axial Flat Optic Plasma Gas Connection Radial Purge Window Aux Gas Connection Torch Shear Gas Connection Connecting the Scott Spray Chamber 1. After the torch and injector are installed, attach the Scott chamber clip assembly to the bottom of the injector adapter. 2.
Page 151 Connecting the Scott Spray Chamber 3. Find the shelf located on the Scott spray chamber clip assembly. Figure 4-21 Location of Shelf on Scott Spray Chamber Clip Assembly 4. Add the Scott spray chamber clip to the injector. 5. Make sure that the Scott spray chamber clip rests securely on the injector shelf.
Page 152 Installation Figure 4-22 Scott Spray Chamber Clip Assembly in Place...
Page 153 Connecting the Scott Spray Chamber 6. With the Scott spray chamber clip assembly handle open insert the bottom of the injector adapter into the opening of the Scott spray chamber. Figure 4-23 Scott Spray Chamber Clip Assembly Open Item Description Scott Spray Chamber in Place Scott Spray Chamber Assembly open Opening in Scott Spray Chamber...
Page 154 Installation 7. Close the clip by pulling it up. This secures the Scott spray chamber into the injector and seals the o-rings. Figure 4-24 Scott Spray Chamber Clip Assembly Closed Item Description Scott Spray Chamber in Place Scott Spray Chamber Assembly closed 8.
Page 155: Connecting The Nebulizer (Neb) Tubing
Connecting the Scott Spray Chamber 10. The Scott system is now fully installed. Figure 4-25 Scott Spray Chamber Installed Connecting the Nebulizer (NEB) Tubing To connect the nebulizer (NEB) tubing follow these steps and refer to the next figure. 1. Connect the end of the nebulizer (NEB) argon tubing to the nebulizer end cap and the other end to the quick disconnect by pushing the male quick connect fitting into the quick disconnect.
Page 156 Installation 2. Make sure that the Teflon tubing is in good condition. Replace the tubing if necessary. Connect the sample capillary tubing to the nebulizer sample inlet. Figure 4-26 Nebulizer connections Item Description Item Description Sample compartment Neb tubing Nebulizer end cap Quick Connect 3.
Page 157: Connecting The Cyclonic Spray Chamber
Connecting the Cyclonic Spray Chamber Connecting the Cyclonic Spray Chamber Handle the cyclonic spray chamber carefully to avoid breaking the glassware and possible injury. Warning Avertissement: Manipuler avec soin la chambre de nébulisation cyclonique pour éviter de casser la verrerie et des blessures. 1.
Page 158 Installation 2. With one hand carefully holding on to the base of the cyclonic spray chamber, and with the other hand holding the clip, attach the clip to the bottom of the injector adapter and the top of the spray chamber. See the following figure. Figure 4-27 Installing the Cyclonic Spray Chamber Item...
Page 159 Connecting the Cyclonic Spray Chamber 3. The following figure shows the cyclonic spray chamber in place. 4. The white spacer should be installed around the neck of the nebulizer. See the following figure. The white spacer puts the nebulizer in a position for good intensity and precision.
Page 160: Setting The Torch Position
Installation Setting the Torch Position After you have installed the torch and spray chamber you will need to set the torch position to get optimal performance. In most cases the optimal position is -3. For more information on Setting Note Instrument Parameters see page 182.
Page 161 Setting the Torch Position 2. Raise or lower the inner adjustment plate to either a positive or negative value. In the following figure, the inner adjustment plate needs to be raised until the horizontal black line is just below the -3 to reach the optimal, desired position. Figure 4-29 Setting the Position Item...
Page 162: Installing The Autosampler
Locking Into Position Item Description Latch Closed Locking Pin Inner Adjustment Plate in Place Installing The Autosampler The instrument can be used with the PerkinElmer S10 Autosamplers. The following procedures describe the electrical connections necessary to install the PerkinElmer autosamplers.
Page 163 Installing The Autosampler After the autosampler is installed, the software must be configured for the type of autosampler you are using. This can be done during the software installation or, in the ICP software, by selecting the Configure Autosampler command from the System menu.
Page 164 2. Place the autosampler adjacent to the spectrometer. The best location for the autosampler is to the right of the torch enclosure. See the following figure. Figure 4-32 Electrical connection for the S10 autosampler to the Avio 500 Item Description...
Page 165 Installing The Autosampler 3. Connect the RS232 serial communication cable provided (Part No. 09290259), between the Com 1 port on the underside of the autosampler (as shown in Figure 4-11 page 161 ) and one of the Com ports on the PC. 4.
Page 166: Fitting And Connecting The Autosampler Sampling Probe
Installation Fitting and Connecting the Autosampler Sampling Probe When you fit the sampling probe, take care not to press forcefully Caution in any direction on the autosampler arm since this can damage the arm. The sampling probe is a complete assembly. Do not attempt to take the probe apart as this will damage it, and reassembly is not possible.
Page 167: Fitting The Sampling Probe
Fitting and Connecting the Autosampler Sampling Probe Fitting the Sampling Probe 1. If not already done, carefully insert the sampling probe guide from above into the sampling probe holder on the autosampler arm and push it down fully, as shown in the following figure. 2.
Page 168 Installation Figure 4-33. Inserting the sampling probe. Item Description Sample Tube Holder O-Ring About 20 mm Sampling Probe Tower Sampling Probe Guide...
Page 169: Adjusting The Sampling Probe Height
Fitting and Connecting the Autosampler Sampling Probe Adjusting the Sampling Probe Height The procedure described below assumes that you are using a spectrometer Note operated via ICP Syngistix software. If you are using an AA or ICP-MS instrument, please refer to the information on operating an autosampler in the on-line help for the respective instrument.
Page 170 Installation 6. To remove the sample rack, first select Instrument tab->Load Tray to raise the sampling probe, then remove the rack. Figure 4-34. Inserting the sampling probe. Item Description Sampling Probe Rinsing Probe This completes installation of the sampling probe. For detailed information on adjusting the sample probe height and connecting the sample tube between the sample probe and the spectrometer’s sample input system see the S10 Autosamplers User’s Guide (Part No.
Page 171: Setting The Torch Viewing Position
Setting the Torch Viewing Position Setting the Torch Viewing Position This procedure adjusts the torch viewing position for the highest signal intensity. Perform this procedure when: • the instrument or software is first installed • the instrument is moved to a new location •...
Page 172: Switching On The System
Installation Select Manganese, which is typically used as the alignment wavelength for the majority of analyses. -or- Select another element from the drop-down list. This feature is for specialized analyses where you want to optimize the intensity for an individual analyte of interest. This may adversely affect the intensities of other analytes.
Page 173: Instrument Start-Up
Instrument Start-up • Air/N Shear gas: 5.5 to 8.25 bar or 80-120 psig. • gas: 2.75 to 8.25 bar or 40-120 psig. 3. Make sure that the torch is correctly installed, the torch compartment door is shut, and the EMO switch is released. 4.
Page 174: Automatically Aligning The Torch Viewing Position
Installation Automatically Aligning the Torch Viewing Position This procedure adjusts the torch viewing position for the highest signal intensity. Perform this procedure when: • the instrument or software is first installed • the instrument is moved to a new location •...
Page 175: Detector Calibration
Automatically Aligning the Torch Viewing Position 11. Select the element and wavelength. This is the wavelength that the system will use to measure the intensities at different viewing positions and locate the position that gives the highest intensity. Your options are: Select Manganese, which is typically used as the alignment wavelength for the majority of analyses.
Page 176: Wavelength Calibration
100 mg/L of P, K, S; and 20 mg/L of As, La, Li, Mn, Mo, Ni, Sc, Na.  VIS Wavecal mix (Part No. N9302946) available through PerkinElmer, which contains 1 mg/mL Ba, Ca; and 10 mg/L of La, Li, Mn, Na, Sr; and 50 mg/L of ...
Page 177 If these specifications are not met, repeat the wavelength calibration and make sure all peaks can be seen in the Spectra Display window. If these specifications are still not met, a complete optical alignment may be required. Contact a PerkinElmer Service Representative.
Page 178: Setting Instrument Parameters
If these specifications are not met, repeat the wavelength calibration and make sure all peaks can be seen in the Spectra Display window. If these specifications are still not met, a complete optical alignment may be required. Contact a PerkinElmer Service Representative.
