The Americas Europe/Middle East/Africa Asia Pacific 6060 Spine Road T +44 (0) 161 864 6800 T +(8621) 38777735 Boulder, CO 80301-3687 USA email@example.com firstname.lastname@example.org T +1 800 255 6964 ServiceUK.Instruments@ge.com TechSupportSG.GEAI@ge.com T +1 303 444 2009 F +1 303 444 9543 www.geinstruments.com...
Confidentiality The information contained in this manual may be confidential and proprietary and is the property of GE Analytical Instruments. Information disclosed herein shall not be used to manufacture, construct, or otherwise reproduce the goods disclosed herein. The information disclosed herein shall not be disclosed to others or made public in any manner without the express written consent of GE Analytical Instruments.
Warranty Term The GE Analytical Instruments warranty term is thirteen (13) months ex-works, or twelve (12) months from installation or start up by GE Ana- lytical Instruments certified service personnel. In no event shall the standard limited warranty coverage extend beyond thirteen (13) months from original shipment date.
Operation and Maintenance Manual. Usage of non-recommended maintenance materials may void a warranty claim. The remedies provided herein are the customer's sole and exclusive remedies. In no event shall GE Analytical Instruments be liable for direct, indirect, special, incidental or consequential damages (including loss of profits) whether based on contract, tort, or any other legal theory.
Gli unici rimedi spettanti all’utente sono quelli qui inclusi. In nessun caso GE Analytical Instruments sarà responsabile per danni diretti, indiretti, speciali, accidentali o consequenziali (inclusa la perdita di profitti) risultanti dall’applicazione del contratto, atto illecito o altra teoria legale. Il manuale d’uso e manutenzione è...
Warning If this instrument is used in a manner not specified by GE Analytical Instruments, the protection provided by the instrument may be impaired. Warning Consult the MSDS that accompanies each standards set and the reagents to identify proper disposal techniques.
Warning If you experience an issue with the printed circuit assembly (PCA) that contains a lithium battery, please contact GE Analytical instruments for return instructions. Whenever changing the lithium battery, observe the correct polarity. Dispose of used batteries according to the manufacturer’s instructions and local disposal requirements.
Advertencia La utilización de este instrumento de un modo no especificado por GE Analytical Instruments puede afectar la protección que brinda el instrumento. Advertencia Para conocer las técnicas apropiadas de desecho, consulte la hoja de datos de...
Se você se deparar com um problema com as placas de circuitos impressos que contenha bateria de lítio, entre em contato com a GE Analytical Instruments para obter instruções para a devolução. Sempre que trocar a bateria de lítio, observe a polaridade correta.
Warnung Alle Arbeiten im Inneren des Analysators, einschließlich der Anbringung von Verschleißteilen, können zu Verletzungen führen. Um elektrische Schläge oder Verbrennungen zu vermeiden, schalten Sie den Analysator aus und ziehen Sie den Netzstecker, bevor Sie ihn öffnen. Seien Sie vorsichtig, wenn Sie elektrische Komponenten berühren.
Wenn sich Probleme mit der bestückten Leiterplatte (PCA) ergeben, die eine Lithiumbatterie enthält, wenden Sie sich bitte wegen der Rücksendeanweisungen an GE Analytical Instruments. Beachten Sie bei jedem Wechsel der Lithiumbatterie die richtige Polung. Entsorgen Sie die gebrauchten Batterien gemäß den Herstelleranweisungen und den örtlichen Entsorgungsbestimmungen.
électromagnétiques, auquel cas l'utilisateur peut être contraint de prendre les mesures adéquates pour y remédier. Avertissement Si cet instrument est utilisé d'une manière non spécifiée par GE Analytical Instruments, la protection offerte par l'instrument peut s'en trouver affaiblie. Avertissement Consulter les fiches techniques des substances dangereuses fournies avec chaque jeu de standards et avec les réactifs afin d'identifier les bonnes techniques de mise...
Chapter 1. Introduction The Sievers* InnovOx On-Line TOC Analyzer from GE Analytical Instruments is a high-sensitivity Analyzer used to measure the concentration of total organic carbon (TOC), non-purgeable organic carbon (NPOC), total carbon (TC), and inorganic carbon (IC) in water samples. The Analyzer uses supercritical water oxidation (SCWO) to measure a wide range of carbon concentrations in complex sample matrices, including those containing high concentrations of total dissolved solids (TDS) and particulates.
USEPA SW 9060, DIN-EN1484, ISO 8245. System Overview The Sievers InnovOx On-Line TOC Analyzer consists of eleven major modules: Multistream module, which accommodates two or five sample streams, depending on the Analyzer configuration. It also includes a vial port, which is used to calibrate the Analyzer. The multistream module also includes a port through which a check standard can be measured.
