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GE Sievers Innovox Operation And Maintenance Manual

GE Sievers Innovox Operation And Maintenance Manual (270 pages)

TOC analyzer  
Brand: GE | Category: Analytical Instruments | Size: 14.81 MB
Table of contents
Identification Records3................................................................................................................................................................
Table Of Contents4................................................................................................................................................................
List Of Tables10................................................................................................................................................................
List Of Figures11................................................................................................................................................................
Revision History15................................................................................................................................................................
Confidentiality16................................................................................................................................................................
Declaration Of Conformity17................................................................................................................................................................
Standard Limited Warranty17................................................................................................................................................................
Limitation Of Remedies And Liability18................................................................................................................................................................
Limitación De Remedios Y Responsabilidad18................................................................................................................................................................
Limites De Correction Et De Fiabilité18................................................................................................................................................................
Beschränkte Ansprüche Und Haftung18................................................................................................................................................................
Limitazione Di Rimedi E Responsabilità19................................................................................................................................................................
限定責任および救済19................................................................................................................................................................
赔偿与责任限制19................................................................................................................................................................
Warnings20................................................................................................................................................................
Chapter 1: Introduction49................................................................................................................................................................
Chapter 2: System Description51................................................................................................................................................................
System Specifications51................................................................................................................................................................
Additional System Specifications53................................................................................................................................................................
Operating Specifications53................................................................................................................................................................
Reagent Consumption54................................................................................................................................................................
Scwo Method Compliance54................................................................................................................................................................
System Overview54................................................................................................................................................................
Figure 1: Analyzer Schematic56................................................................................................................................................................
Sample Flow Path57................................................................................................................................................................
Table 1 Innovox Wetted Materials List59................................................................................................................................................................
Additional System Components60................................................................................................................................................................
System/controller And Electronics60................................................................................................................................................................
Data Outputs61................................................................................................................................................................
Sample Preparation Device Options61................................................................................................................................................................
Clean Water Sample Options61................................................................................................................................................................
Sample Preparation Options61................................................................................................................................................................
2-stream Configuration62................................................................................................................................................................
Specifications - (2-stream Or 5-stream) Clean Water Sampler62................................................................................................................................................................
2-stream High Temperature Configuration62................................................................................................................................................................
Specifications - (2-stream) High Temperature Clean Water Sampler63................................................................................................................................................................
Wastewater Sampler Option63................................................................................................................................................................
Specifications - Wastewater Sampler64................................................................................................................................................................
Mounting Stand64................................................................................................................................................................
Regenerative Air Purifier Option64................................................................................................................................................................
Carrier Gas Co 2 Scrubber Option (on-line)65................................................................................................................................................................
Fail Safe Accessory65................................................................................................................................................................
Ip5665................................................................................................................................................................
Nema 4x Cabinet65................................................................................................................................................................
Hazardous Location Enclosures65................................................................................................................................................................
Sample Filter Panel66................................................................................................................................................................
Sample Peristaltic Pump66................................................................................................................................................................
Chapter 3: Interferences67................................................................................................................................................................
Safety67................................................................................................................................................................
Reliability68................................................................................................................................................................
Analytical Performance68................................................................................................................................................................
Chapter 4: Installation71................................................................................................................................................................
Overview71................................................................................................................................................................
Step 1: Unpack And Inspect The Analyzer71................................................................................................................................................................
Additional Installation Equipment73................................................................................................................................................................
Step 2: Complete The Identification Records73................................................................................................................................................................
Step 3: Select A Location For The Analyzer73................................................................................................................................................................
Mounting Stand Installation73................................................................................................................................................................
Figure 2 Mounting Stand - Clearances74................................................................................................................................................................
Figure 3 Attaching Mounting Brackets On The Analyzer75................................................................................................................................................................
Figure 4 Mounting The Analyzer To The Stand76................................................................................................................................................................
Wall Mount Installation77................................................................................................................................................................
Step 4: Connect The Waste Lines77................................................................................................................................................................
Step 5: Fill The Gas-liquid Separator79................................................................................................................................................................
Step 6: Install Input/output, Cables, And Accessories79................................................................................................................................................................
The Gas-liquid Separator79................................................................................................................................................................
Analog Outputs (tb1)81................................................................................................................................................................
Stream Id81................................................................................................................................................................
Alarm Outputs (tb3)82................................................................................................................................................................
Table 5 Binary Input (tb2)82................................................................................................................................................................
Alarm Outputs (tb4)83................................................................................................................................................................