Page 179: Instrument Settings For Aqueous Solutions
Setting Instrument Parameters • To compensate for spectral interferences, use Background Correction, Interelement Correction (IEC), or Multi-component Spectral Fitting (MSF). Confirm using interference check standards. • To compensate for matrix effects, use internal standardization. Instrument Settings for Aqueous Solutions For Cross-Flow Nebulizers Aqueous Nebulizer Flow: 0.6 L/min...
Page 180 Installation Instrument Settings for Organic Solutions Parameter Baffled Cyclonic Spray Chamber, Low-Flow GemCone Nebulizer and 1.2 mm Injector 1500 Watts RF power 0.35 L/min Nebulizer Flow 0.6 L/min Auxiliary Flow 10 L/min Plasma Flow 1.0 to 4.0 mL/min Sample Flow Rate 15 s Equilibration Time Torch Position...
Page 181: Important Considerations For Dual Viewing
Setting Instrument Parameters There is a three slot torch for organics (Part No. N0790249) that can be ordered. This is the best torch to use for axial viewing for samples with organics or high dissolved solids. Using the long torch will extend the torch life since the long torch does not have a slot.
Page 182: Hardware Settings And Options
Removing and Cleaning the Windows on page 232. • PerkinElmer offers different types of nebulizers for a wide variety of applications. For descriptions of the nebulizers and their different uses and advantages, see Nebulizers on page 254.
Page 183: Shipping Lists
Shipping Lists Shipping Lists Every day you count on PerkinElmer to provide you with solutions that deliver reliable performance, control operating costs and maximize operational time. Our complete portfolio of consumables, parts, supplies, training and service helps you meet both routine and demanding measurement challenges. We invest heavily in testing and validating our products to ensure you receive guaranteed compatibility and performance - on-time, every time, for every instrument in your laboratory.
Page 184 Installation Part No. Description Quantity N0810439 O-Ring DV Spares Kit N0810607 Torch Assembly- Cyclonic Spray Chamber N0811234 Shipping Pack N0810110 Instrument Assembly N0790434 Spares Kit Table 4-3. Installation Kit (Part No. N0810432) Part No. Description Quantity 09200486 Drain Bottle (Carboy 15 Liter) 09936225 ICP-OES Instrument Maintenance Log Book N0690271...
Page 185 Shipping Lists Table 4-4. Spares Kit (Part No. N0790433) Part No. Description Quantity 00473550 Solvent Flex Pump Tubing, 0.76 mm ID, (Black/Black-Sample Tubing) 02506516 Tygon Tubing 1/4 in. OD x 1/8 in. ID 0.98 feet 02506532 Organic Drain Tubing 0.63 feet 09902033 O-Ring for Cross Flow Nebulizer End Cap 09903730...
Page 186 Installation Part No. Description Quantity 09995098 Air Filter for Spectrometer N0582325 ICP Concepts Book N0695414 Drain Adapter N0790131 Quartz Torch (standard single slot torch) N0790437 O-Ring Kit for the Dual View Torch Peri- scope N0790438 O-Ring Kit for Injector Adapter N0791183 Alumina Injector, 2.0 mm ID Table 4-5.
Page 187 Shipping Lists Part No. Description Quantity 09920267 Barb Fitting Male 10-32 UNF 09920865 Coupler 3/32 Tubing 09921045 O-Ring 0.126 ID x 0.040 WD (For Cross- Flow Nebulizer GemTips 09923037 Solvent Flex Tubing, 1.14 mm ID, Red/Red (Drain Tubing) 09923383 Cap Sleeve 0.406 in. (Brown Vinyl) 09985708 PFTE Tubing, 0.031 x 0.016 10 feet...
Page 188 Description Documentation N0582325 Concepts, Instrumentation and Techniques in ICP-OES (Book) 09936225 ICP-OES Instrument Maintenance Log Book 09931200 Avio 500 Hardware Guide 09931199 Avio 500 Unpacking Instructions N0788003 Syngistix ICP Document Pack CD Software: N0788003 CD-ROM ICP Syngistix Software Peristaltic Pump Tubing 09908585 PVC Pump Tubing, 1.14 mm ID, Red/Red (Drain Tubing)
Page 189 Shipping Lists Table 4-6. Spares Available (Continued) Part No. Description N0773115 Viton Pump Tubing, 1.14mm ID, Red/Red (Drain tubing) N0773118 Viton Pump Tubing, 0.76mm ID, Black/Black (Sample tub- ing) Nebulizer and Related Parts N0780546 GemTip Cross-Flow II Nebulizer N0780676 Gem Tip Kit for Cross-Flow II Nebulizer N9300067 Gem Tip Cross-Flow Nebulizer 0-Ring Kit N0770358...
Page 190 Installation Table 4-6. Spares Available (Continued) Part No. Description N0777460 Nebulizer Clip for MEINHARD® Nebulizers N0777219 PolyPro ST Nebulizer N0777049 PFA-ST Nebulizer N0777676 PFA-ST3 Microflow Nebulizer N0775330 PEEK Mira Mist Nebulizer (0.2 to 2.5 mL/min) N0775331 PEEK Mira Mist Nebulizer (0.02 to 2.5 mL/min) N0775332 Ari Mist (0.05 to 1.0 mL/min) N0775333...
Page 191 Shipping Lists Table 4-6. Spares Available (Continued) Part No. Description N0691709 CETAC U-6000AT+ Ultrasonic Nebulizer System, 115V, 50/ 60 Hz N0691710 CETAC U-6000AT+ Ultrasonic Nebulizer System, 230V, 50/ 60 Hz N0690770 Dry Aerosol Adapter Spray Chamber and Related Parts N0791352 Cyclonic Spray Chambers Baffled Cyclonic (Standard) N0790373 HF Resistant Cyclonic Spray Chamber TFE PTFE O-Ring...
Page 192 Installation Table 4-6. Spares Available (Continued) N0791189 Quartz Injector, 2.0mm ID, 150 mm LG N0791188 Quartz Injector, 1.6 mm ID, 150 mm LG N0791187 Quartz Injector, 1.2 mm ID, (1.2 mm entire length of tube) N0791186 Quartz Injector, 1.2 mm ID N0791185 Quartz Injector, 0.80 mm ID N0791184...
Page 193 Shipping Lists Table 4-6. Spares Available (Continued) Purge System Parts Part No. Description 09992731 Axial Purge Window N0810346 Radial Purge Window N0810194 Axial Mirror Kit Optical Kit (includes windows and O-rings see below) N0810439 09210598 O-Ring 0.799 ID 0.103WD Teflon 50 DUR 09902131 O-Ring 1.171 ID 0.139WD 09921058...
Page 194 Cyclonic Injector Adapter O-Ring Kit N0790441 Scott Injector Adapter O-Ring Kit N0790440 Miscellaneous 09290332 Ethernet Cable Assembly N0811592 Avio 500 Drip Tray 09406322 Network Card N0790212 Peristaltic Pump Assembly N0776200 Chiller Coolant Mix 30 Plus-Five 1/2 Gallons 09220410 O-Ring Removal Tool...
Page 195 Shipping Lists Table 4-6. Spares Available (Continued) 09290798 USB Cable...
Page 196 Installation...
Page 197 C h a p t e r 5...
Page 199: Chapter 5: Maintenance
You should perform only the maintenance procedures described in this chapter. Record your daily maintenance procedures in the ICP-OES Maintenance Log (Part. No. 09936225). If additional maintenance is required, contact a PerkinElmer service engineer. This instrument requires no specified inspection or preventive maintenance to ensure the continuous functioning of its safety features.
Page 200: Daily Checks
Nitrogen output pressure: 275-825 kPa (40-120 psig) Shear Gas Supply The Avio 500 requires a supply of shear gas. The shear gas used is typically compressed air; however, nitrogen may also be used. Make sure that an adequate supply of shear gas is available and connected to the system. Check that the supply has sufficient pressure, and that a spare cylinder is ready if necessary.
Page 201: Chiller
Daily Checks Chiller Fill the reservoir up with the coolant fluid with inhibitor (Part No. N0776200). The chiller reservoir has a capacity of 4.2 liters (1.1 US gallons). Cooling water pressure: 310-550 kPa (3.1 to 5.5 bar or 45-80 psig) Vent Check that your vent system is switched on and is not blocked.