The consumable scrubber cartridge must be replaced per the maintenance schedule presented in Table 15, “2-Year Maintenance Worksheet — Sievers InnovOx Online TOC Analyzer,” on page 196. Fail Safe Accessory If the Fail Safe accessory is selected, sensors are installed in the Analyzer to detect when the flow rate of each sample stream stops.
To overcome the effect of reducing agents in the sample, increase the oxidizer percentage until further increases do not produce significantly greater NPOC, TC, or TOC readings. Contact GE Analytical Instruments for questions about specific applications. In North America, contact GE Analytical Instruments Technical Support at 303.444-2009 or 888.245.2595 or techSupport.GEAI@ge.com.
Support at 303.444-2009 or 888.245.2595 or techSupport.GEAI@ge.com. Technical support in Europe, Middle East, and Africa is available at 44 (0) 161 864 6800 or ServiceUK.Instruments@ge.com. Technical support in Asia Pacific is available at (65) 62674659 or TechSupportSG.GEAI@ge.com. In other parts of the world, contact your local GE Analytical instruments representative.
Chapter 4: Installation • Sievers InnovOx On-Line TOC Analyzer Operations and Maintenance Manual (Available for download from www.geinstruments.com). • Accessories included: • Reagent, dilution water, check standard tubes (and tubing weights and fittings) • Vial port tube and fittings • Waste tube ®...
To mount a Filter Panel on the Mounting Stand, attach the two Filter Panel brackets 30.5 cm apart, as shown in Figure 2. Further instructions for installation of the Filter Panel are provided in the GE InnovOx Filter Panel Operation and Maintenance Manual.
Step 7: Connecting to a Power Supply Installation of the Sievers InnovOx On-Line TOC Analyzer requires an external source of AC power connected to the enclosure using a watertight, grounded conductive conduit connector. A qualified electrician should make the electrical connections according to local Electrical Code.
Chapter 5. Calibration and Verification Overview Calibration of the Sievers InnovOx On-Line TOC Analyzer for NPOC, IC, TC and TOC (TC- IC) measurements is accomplished using standards that contain known concentrations of carbon of interest. It is required that the InnovOx be calibrated for the specific mode that you will be running samples.
Calibration Group. Handling Standards GE Analytical Instruments recommends special handling of all standards to ensure proper preparation and analysis. Most standards are provided in 250 mL bottles. Before performing calibration or verification, standards solutions should be transferred into 40 mL vials for use with the Analyzer’s vial port. Additionally, observe the following practices: •...
Analyzer. When the Analyzer is first powered on, a startup screen appears with basic GE Analytical Instruments contact information and the firmware version number. The Analyzer then begins initialization to check the status of consumables and prepare for making measurements.
Use Sample Flushes to quickly reach steady-state response when the Analyzer will be switching from one stream to another and the two streams have very different concentrations. • If you have a GE InnovOx Filter Panel installed (ONLY), press the Blowback Pulses button to set the number of pulses.
Press Password to enter a unique user password, and then press Enter. Write down your passwords and store them in a safe place for future reference. If you have forgotten your password, you will need to contact GE to help unlock your Analyzer with the keycode that appears on the Login screen.
USB key. If you downloaded the upgrade files from the GE website, make sure that the files are saved in the proper folders on your USB key (:\InnovOx\Upgrade). After you install your USB key in the USB port, wait 15 seconds and then select the Upgrade button.
200 m. The InnovOx On-Line TOC Analyzer is designed to control up to five Filter Panels. Refer to the GE Filter Panel Operation and Maintenance Manual for instructions on the installation and setup of the Filter Panel.
Table 14 for the recommended consumables replacement schedule. Maintenance items MUST be purchased from GE Analytical Instruments. If you need additional assistance in North America, contact GE Analytical Instruments Technical Support at 303.444-2009 or 888.245.2595 or techSupport.GEAI@ge.com. Technical support in Europe, Middle East, and Africa is available at 44 (0) 161 864 6800 or .
6800 and in Asia Pacific, contact us at (8621) 38777735. Technical support in North America is available at 303.444-2009 or 888.245.2595 or TechSupport.GEAI@ge.com. Technical support in Europe, Middle East, and Africa is available at 44 (0) 161 864 6800 or ServiceUK.Instruments@ge.com. Technical support in Asia Pacific is . ...
Analyzer’s Main screen and on the Consumables screen. For this procedure, the Analyzer should be powered on. Contact GE Analytical Instruments at 303. 444.2009 or 800.255.2595 for a replacement kit. Technical Support in North America is available at 303.444-2009 or 888.245.2595 or techSupport.GEAI@ge.com.