Installing The 4-20 Ma Connection84................................................................................................................................................................
Installing The Remote Start (binary Input) Connection84................................................................................................................................................................
Installing The Analysis Complete Output Connection85................................................................................................................................................................
Figure 8 Wiring Option - Binary Input Using Analyzer's Internal Supply85................................................................................................................................................................
Figure 9 Wiring Option - Binary Input Using Analyzer's External Supply85................................................................................................................................................................
Installing The Alarms And System Fault Output Connection86................................................................................................................................................................
Installing The Ethernet Connection86................................................................................................................................................................
Connecting The Analyzer To A Computer86................................................................................................................................................................
Installing The Usb Connection87................................................................................................................................................................
Connecting The Analyzer To A Network87................................................................................................................................................................
Step 7: Connecting To A Power Supply88................................................................................................................................................................
Step 8: Connect The Sample Inlet System89................................................................................................................................................................
Installing The Online Sample System89................................................................................................................................................................
Installing The Wastewater Sampler90................................................................................................................................................................
To Install The Wastewater Sampler (velocity Method)91................................................................................................................................................................
Figure 16 Top Wastewater Sampler Bracket W/plate Adapter91................................................................................................................................................................
Figure 17: Lower Wastewater Sampler Bracket92................................................................................................................................................................
Velocity Method - Barb Fittings Identification92................................................................................................................................................................
Figure 19: Velocity Method - Installation93................................................................................................................................................................
Figure 20 Velocity Method - Adjusting The Sipper Tube Height93................................................................................................................................................................
To Install The Wastewater Sampler (overflow Method)94................................................................................................................................................................
Velocity Method - Failsafe Installation94................................................................................................................................................................
Figure 23 Top Wastewater Sampler Bracket W/plate Adapter95................................................................................................................................................................
Lower Wastewater Sampler Bracket95................................................................................................................................................................
Figure 25 Overflow Method - External Sample Pump Position96................................................................................................................................................................
Figure 26 Overflow Method - Barb Fittings Identification96................................................................................................................................................................
Figure 27: Overflow Method - Installation97................................................................................................................................................................
Figure 28 Overflow Method - Adjusting The Sipper Tube Height97................................................................................................................................................................
Installing The Check Standard System98................................................................................................................................................................
Overflow Method - Failsafe Installation98................................................................................................................................................................
Installing The Grab Sample System99................................................................................................................................................................
Step 9: Connect The Reagent And Dilution Water Lines99................................................................................................................................................................
Step 10: Connect The Compressed Gas100................................................................................................................................................................
Installing The Carrier Gas Supply100................................................................................................................................................................
Installing The Gas Supply For The Ip56 Accessory101................................................................................................................................................................
Specifications - Ip56 Accessory102................................................................................................................................................................
Step 11: Turn On Power And Configure Basic Settings102................................................................................................................................................................
Setting The Clock102................................................................................................................................................................
Step 12: Perform A Test Analysis102................................................................................................................................................................
Step 13: Calibrate The Analyzer104................................................................................................................................................................
Chapter 5: Calibration And Verification105................................................................................................................................................................
Handling Standards106................................................................................................................................................................
Prepare Ic Standard Solution106................................................................................................................................................................
Calibration And Verification Options107................................................................................................................................................................
Single-point Calibration107................................................................................................................................................................
Figure 31 Calibration Curve For Single-point Calibration108................................................................................................................................................................
Two-point Calibration109................................................................................................................................................................
Figure 33 Two-point Calibration (point 1 Is Reagent Water)110................................................................................................................................................................
Calibration With More Than Two Points111................................................................................................................................................................
Linear Fit Multi-point Calibration111................................................................................................................................................................
Point-to-point Multi-point Calibration112................................................................................................................................................................
Auto Dilution113................................................................................................................................................................
Blank Correction114................................................................................................................................................................
Calibration Groups114................................................................................................................................................................
Table 8 Maximum Dilution Allowed Using Auto Dilution Feature114................................................................................................................................................................
Preparing For Calibration115................................................................................................................................................................
Save System Settings115................................................................................................................................................................
Perform Maintenance Tasks116................................................................................................................................................................
Setting Up Npoc, Ic, Tc/toc Calibration116................................................................................................................................................................
Calibrating The Analyzer118................................................................................................................................................................
Table 9 Approximate Number Of Calibration Repetitions Possible118................................................................................................................................................................
Editing A Calibration119................................................................................................................................................................
Performing A Calibration Verification121................................................................................................................................................................