Page 202: Nebulizer
Maintenance When the humidity in your lab is high, water can condense on the plasma Caution induction plates when the torch is not in operation. To prevent damage to the plasma induction plates, use a soft dry cloth to gently dry the plasma induction plates before igniting the torch.
Page 203: Periodic Checks
The plasma induction plates must be kept clean to prevent arcing across the plasma induction plates. Inspect the plasma induction plates for any deformations or carbon buildup. Contact your PerkinElmer Service Representative to replace the plasma induction plates if there are any signs of pitting. Pitting causes weakness in the plasma induction plates which can result in a hole in the plasma induction plates and a gas leak.
Page 204: Purge Viewing Window/Tubes
Maintenance Purge Viewing Window/Tubes Remove and examine the window or purge tube for deposits. If you notice a drop in UV performance clean or replace the windows. Clean according to the instructions given later in this chapter or replace as necessary. Nebulizer Check the nebulizer spray pattern with deionized water.
Page 205: Torch Viewing Position Alignment
Periodic Checks Do not use deionized or tap water in the chiller. Only use coolant fluid Caution that includes inhibitor (Part No. N0776200). Ne pas utiliser déminéralisée ou l'eau du robinet dans le refroidisseur. Attention Utiliser uniquement du fluide de refroidissement qui comprend un inhibiteur (N0776200).
Page 206: Cleaning The Sample Introduction System
Maintenance Cleaning the Sample Introduction System See the following table for the recommended cleaning procedures for the sample introduction system. Table 5-1. Recommended Cleaning Procedure Daily cleaning After analyzing aqueous solutions, flush with deionized water, or 2% nitric acid, followed by deionized water.
Page 207: Quick-Change Adjustable Torch Module
Quick-Change Adjustable Torch Module Table 5-1. Recommended Cleaning Procedure (Continued) Spray Chamber By handling the spray chamber oil and dirt can accumulate on it and this will affect performance. To assure proper wetting wipe the spray chamber with acetone to remove all oils and dirt. Pump Head Remove and clean with water or a mild solvent.
Page 208: Plasma Torch
Maintenance Plasma Torch Caution Only use PerkinElmer Flat Plate Torch Glassware . Using any other glassware will damage the torch. Utiliser uniquement PerkinElmer Plate Flat Torch Glassware Attention L'utilisation de tout autre verrerie endommager la torche. The plasma torch assembly is comprised of a quartz torch with an inner quartz tube, injector, and adapter for securing the injector into an inlet in the spray chamber.
Page 209 Quick-Change Adjustable Torch Module Figure 5-1. Quartz Torch. Item Description Plasma Induction Plates Torch...
Page 210: Plasma Induction Plates
Maintenance Plasma Induction Plates Regularly inspect the plasma induction plates. They should not show any signs of deforming or pitting. If your lab has high humidity, check the plasma induction plates to make sure they are dry. Use a soft dry cloth to dry the plasma induction plates if necessary. To replace and adjust the plasma induction plates refer to the procedure, see Replacing the Plasma Induction Plates on page 230.
Page 211: Removing And Disassembling The Torch
Quick-Change Adjustable Torch Module 3. Rotate the injector adapter to the left, then pull gently down - when the locking pin is out and you apply pressure, the whole torch body could come out. Figure 5-2 Removing the spray chamber assembly and injector. Item Description Scott spray chamber...
Page 212 Maintenance 2. From the sample compartment remove the spray chamber. See Removing the Scott Spray Chamber on page 222 or Removing the Cyclonic Spray Chamber on page 226. 3. Open the torch compartment door. When installing the Torch Module in the next steps, do so carefully so you will avoid breaking the torch and risking possible injury.
Page 213 Quick-Change Adjustable Torch Module 5. Carefully slide the torch holder through the plasma induction plates and out of the instrument. Figure 5-4 Lowering the Torch Item Description Item Description Torch Compartment Torch Plasma Induction Plates Injector...
Page 214 Maintenance Wear cotton gloves when you handle the torch glassware. Caution Attention Porter des gants de coton lorsque vous manipulez la verrerie de la torche. 6. Inspect the glassware. If damaged the glassware will have to be removed from the torch cassette. 7.
Page 215 Quick-Change Adjustable Torch Module n the next step, be sure to carefully remove the torch so you will avoid breaking the glassware and risking possible injury. If the torch does break, discard the broken torch and replace. Remove the knurled nut, Warning sleeve and washers on the torch mounting shaft to make sure that all glass fragments are removed.
Page 216 Maintenance 11. If the O-rings need to be removed, use your gloved finger to remove them using the O-ring removal tool (Part No. 09220410). Do not use a knife blade because the blade will cut the O-rings and damage the O-ring seats. Replace with new O-rings.
Page 217 Quick-Change Adjustable Torch Module...
Page 218 Maintenance Figure 5-7 Torch Assembly Item Description Item Description Knurled Nut (Part No. N0776027) O-Ring (Part No. 09902207) Injector 2mm Alumina (Part No. Cyclonic Injector Adapter (Part N0791183) No. N0790143) O-Ring Color Coded Blue (Part No. Scott Injector Adapter (Part No. N0791333) N0790143) Lock Collar (Part No.
Page 219: Cleaning The Torch
Quick-Change Adjustable Torch Module Cleaning the Torch The torch components should be cleaned regularly to remove accumulated deposits. After prolonged use, a torch may lose its transparency and become crystalline. In this condition, called devitrification, the torch is very fragile. You should not attempt to clean a devitrified torch, but it can still be used.
Page 220: Replacing The Torch
Maintenance O-rings may be cleaned with soap and water. An ultrasonic bath may be used. Replace if cracked or worn. A torch O-ring kit is available. See the list of replacement parts later in this section. The dark blue torch O-ring (Part No. N0791334) on the outside of the torch Note and the dark blue O-ring on the outside of the injector adapter (Part No.
Page 221 Quick-Change Adjustable Torch Module Figure 5-8 Replacing the Torch Item Description Item Description Torch Glass (Part No. N0790131) Spacer (Part No. N0791125) Torch Cutout O-Ring Color Code Blue (Part No. N0791334)
Page 222: Replacing The Torch On The Mount
The following steps describe how to replace the torch in the mount. Refer to the next two figures. Caution Only use PerkinElmer Flat Plate Torch Glassware . Using any other glassware will damage the torch. Utiliser uniquement PerkinElmer Plate Flat Torch Glassware Attention L'utilisation de tout autre verrerie endommager la torche.
Page 223 Quick-Change Adjustable Torch Module Before installing the Quick-Change Adjustable Torch Module in the sample compartment, check that the plasma induction plates are in place. 1. If the plasma was on, turn off the plasma. If the plasma has been on, the torch glass will be very hot and can cause serious burns.
Page 224: Scott Spray Chamber
Maintenance When installing the Torch Module in the next steps, do so carefully so you will avoid breaking the torch and risking possible injury. Avertissement: Lors de l'installation du module de la flamme dans les Warning prochaines étapes, faire avec soin afin que vous éviter de casser la torche et un risque de blessure possible.
Page 225 Scott Spray Chamber 3. Disconnect the sample tubing from the nebulizer inlet. Check that the tubing is in good condition and replace if necessary 4. Disconnect the nebulizer argon fitting from the gas fitting on the quick disconnect. 5. Open the Scott spray chamber clip assembly that holds the spray chamber in place.
Page 226: Removing The End Cap From The Spray Chamber
Maintenance 7. Replace with a new Scott spray chamber. For the full installation procedure see Connecting the Scott Spray Chamber on page 148. Removing the End Cap from the Spray Chamber 1. Loosen, but do not remove, the two knurled screws in the nebulizer end cap. Support the spray chamber with one hand as you twist the end cap and end cap ring, together, off the spray chamber.
Page 227: Cleaning The Scott-Type Spray Chamber
Scott Spray Chamber Figure 5-10 Spray chamber, end cap, and associated parts. (Illustration shows cross-flow nebulizer end cap assembly, Part No. N0780546.) Item Description Scott Spray Chamber (Part No. N0790384) O-Ring (Part No. 09902033) End Cap Ring (Part No. 00473543) End Cap (Part No.