Replacing the High Pressure Valve Seals Warning Wear eye protection and gloves when performing this task. The Sievers InnovOx Online TOC Analyzer has two high pressure valves (V4-R and V5-R). These valves are identified in Figure on page 190. Each valve contains a seal that wears over time. The seals should be replaced after one month of operation.
Chapter 8: Maintenance Table 15: 2-Year Maintenance Worksheet — Sievers InnovOx Online TOC Analyzer Item Operating Time Installation Date Notes GLS (clean and refill with DI water) 1 month Oxidizer reagent 1 month, or as needed Dilution water 1 month...
Chapter 8: Maintenance Table 15: 2-Year Maintenance Worksheet — Sievers InnovOx Online TOC Analyzer Item Operating Time Installation Date Notes High pressure valve seals 13 months High pressure valve seals 14 months High pressure valve seals 15 months Exterior sample pump tubing...
This chapter provides the starting point for troubleshooting basic issues with your Analyzer. If you need additional assistance in North America, contact GE Analytical Instruments Technical Support at 303.444-2009 or 888.245.2595 or techSupport.GEAI@ge.com. Technical support in Europe, Middle East, and Africa is available at 44 (0) 161 864 6800 or .
50 - Power Error on System/Controller Board Message: "Power error on System/Controller Board. Please power cycle the Analyzer. If the problem persists, export errors and contact GE Analytical Instruments for further instructions and analysis." Explanation: Replace the System/Controller Board.150 - Software Control Error Message: "Software control error.
Explanation: Based on the history of usage, the Analyzer estimates that only two weeks of pinch valve tubing remains. The tubing must be replaced to protect the operation of the pinch valves. Order tubing from GE now to avoid down time and more costly failures of pinch valves.
Explanation: Check that water is flowing in the sample cup and the inlet valve (if installed) is properly adjusted. If the problem persists, please export the warnings and contact GE Analytical Instruments for further instructions. 6418 – Stream 3 Flow Warning Message: “Stream 3 flow stopped.”...
Explanation: This error is associated with the creation of a .pdf file. If you are creating a .pdf from the Analyzer, shut down the Analyzer, power cycle and repeat. If the problem persists, contact GE Analytical Instruments for further instructions.‘...
Then, check the cable connections. You may be able to regain control of the unit by plugging a mouse into any of the USB port. If the problem persists please export the errors and contact GE Analytical Instruments for further instructions.”...
Message: “Go to the Diagnostics screen and run the Gas Valves test (V7-SH). If the gas flow rate fails to maintain 200 cc/min, please export the errors and contact GE Analytical Instruments for further instructions.” Explanation: The flow rate of gas through the sparger was found to be too low. There may be a problem with valve V7-SH or with the gas tubing.
6438 – Printer Error Message: “System either failed to detect an HP printer, or the printer is not currently supported. Please export the errors and diagnostics, and contact GE Analytical Instruments for further instructions.” Explanation: Please refer to “Printer Setup” on page 162 for a list of supported printers.
Control Manifold are not leaking. Check gas connections leading to the NDIR end caps. If all of those items are correct, then contact GE Analytical Instruments for further information. To continue the series of gas leak checks, leave the plug on the NDIR end cap outlet gas line and proceed to the next section, “To perform the (Check 2) Reactor Inlet Valve Leak Check.”...
Figure 110: Sparger Diagnostics Screen Contacting Technical Support If you need further help troubleshooting any of these or other issues in North America, contact GE Analytical Instruments Technical Support at 303.444-2009 or 888.245.2595 or techSupport.GEAI@ge.com. Technical support in Europe, Middle East, and Africa is available at 44 (0) 161 864 6800 or .
Returning the Analyzer to GE Analytical Instruments In some instances, after consulting with GE Analytical Instruments Technical Support, it may be necessary to return the Analyzer to the factory for repairs. Only return the Analyzer if Technical Support has issued you a Return Authorization (RA) number.
Check Standard carboy should be refilled. It also automatically skips analysis of sample streams when flow stops. Flush The Sievers InnovOx Online TOC Analyzer can perform two types of flushes: Sample Flushes and Dilution Water Flushes (defined later in this section). Sample Flush Sample Flushes should be performed only when there is a very large concentration difference between one sample and the next.
5,000 ppm is analyzed. Reagent Water Reagent-grade water, having a TOC concentration less than 0.1 ppm. Sievers Reagent Water is available in 40 mL vials with a concentration of less than 0.05 ppm from GE Analytical Instruments. Rejects The number of initial measurements for a sample in the Grab, Check Standard, Calibration, or Verification mode that will be omitted from the Analyzer’s calculations.