Page 228: Replacing The Scott-Type Spray Chamber
Maintenance manufacturer's safety recommendations. These recommendations are normally provided in a material safety data sheet (MSDS) supplied with the chemical. If you have been analyzing organic solutions, the spray chamber can be cleaned using a solvent or diluted soap solution. Be sure to inspect the torch and injector daily for carbon buildup.
Page 229 Cyclonic Spray Chamber 2. With one hand carefully holding on to the base of the cyclonic spray chamber and with the other hand holding the clip disconnect the clip to remove the spray chamber from the injector. See the following figure. Figure 5-11 Installing the Cyclonic Spray Chamber Item...
Page 230: Etching The Cyclonic Spray Chamber
Maintenance Etching the Cyclonic Spray Chamber Hydrofluoric acid — toxic and corrosive. Hydrofluoric acid (HF) is toxic, extremely corrosive, and can cause severe burns. Hydrofluoric acid will readily burn skin, and if the fumes are inhaled, lung tissue. Burns may not be immediately painful Warning or visible.
Page 231: Cleaning The Cyclonic Spray Chamber
Cyclonic Spray Chamber Cleaning the Cyclonic Spray Chamber If you have been analyzing aqueous solutions, the spray chamber should be cleaned in an acid bath. An ultrasonic bath may be used. Start with a solution of 5% nitric acid or aqua regia and, if deposits persist, increase the acid concentration, up to 20% if necessary.
Page 232: Replacing The Plasma Induction Plates
If your lab has high humidity, check the plasma induction plates to make sure they are dry. Use a soft dry cloth to dry the plasma induction plates if necessary. Contact your PerkinElmer Service Representative to replace and adjust the plasma induction plates.
Page 233 Replacing the Plasma Induction Plates Table 5-3. Replacement Parts: Torch Module (Continued) N0791184 Sapphire Injector, 2.0 mm ID, 150 mm LG N0791185 Quartz Injector 0.8 mm ID N0791186 Quartz Injector 1.2 mm ID N0791187 Quartz Injector Straight 1.2 mm ID N0791188 Quartz Injector 1.6 mm ID N0791189...
Page 234: Windows
Maintenance Windows Removing and Cleaning the Windows If the plasma has been on, the torch will be very hot and can cause serious burns. Wait five minutes after turning off the plasma before you begin these maintenance procedures. Warning Avertissement: Si le plasma a été mis sur, la torche sera très chaude et peut causer des brûlures graves.
Page 235: Removing And Replacing The Windows
Windows Removing and Replacing the Windows These windows are important parts of the optical system. Handle them Caution carefully, as you would any sensitive optical component. Do not directly touch the windows. Always remove the axial window before the radial window and refit the radial window before the axial window.
Page 236 Maintenance If the plasma has been on, the torch glass will be very hot and can cause serious burns. Wait five minutes after turning off the plasma before you begin these maintenance procedures. Warning Avertissement: Si le plasma a été mis sur le verre de la torche sera très chaude et peut causer des brûlures graves.
Page 237 Windows 3. Use the special removal tool to grip the sides of the ring that holds the axial purge window in place. 4. With the tool in place rotate the tool to the left to loosen the retaining ring. Figure 5-13 Removing the Axial Purge Window Item Description...
Page 238 Maintenance 7. Remove the Axial Purge window. Figure 5-14 Removing the Axial Purge Window Item Description Retaining Axial Purge Window Ring Rubber O-Ring Axial Purge Window 8. Lift the axial window and ring out of the mount — take care if the spectrometer purge is set to high and you have not removed the axial window —...
Page 239 Windows 14. Use the tool to tighten down the stainless steel ring and axial purge window into place. 15. Turn on the plasma. Removing and Returning the Radial Purge Window Do not leave finger marks on the window. Use an optical cloth to handle Caution the window.
Page 240 Maintenance Tool Required: • Purge window aluminum ring removal tool (Part No. N0790448) 1. Turn off the plasma. 2. In order to gain access to the Radial Purge window you must remove the Shear Gas Nozzle. See Removing the Shear Gas Nozzle on page 242. If the plasma has been on, the torch glass will be very hot and can cause serious burns.
Page 241 Windows 3. Locate the radial purge window in the torch compartment. Figure 5-15 Location of Radial Purge Windows Item Description Radial Purge Window (Part No. N0810346) 4. Use the special removal tool to grip the sides of the ring that holds the radial purge window in place.
Page 242: Cleaning The Windows
Maintenance 5. With the tool in place rotate the tool to loosen the stainless steel ring. 6. With the ring now loosened carefully unscrew the radial purge window mount the rest of the way by hand. 7. Remove the ring that holds the radial purge window in the mount 8.
Page 243: Replacing And Adjusting The Shear Gas Nozzle
Replacing and Adjusting the Shear Gas Nozzle 1. Rinse the windows thoroughly with deionized water. 2. To remove more stubborn marks: Soak the windows in warm, 40°C, 10-20% nitric acid for one hour. Rinse the windows thoroughly with deionized water. 3.
Page 244: Removing The Shear Gas Nozzle
Maintenance Removing the Shear Gas Nozzle Figure 5-16 Location of Shear Gas Nozzle Item Description Item Description Shear Gas Nozzle T10 Screw Location T20 Screws Location Torch Slot Bracket...
Page 245 Replacing and Adjusting the Shear Gas Nozzle 1. Turn off the plasma. If the plasma has been on, the torch glass will be very hot and can cause serious burns. Wait five minutes after turning off the plasma before you begin these maintenance procedures. Warning Avertissement: Si le plasma a été...
Page 246 Maintenance 3. Remove the Radial Purge tube. See Removing and Returning the Radial Purge Window on page 237. Figure 5-17 Removing the Radial Purge Tube Item Description Radial Purge Tube Bracket Screw Removed...
Page 247: Returning The Shear Gas Nozzle
Replacing and Adjusting the Shear Gas Nozzle 4. Use a T20 screwdriver to remove the two top bracket screws and use a T10 screwdriver to loosen the bottom bracket screw that secure the shear gas nozzle in place. Figure 5-18 Removing the Shear Gas Nozzle Item Description...
Page 248 Maintenance 1. Place the shear gas assembly back into position. 2. Use a T20 screwdriver to secure the two top bracket screws and use a T10 screwdriver to tighten the bottom bracket screw to secure the shear gas nozzle in place. See Figure 5-16. 3.
Page 249: Remove And Replacing The Axial Heat Sink Cooling Tube
Remove and Replacing the Axial Heat Sink Cooling Tube Remove and Replacing the Axial Heat Sink Cooling Tube 1. Turn off the plasma. If the plasma has been on, the torch glass will be very hot and can cause serious burns. Wait five minutes after turning off the plasma before you begin these maintenance procedures.
Page 250 Maintenance 2. Locate the Axial Heat Sink Cooling Tube in the torch compartment. Figure 5-19 Location of Axial Heat Sink Cooling Tube Item Description Axial Heat Sink Cooling Tube...
Page 251: Removing And Replacing The Axial Flat Optic
Removing and Replacing the Axial Flat Optic 3. Slowly and carefully twist out towards the front of the instrument the Axial Heat Sink Cooling Tube. 4. Slowly and carefully twist in the new Axial Heat Sink Cooling Tube into place. Removing and Replacing the Axial Flat Optic You may need to remove and replace the Axial Flat Optic if you notice reduced Axial sensitivity or counts.
Page 252 Maintenance 3. Remove the thumbscrew on the heat sink cover. See the following figure. Figure 5-20 Location of Axial Heat Sink Cooling Tube Item Description Axial Heat Sink Cooling Tube Pushed to the Right Thumbscrew...
Page 253 Removing and Replacing the Axial Flat Optic 4. Slide back the sheet metal and lift up. Figure 5-21 Removing Heat Sink Cover Item Description Heat Sink Cover Heat Sink...
Page 254 Maintenance 5. Disconnect the Axial Flat Optic Temperature Sensor from the instrument. Figure 5-22. Axial Flat Optic Temperature Sensor 6. Use the 6mm Hex Mini Ratchet to remove the three threaded standoffs screws that secure the Axial Flat Optic in place. Wear powder free gloves to avoid contaminating the optics.
Page 255 Removing and Replacing the Axial Flat Optic 7. Install the new Axial Flat optic and secure with the three screws with the 6mm Hex Mini Ratchet. Figure 5-23 Location of Three Screws Item Description Heat Sink Screw Locations Heat Sink Screws...
Page 256: Nebulizers
Axial Heat Sink Cooling Tube on page 247. Nebulizers PerkinElmer offers different types of nebulizers for a wide variety of applications. For descriptions of the nebulizers and their different uses and advantages, refer to Chapter 3, System Description. Part numbers and replacement parts for the different types of nebulizers are listed on the next page.
Page 257 Nebulizers Table 5-5. Nebulizer Flow Rates Concentric Glass 0.70 L/min 0.4 - 1.3 L/min (MEINHARD) Type A Concentric Glass 0.70 L/min 0.4 - 1.3 L/min (MEINHARD) Type C Concentric Glass 0.70 L/min 0.4 - 0.95 L/min (MEINHARD) Type K1 Concentric Glass 0.70 L/min 2.5 - 3.5 mL/min (MEINHARD) Type K3...
Page 258 Maintenance Table 5-6. Replacement Parts: Nebulizers and End Caps N0775330 PEEK Mira Mist Nebulizer N0777707 MEINHARD Nebulizer (Type K1) Note: This is the standard nebulizer for the Cyclonic/Meinhard systems. N0780546 GemTip Cross-Flow II Nebulizer N0780676 GemTip Replacement Nebulizer Tips for GemTip Cross- Flow Nebulizer...
Page 259: Gemtip Cross-Flow Nebulizer
GemTip Cross-Flow Nebulizer GemTip Cross-Flow Nebulizer The following procedures cover the maintenance of the GemTip Cross-Flow nebulizer supplied with the instrument. To check the performance of the nebulizer, aspirate a standard and note the intensity reading. If the intensity is significantly lower than it should be, first check that: •...
Page 260: Removing The Nebulizer/End Cap
Maintenance Removing the Nebulizer/End Cap To remove the nebulizer/end cap assembly: 1. Turn off the plasma if it is on. If the plasma has been on, allow one minute for the Quick-Change Adjustable Torch Module to cool and an additional two minutes for the torch to cool before handling.
Page 261 GemTip Cross-Flow Nebulizer Figure 5-24 The nebulizer/end cap assembly removed from the spray chamber. Illustration shows cross-flow nebulizer end cap assembly. Item Description Cross-Flow GemTip Nebulizer End Cap Assembly (Part No. N0780546) Knurled Screw (Part No. 00473539) Knurled Screw (Part No. 00473539) Spray Chamber (Part No.
Page 262: Checking The Spray Pattern
Maintenance Checking the Spray Pattern Once you have thoroughly flushed out the nebulizer with deionized water and removed the nebulizer/end cap, you can follow these steps to check the nebulizer spray pattern: When checking the spray pattern of the nebulizer, pump only use deionized water.
Page 263 GemTip Cross-Flow Nebulizer Figure 5-25 Cross-section of GemTip Cross-Flow Nebulizer shown with Cross- Flow End Cap, Part No. N0780546. Item Description Clear GemTip Red GemTip Argon Inlet Sample Inlet To begin disassembling the nebulizer:...
Page 264: Removing The Sample Tip From The End Cap, N0780546
Maintenance 1. If you have not already done so, remove the nebulizer/end cap assembly from the spray chamber. 2. Disconnect the sample capillary tubing by removing it from the pump tube. 3. Disconnect the nebulizer argon tubing at the gas fitting. Do not disconnect nebulizer argon tubing from the end cap because the GemTip could fall out.
Page 265 GemTip Cross-Flow Nebulizer Figure 5-26 Clear GemTip for sample inlet and associated parts for Cross-Flow End Cap, Part No. N0780546. Item Description Item Description O-Ring (Part No. 09921045) Nut (Part No. 09920546) Clear GemTip Nebulizer 1/16 inch O.D. Teflon Tubing Piece (Part No. (Sample Inlet Available in 09985708) GemTip Kit Part No.
Page 266 Maintenance 5. Check the condition of the tubing piece (Part No. 09985708). If the tubing is worn, replace it as follows: • Obtain a new piece of 1/16-in. O.D. Teflon tubing (Part No. 09985708). • Using a razor blade, make a straight cut on one end of the tubing. •...
Page 267: Removing The Argon Tip From The End Cap, N0780546
GemTip Cross-Flow Nebulizer 9. If you have installed new 1/16-in. tubing, cut the tubing so that it extends approximately 1/2 in. beyond the nut. 10. For the sample capillary tubing, use a piece of 0.023 in. (inner diameter) polyethylene tubing (Part No. 09908265). Using a razor blade, bevel the tubing by cutting it at an angle.
Page 268 Maintenance 4. Inspect the O-ring (Part No. N09921045), replace if it is worn or cracked. Figure 5-28 Red GemTip for argon inlet and associated parts for Cross-Flow End Cap (Part No. N0780546). Item Description End Cap O-Ring (par No. 09902033) O-Ring (Part No.
Page 269 GemTip Cross-Flow Nebulizer 5. To reassemble the nebulizer make sure that the O-ring is completely seated on the base of the argon tip, then insert the argon tip into the argon inlet. 6. Check the condition of the argon inlet tubing (Part No. 09985723). If the tubing is worn, replace it as follows.
Page 270: Connecting The Nebulizer Argon Tubing (Cross-Flow End Cap, N0780546)
Maintenance Connecting the Nebulizer Argon Tubing (Cross-Flow End Cap, N0780546) 1. Pass the tubing (Part No. 09985723) through the nut (Part No. 09920545) and attach the ferrule (Part No. 09920515) on the end of the tubing. See the following figure. 2.
Page 271 GemTip Cross-Flow Nebulizer 4. Connect the nebulizer argon tubing to the NEB connection with the quick disconnect. Figure 5-30 Connecting the tubing. Item Description Sample Compartment Scott Spay Chamber Clip Nut (Part No. 09920545) 1/8 inch O.D. Tubing (Part No. 09985723)
Page 272: Replacing The Nebulizer/End Cap
Maintenance Replacing the Nebulizer/End Cap Before replacing the end cap: • Check the end cap O-ring (Part No. 09902033) for nicks or cracks. If you need to replace the O-ring, remove the two knurled screws and the end cap ring. When placing the end cap ring back on the end cap, install it with the flat side against the O-ring and the molding marks (small circular indentations) against the end cap.
Page 273: Gemcone Nebulizer
GemCone Nebulizer GemCone Nebulizer Daily Cleaning of the Low-Flow GemCone Nebulizer Each day after use, the low-flow GemCone nebulizer should be rinsed out by pumping deionized water to the nebulizer for several minutes. This should be done with both the plasma on and the nebulizer gas on. This helps prevent the formation of salt crystals near the exit of the nebulizer gas orifice.
Page 274: Installing The Gemcone Nebulizer On The Scott-Type Spray Chamber
Maintenance Installing the GemCone Nebulizer on the Scott-Type Spray Chamber To install the GemCone nebulizer on the Scott-type spray chamber, the end cap assembly (Part No. N0680504) and the tubing assembly (Part No. N0770336) must be used. 1. Remove the existing nebulizer/end cap assembly (if the wrong one is installed) by loosening the knurled nuts on the end cap.
Page 275 GemCone Nebulizer Figure 5-31 Installing the GemCone nebulizer to a Scott-type spray chamber. Item Description End Cap Assembly (Part No. N0680504) Knurled Nut-2 (Part No. 00473539) Capillary Tubing (Part No. 09908265) GemCone Nebulizer Assembly Argon Gas Fitting Tubing Assembly (Part No. N0770336)
Page 276: Installing The Gemcone Nebulizer On The Cyclonic Spray Chamber
Maintenance Installing the GemCone Nebulizer on the Cyclonic Spray Chamber 1. Before inserting the GemCone nebulizer into the chamber, connect the argon gas fitting to the nebulizer threads. First, tighten the gas fitting by hand. Tighten the fitting another 1/8 of a turn using a 9/16-in. open-end wrench. Support the nebulizer with a back-up wrench when tightening or loosening fittings.
Page 277: Cleaning The Gemcone Nebulizer
GemCone Nebulizer Figure 5-32 Connecting the GemCone nebulizer to the cyclonic spray chamber. Item Description Item Description Cyclonic Spray Chamber GemCone Nebulizer Assembly Tubing Assembly for the Teflon Tubing-1 inch (Part No. GemCone Nebulizer (Part No. 09985708) N0770336) Argon Gas Fitting Capillary Tubing (Part No.
Page 278: Gemcone Liquid Fitting Maintenance
Maintenance 4. Apply ultra-sonication to the solution containing the nebulizer for about five minutes. 5. Rinse the nebulizer thoroughly using deionized water. 6. Dry the gas passages of the conespray nebulizer by connecting the argon gas fitting and turning on the argon flow to 1 L/min. Allow the argon flow to dry the internal passages for several minutes.
Page 279 Concentric Glass Nebulizer 1. The spacer must be installed on the concentric glass nebulizer assembly. Figure 5-33 Concentric Glass Nebulizer Assembly Item Description Concentric Glass Nebuizer Assembly Spacer 2. Install the concentric glass nebulizer assembly into the spray chamber.
Page 280 Maintenance 3. The nebulizer should be pushed flush against the spacer, which will sit flush against the knurled nut on the spray chamber. However, the nebulizer may be moved slightly out to optimize intensities and RSDs. Figure 5-34 Concentric Glass Nebulizer Assembly Attached to the Spray Cham- Item Description Concentric Glass Nebulizer Assembly (Part No.
Page 281: Installing The Concentric Nebulizer On The Scott's Spray Chamber
Concentric Glass Nebulizer Installing the Concentric Nebulizer on the Scott's Spray Chamber 1. The spacer must be installed on the concentric glass nebulizer assembly. See Figure 5-33. 2. Insert the Concentric Glass nebulizer, as far as it will go, through the opening in the end cap of the Scott's spray chamber.
Page 282: Cleaning The Concentric Glass Nebulizer
Cleaning the Concentric Glass Nebulizer For detailed information on cleaning MEINHARD Concentric Glass nebulizer, see Maintenance Tips for Users of the MEINHARD Concentric Glass Nebulizer (PerkinElmer Part No. 099936334), which is also available upon request from J.E. Meinhard Associates, Inc. J.E. Meinhard Associates, Inc.
Page 283 Concentric Glass Nebulizer Golden, CO 80401-5636 Telephone: 303-277-9776 FAX: 303-279-5156 Toll Free Telephone:800-MEINHARD (800-634-6427) Internet address: http://www.meinhard.com The following table summarizes the cleaning procedures for the MEINHARD Concentric Glass nebulizer. Figure 5-36 Cleaning Strategy for the MEINHARD Nebulizer. (Reprinted with the permission of JE Meinhard Assoc., Inc.) When cleaning the concentric glass nebulizer, do not use ultrasonic Caution cleaning.
Page 284: Mira Mist Nebulizer
Maintenance Mira Mist Nebulizer This device operates on compressed gases. Appropriate care must be taken. If in doubt about correct operating procedures, call an experienced operator. Burgener Mira Mist Nebulizers require 45 - 55 psi to have a 1 liter per minute of Argon gas flow, so the Warning operating pressures are in the range of 25 - 45 psi, depending on the torch optimum flow rate.
Page 285: Sample Capillary Tubing
Mira Mist Nebulizer The gas orifice is at the very tip of the nebulizer. It is made of Teflon which Caution is VERY SOFT. This tip is very easily damaged and should NEVER be touched with fingers, tissues, or anything else. If the tip is accidentally touched and the nebulizer continues to operate, then it is still functional, and its use can be safely continued.
Page 286: Sample Introduction / Maximizing Stability
The gas line terminates in the Avio 500 quick disconnect. It is a direct replacement for typical concentric nebulizers. Sample Introduction / Maximizing Stability The Mira Mist does not have any suction, so it requires a pump to supply the sample solution.
Page 287: Peristaltic Pump
Peristaltic Pump Peristaltic Pump The peristaltic pump requires routine maintenance to ensure that the system will run properly. The pump tubing should be replaced when flat spots develop (on a daily basis or after approximately eight hours of use). When replacing the pump tubing, the drain tubing should be replaced at the same time since uneven wear can cause the spray chamber to back up.
Page 288 Maintenance Figure 5-37 Tubing installed on pump for sample and drain Item Description From Spray Chamber Drain To Drain Bottle To Nebulizer From Sample Container...
Page 289: Installing The Sample Tubing
Peristaltic Pump Installing the Sample Tubing To install the sample tubing refer to the instructions below and the next two figures: 1. Turn off the peristaltic pump using the software control. 2. Take a piece of 0.76 mm (0.030 in.) pump sample tubing. New pump tubing will work better if it is pre-stretched, and analytical precision will be improved.
Page 290 Maintenance 5. Insert the beveled end of the sample capillary tubing into one end of the pump tubing. Lead the capillary tubing to the sample bottle. Figure 5-38 Tubing assembly for sample. Item Description Item Description Scott Spray Chamber Polyethylene tubing (including with the Nebulizer, 0.58 mm i.d.
Page 291: Connecting The Drain Tubing Assembly
Peristaltic Pump 6. Insert the beveled end of the nebulizer capillary tubing into the other end of the pump tubing. 7. Attach the capillary tubing to the sample inlet of the nebulizer. Connecting the Drain Tubing Assembly Table 5-8. Spray Chamber Drain Spare Parts Part No.
Page 292 Maintenance 1. Attach a small piece of 1.5 mm (0.06 in.) i.d. PVC tubing (Part No. 09985729) to the barbed fitting (Part No. 09920267). 2. Cut the 1 mm i.d. tubing at an angle and insert it into the 1.5 mm tubing. Figure 5-39 Drain tubing assembly.
Page 293: Installing The Drain Tubing
Peristaltic Pump Item Description Item Description Sleeve (Part No. N0695415) Teflon Tubing 1 mm i.d. (Part No. 09985708) Spray Chamber Drain bottle PVC Tubing 1.5 mm i.d. Peristaltic Pump (Part No. 09985735) Installing the Drain Tubing Install the drain tubing on an open channel of the peristaltic pump as follows: 1.
Page 294: Adjusting The Pump Tubing
Maintenance Adjusting the Pump Tubing Adjust the tension on the sample and drain tubing, one at a time, using deionized water as follows: Adjusting the Sample Tubing 1. Make sure the sample tubing is centered in the channel, then place the clamp around the tubing and lower the clamp arm on onto the pump.
Page 295: Cleaning The Pump
Peristaltic Pump 5. Tighten the adjustment screw slowly (turn clockwise) until you just see a smooth flow of bubbles. Add an additional three more turns. 6. Turn off the pump. The tension is now correctly set. No bubbles should be seen in the sample tubing once the sample tube is kept in the solution.
Page 296: Drain
Maintenance Drain One drain is used on the Avio 500. This pumped drain leads from the spray chamber. To connect the drain to the drain bottle, refer to the next figure and follow the steps below: 1. Connect the drain tubing leading from below the sample compartment to one of the large fittings on the drain bottle.
Page 297 Peristaltic Pump Figure 5-40 Tubing connections to the drain bottle. Item Description Item Description Sample Compartment Drain Tubing Piece 1.6 mm i.d. (Part No. 02506241)
Page 298: General System Maintenance
Maintenance Item Description Item Description Spray Chamber Teflon Tubing 1 mm i.d. (Part No. 09985708) PVC Tubing 1.5 mm i.d. (Part No. Pump Tubing 1.14 mm i.d. 09985735) Coupler (Part No. 09920186) Peristaltic Pump General System Maintenance Cleaning the Instrument Exterior surfaces may be cleaned with a soft cloth, dampened with a mild detergent and water solution.
Page 299: Chiller And Filters
General System Maintenance Figure 5-41 Location of the air filters on the left and right side of the instrument. Item Description Left Side of the Instrument Right Side of the Instrument Air Filters (Part No. 09995098) Chiller and Filters Inspect the metal strainer (Part No. N0776075) that is suspended inside the chiller reservoir;...
Page 300: Fuses
For additional information on the chiller, refer to the manufacturer's maintenance guidelines. Figure 5-42 Location of the filter on the chiller. Item Description Chiller Air Filter (remove in this direction) (PolyScience Part No. 750-855) Fuses Fuses may only be replaced by a PerkinElmer service engineer.
Page 301: Replacement Parts: General
Replacement Parts: General Replacement Parts: General Every day you count on PerkinElmer to provide you with solutions that deliver reliable performance, control operating costs and maximize operational time. Our complete portfolio of consumables, parts, supplies, training and service helps you meet both routine and demanding measurement challenges.
Page 302 Maintenance Table 5-12. Gas and Water Supply Connections Part No. Description 09920584 Space Collar for 3/8-in. Swagelok Fittings 09995098 Air Filter for Spectrometer N0690274 Argon Supply Hose N0690275 Nitrogen Supply Hose N0770341 Water Supply Hose N0770342 Water Drain Hose N0770348 Shear Gas Supply Hose N0775325 Air Dry Filter Assembly with R250 Regulator...
Page 303 Description 09920044 Clamp for RF Generator Exhaust Hose N0770434 Fresh Air Kit (which includes the Flex Hose and Hose Clamp) N0811592 Avio 500 Drip Tray Table 5-14. Organic Sample Introduction Kit (Part No. N0790610) Part No. Description N0790249 3 Slot Quartz Torch N0791181 1.2 mm i.d.
Page 304 Maintenance Table 5-15. All Replacement Parts by Part Number Part No. Description 00473194 O-Ring (for Nebulizer Seal on N0680504 End Cap) 00473539 Knurled Screw used on End Cap 00473550 Solvent Flex Pump Tubing, 0.76mm ID, Black/Black (Sample tubing) 00473552 Silicone Pump Tubing, 0.76mm ID, Black/Black (Sample tub- ing) 02506241 Micro Line Tube 0.125 x 0.0625...
Page 305 Replacement Parts: General Table 5-15. All Replacement Parts by Part Number Part No. Description 09902143 O-Ring (for Dual View Axial Purge Window) 09902207 O-Ring (Injector Adapter - inside) 09903730 Nipple, 1/16 to 1/8 09904991 Drain Bottle (Carboy 15 Liter) 09907917 Wrench - Hex Key Right Angle 2.0MM 09908265 Polyethylene Tubing, Sample Capillary...
Page 306 Viton Pump Tubing, 0.89mm ID, Orange/Orange (Sample tubing) 09926070 O-Ring (for Cyclonic Spray Chamber Ball Mount) 09936225 ICP-OES Instrument Maintenance Log Book 09931199 Unpacking Instructions Avio 500 09985708 PTFE Tubing 0.031 x 0.016 09985723 1/8 in. OD Teflon Tubing 09985729 PVC Tubing 1.5mm ID 09985730 PVC Tubing 0.031 ID, 10 FT.
Page 307 Replacement Parts: General Table 5-15. All Replacement Parts by Part Number Part No. Description N0371505 GemCone™ Sample Capillary Adapter N0581455 Ceramic Purge Extension N0581497 Purge Window N0582152 Calmix 3 Solution N0582325 ICP Concepts Book N0680504 End Cap for GemCone Nebulizers N0681574 MEINHARD Nebulizer (Type K3, Reduced flow and organ- ics)
Page 308 Maintenance Table 5-15. All Replacement Parts by Part Number Part No. Description N0695258 O-Ring for Purge Extension N0695414 Drain Adapter N0695415 Drain Coupling N0770183 Hose Kit (includes gas and cooling water hoses) N0770336 Quick Disconnect Tubing Assembly for GemCone Nebulizer N0770341 Water Supply Hose N0770342...
Page 309 Replacement Parts: General Table 5-15. All Replacement Parts by Part Number Part No. Description N0770448 Wrench Assembly for DV Nut N0770603 Injector Adapter Assembly (includes O-Rings but not injector) N0770605 Cyclonic Spray Chamber with Cap for Aqueous Solutions N0770608 External Spray Chamber Mount for use with high-volatility organic solutions N0770609 Stand for Dual View Torch Assembly...
Page 310 Maintenance Table 5-15. All Replacement Parts by Part Number Part No. Description N0771550 TC44 HF Resistant Cyclonic Spray Chamber N0773061 Tray for Peristaltic Pump N0773084 DV Axial Window Cap N0773090 DV Axial Window Holder N0773115 Viton Pump Tubing, 1.14mm ID, Red/Red (Drain tubing) N0773118 Viton Pump Tubing, 0.76mm ID, Black/Black (Sample tub- ing)
Page 311 Replacement Parts: General Table 5-15. All Replacement Parts by Part Number Part No. Description N0775346 MicroMist Nebulizer (0.7 L/min. Ar flow rate, 0.6 mL/min. uptake rate) N0775347 MicroMist Nebulizer (0.7 L/min. Ar flow rate, 0.2 mL/min. uptake rate) N0775348 MicroMist Nebulizer (0.7 L/min. Ar flow rate, 0.1 mL/min. uptake rate) N0775349 MicroMist Nebulizer (0.7 L/min.
Page 312 Maintenance Table 5-15. All Replacement Parts by Part Number Part No. Description N0777707 MEINHARD Nebulizer (Type K1, Low Ar Flow nebulizer for routine aqueous samples) N0777111 Sample capillary tubing with fitting N0777112 Sample capillary tubing with fitting (pack of 10) N0777113 Gas Line 2MM With UpChurch Fittings N0777116...
Page 313 Replacement Parts: General Table 5-15. All Replacement Parts by Part Number Part No. Description N0790156 Injector Adapter Kit-Scott (includes o-rings) N0790249 Quartz Torch Hybrid XLT Organics (not ceramic) N0790296 Scott Spray Chamber Clamp Adapter N0790373 HF Resistant Cyclonic Spray Chamber N0790384 Scott Spray Chamber N0790437...
Page 314 Peristaltic Pump Assembly N0810606 Quick Change Torch Module-Scott Spray Chamber N0810607 Quick Change Torch Module-Cyclonic Spray Chamber N0810128 Torch Body Assembly for Avio 500 N8120160 O-Rings for Cyclonic Spray Chamber (PK/10) N8122258 Pump Tubing Adapter N9300067 GemTip™ Cross-Flow Nebulizer O-Ring Kit...
Page 315: Consumables And Supplies
If you are located within the U.S., call toll free 1-800-762-4000, 8 a.m. to 8 p.m. EST. Your order will be shipped promptly, usually within 24 hours. • If you are located outside of the U.S., call your local PerkinElmer sales or service office. Order Online...
Page 316 Maintenance...
Page 317 C h a p t e r 6...
Page 319: Chapter 6: Troubleshooting
Troubleshooting Use the following table to guide you to the appropriate section or manual. Problem Refer to section You are not getting the desired Optimizing and results. Verifying Performance in the Syngistix Software Guide on the Syngistix Document Pack CD or Performance Problems: Troubleshooting Table in this chapter or...
Page 320: What The Performance Checks Measure
Pump Problems on page 332. If after using the troubleshooting techniques in this chapter your instrument is still not performing properly contact PerkinElmer service. What the Performance Checks Measure The tests in this section allow the operator to measure performance aspects of the instrument.
Page 321: Sodium Bullet Test
Sodium Bullet Test • Precision Test: This test indicates the Relative Standard Deviation (RSD) of the instrument's analyte emission intensity or concentration measurements. The RSD may also be referred to as the CV (Coefficient of Variation). A high RSD or CV is usually indicative of a problem with the sample introduction system such as improper drainage, leaks, improper tension on the pump tubing, worn pump tubing, or nebulizer problems.
Page 322: Performance Problems
Troubleshooting If the above checks fail to make an improvement, turn off the plasma, then check the following: • Check that the nebulizer end cap is connected tightly. • Check the nebulizer spray pattern: run deionized water for several minutes, then remove the nebulizer end cap.
Page 323 Do the pump rollers bind or not roll easily? Are there grooves in the pump rollers? On the PerkinElmer pump, the pump head may be removed for cleaning. The pump head may also be replaced. See Peristaltic Pump on page 285.
Page 324 Troubleshooting Are there deposits inside the end cap or spray chamber? Clean out deposits. See Chapter 5, Maintenance for recommended cleaning procedures (Table 5-1 on page 204). Torch Assembly Are the torch fittings for the gas inlets secure? Finger-tighten the fittings. Do not overtighten them. Is the quartz torch cloudy or dirty? Check for deposits, particularly if running organics, alloys, or samples with high dissolved solids.
Page 325 Performance Problems with a soft cloth. If the UV performance does not improve replace the purge windows. Do not touch the window. If oils from the skin are deposited on the window, this can cause inaccurate results. A 10% solution of hydrofluoric acid may be used to clean the window.
Page 326: Performance Problems: Troubleshooting Table
Troubleshooting Performance Problems: Troubleshooting Table Table 6-16. Performance Problems: Troubleshooting Table Problem Possible Cause(s) Corrective Action The sample introduction Refer to General System Maintenance on (Relative system may not be set up page 296. Standard correctly or may require Deviation) maintenance.
Page 327 Performance Problems: Troubleshooting Table Table 6-16. Performance Problems: Troubleshooting Table Problem Possible Cause(s) Corrective Action Cannot obtain You may not be comparing Refer to the Syngistix Software Guide on the suggested the appropriate BEC value for Syngistix Document Pack CD for details. BEC value the wavelength you are using.
Page 328 Troubleshooting Table 6-16. Performance Problems: Troubleshooting Table Problem Possible Cause(s) Corrective Action Results Corrections may not have Aspirate a blank and rerun standards and erroneously been made for the reagent samples. high blank. Standard solutions may have Restandardize with a proven standard. deteriorated or may have been improperly made.
Page 329 Performance Problems: Troubleshooting Table Table 6-16. Performance Problems: Troubleshooting Table Problem Possible Cause(s) Corrective Action Undetectable The sample introduction Refer to General System Maintenance on emission system may not be set up page 296. signal correctly, or may require maintenance. The shutter may be closed.
Page 330: Plasma Ignition And Stability Problems
Troubleshooting Table 6-16. Performance Problems: Troubleshooting Table Problem Possible Cause(s) Corrective Action Cannot get The standard may have too The standard should be 100 times the suggested high a concentration. estimated detection limit. detection limits (continued) You may not be comparing Confirm that you are using the appropriate the appropriate value for the wavelength and recheck the value.
Page 331 Plasma Ignition and Stability Problems torch glassware. Also, check the ignitor ground. If necessary, use a brush to clean it. Refer to Chapter 4, Installation, to Figure 4-9 for an illustration on the location of the ignitor contact finger and the ignitor ground. •...
Page 332: Plasma Stability Problems
Troubleshooting • Organics. If you analyzing organic solutions and cannot ignite the plasma, run the nebulizer argon for a couple of minutes with the pump off to purge the spray chamber. • Organic Vapors. If these remain in the torch from an earlier analysis, they can sometimes cause ignition problems.
Page 333: Printing Problems
Printing Problems Printing Problems Table 6-17. Printing Problems Problem Possible Cause(s) Corrective Action Printer does not The correct printer driver may Check the printer drivers in Windows. print or does not not be installed or selected in For more information, see the print correctly Windows.
Page 334: Pump Problems
Check the rollers in the pump head to other end Rollers may be stuck. see if they roll freely. Tubing may be worn. Replace tubing. Pump makes A mechanical problem may Call a PerkinElmer Service excessive noise have occurred. Representative.
Page 335: Autosampler Problems
Autosampler Problems Autosampler Problems Table 6-19. Autosampler Problems Problem Possible Cause(s) Corrective Action Autosampler does There may be a Use the Instrument Diagnostics not respond communication problem. window to reset the autosampler. The software may not be Select the Instrument tab -> Devices configured for the click on the Autosampler tab and autosampler you are using.
Page 336: Rf Generator/Sample Introduction System Troubleshooting Form
Troubleshooting RF Generator/Sample Introduction System Troubleshooting Form Fill out the following form before you contact PerkinElmer service. Troubleshooting Form General: Instrument Serial Number: Site: Date: Sample Introduction Configuration: Nebulizer Type: CROSS FLOW / LF GEMCONE / MEINHARD Spray Chamber Type:...
Page 337: Troubleshooting Tasks Performed
RF Generator/Sample Introduction System Troubleshooting Form Troubleshooting Tasks Performed: Did the plasma light: Yes/No Did the plasma stay lit after ignition: Yes/No Plasma went out after pump turned on: Yes/No Plasma went out after how long of operation: Plasma went out with Dry Plasma (neb on, no pump): Yes/No Plasma went out when injector capped off: Yes/No...
Page 338 Troubleshooting The following illustrations show various torch positions. Figure 6-1 and 6-2 show the correct position of the injector for normal plasma conditions. The dotted line represents the center of the hex nut and its relationship to the position of the injector.
Page 339 RF Generator/Sample Introduction System Troubleshooting Form Figure 6-2. Normal plasma at -3mm position.
Page 340 Troubleshooting Figure 6-3. Rounded Plasma due to sample or air getting around the outside (typically subtle air leak).
Page 341 RF Generator/Sample Introduction System Troubleshooting Form Figure 6-4. Aux Gas too high, air leak, or spray chamber temperature too high.
Page 342 Troubleshooting Figure 6-5. Injector too far forward.
Page 343 RF Generator/Sample Introduction System Troubleshooting Form Figure 6-6. No Aux Gas (torch may be glowing).
Page 344 Troubleshooting Figure 6-7. Air leak or spray chamber temperature too high.
Page 345 RF Generator/Sample Introduction System Troubleshooting Form Figure 6-8. Thin plasma due to leak in plasma gas line.
Page 346 Troubleshooting...
Page 347 Index daily checks electrical requirements Acid Digestions 126, 127 filling Adjusting the Sampling Probe Height filters Air Filters remote connections general maintenance remote operations maintenance space requirements periodic checks starting RF generator, changing Coil, RF spectrometer, changing see RF Coil Alignment Connections 169, 172...
Page 348 Index Dissolving Solid Samples daily checks in organics requirements, laboratory preparation using acids Drain Filters 200, 329 daily checks periodic checks part numbers safety practices replacement parts tubing, connecting water Drain Tubing Fitting the Sampling Probe adjusting Fold Flat Mirror connecting Fuses 285, 291...
Page 349 Index Ignitor environmental conditions checking cable exhaust vent requirements Indicator Lights laboratory space requirements illustration Laboratory Requirements Initialization of Instrument chiller initialization steps Laboratory Ventilation interlocks Initialization of instrument Maintenance Injector air filters checking cleaning procedures removing 276, 280 concentric glass nebulizer Input Module cyclonic spray chamber, cleaning description...
Page 350 Index Mira Mist tubing,connecting Mira Mist Nebulizer Nebulizer End Cap cleaning checking Nebulizer, Mira Mist Nebulizer Tubing Moving connecting instrument Neon Lamp changing Nitrogen Purge Rate Nebulizer Nitrogen Supply argon flow rate 96, 118 connecting, instructions argon tubing, connecting argon tubing, replacing comparison of different types Optical System concentric glass nebulizer, maintenance...
Page 351 Index pump head, removing Purge Windows replacement parts instruments troubleshooting problems with replacement parts TubingSaver Peristaltic Pump Tubing Quick-Change Adjustable Torch Module inspecting installation replacing Quick-Change Torch Module Plasma description troubleshooting ignition problems troubleshooting stability problems regulatory information Plasma Argon Flow Rates electromagnetic compatibility Plasma Induction Plates Replacement Parts...
Page 352 Index electrical safety subarray pattern environmental conditions Schmidt Cross Disperser fusion mixtures Shear Gas 96, 120 general practices connecting, instructions hazardous chemicals warnings connection at back of instrument hot exhaust gases daily checks hydrofluoric acid purpose instrument handling Shear Gas Nozzle laboratory guidelines replacing laboratory ventilation...
Page 353 Index spare parts Spray Chamber, Scott Ultraviolet Radiation cleaning safety practices replacing UV Module Switch description illustration Symbols 169, 172 Viewing graphics on the instrument Visible Channel used on the instrument description warnings on the instrument Warnings Test Solutions symbols used on instrument Torch Waste Disposal Procedures 169, 172...
Page 355 PerkinElmer, Inc. 710 Bridgeport Avenue Shelton, CT 06484-4794, U.S.A. Internet: http://www.perkinelmer.com email: info@perkinelmer.com PerkinElmer is a registered trademark of PerkinElmer, Inc.

PerkinElmer AVIO 500 Customer Hardware And Service Manual

Chapter 1: Safety Practices

Chapter 2: Preparing Your Laboratory

Chapter 3: System Description

Chapter 4: Installation

Chapter 5: Maintenance

Chapter 6: Troubleshooting

Quick Links

Troubleshooting

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Summary of Contents for PerkinElmer AVIO 500