Reviewing Calibration And Verification History122................................................................................................................................................................
Table 10 Approximate Number Of Verification Repetitions Possible122................................................................................................................................................................
Chapter 6: Analyzer Operation123................................................................................................................................................................
The Main Screen123................................................................................................................................................................
Figure 38 The Main Screen (grab Mode)124................................................................................................................................................................
The Menu Screen125................................................................................................................................................................
Setting Up Measurements (the Setup Tab)126................................................................................................................................................................
Online Measurements126................................................................................................................................................................
Continuous Measurements127................................................................................................................................................................
Operation With Multiple Streams128................................................................................................................................................................
Cycle Frequency128................................................................................................................................................................
Figure 43 Operation With Five Streams And The Check Standard128................................................................................................................................................................
Configure Online Screen129................................................................................................................................................................
Figure 44 Calculating The Run Time130................................................................................................................................................................
Online Measurement-configuration131................................................................................................................................................................
Figure 46: Stream 1 Screen132................................................................................................................................................................
Check Standards134................................................................................................................................................................
Figure 47: Check Standard Setup Screen135................................................................................................................................................................
Check Standard (setup) Screen137................................................................................................................................................................
Clean Inlet138................................................................................................................................................................
Auto Restart138................................................................................................................................................................
Daily Flush138................................................................................................................................................................
Summary139................................................................................................................................................................
Grab Measurements139................................................................................................................................................................
Figure 51 The Grab (setup) Screen140................................................................................................................................................................
Table 11 Vial Port - Repetitions Possible142................................................................................................................................................................
Rinse143................................................................................................................................................................
Measurement Settings143................................................................................................................................................................
Measure143................................................................................................................................................................
Range144................................................................................................................................................................
Auto Range144................................................................................................................................................................
Acid145................................................................................................................................................................
Oxidizer145................................................................................................................................................................
Repetitions145................................................................................................................................................................
Rejects145................................................................................................................................................................
Repeat Criteria145................................................................................................................................................................
Sparge146................................................................................................................................................................
Flush146................................................................................................................................................................
Manual Dilution146................................................................................................................................................................
Configuring Conversion Factors146................................................................................................................................................................
Figure 52: The Maintenance Tab147................................................................................................................................................................
Figure 54: Configuring The Factor Equation148................................................................................................................................................................
Configuring The Factor Units148................................................................................................................................................................
Figure 56: Configuring The Factor Name149................................................................................................................................................................
User Management150................................................................................................................................................................
Measuring The Blank151................................................................................................................................................................
Viewing And Exporting Data152................................................................................................................................................................
Viewing Data On Screen152................................................................................................................................................................
Exporting Data152................................................................................................................................................................
The Data Screen152................................................................................................................................................................
Export (data) Screen153................................................................................................................................................................
Figure 60: Export Data Screen154................................................................................................................................................................
Reviewing Exported Data155................................................................................................................................................................
Data Fields Output155................................................................................................................................................................
Setting Up Input And Output (i/o)156................................................................................................................................................................
The I/o Tab156................................................................................................................................................................
Connecting The Analyzer To A Network Via Ethernet156................................................................................................................................................................
Configuring The Analyzer's Ip Address156................................................................................................................................................................
Configuring A Personal Computer157................................................................................................................................................................
Collecting Historical And Real-time Data159................................................................................................................................................................
To Collect Real-time Data (w/ethernet Connection)159................................................................................................................................................................
Using The Ethernet Connection And Modbus160................................................................................................................................................................
Configuring Alarm Outputs160................................................................................................................................................................
Figure 62 Alarm Output Screen161................................................................................................................................................................
Changing The Alarms On Or Off Setting162................................................................................................................................................................
Resetting Alarms162................................................................................................................................................................
Printer Setup162................................................................................................................................................................
Liquid Sensor Setup163................................................................................................................................................................
To Enable A Liquid Sensor163................................................................................................................................................................
Figure 65 Liquid Sensor Location - Hazardous Location Enclosure (atex Or C1/d2)164................................................................................................................................................................
Configuring Advanced Setup165................................................................................................................................................................
The Maintenance Tab165................................................................................................................................................................
Setting Analyzer Name And Location165................................................................................................................................................................
Setting System Properties166................................................................................................................................................................
System Properties Screen166................................................................................................................................................................
Upgrade Option167................................................................................................................................................................
Gas Valve Pid Parameters167................................................................................................................................................................
Cleaning The Analyzer Screen168................................................................................................................................................................
Setting The Fail Safe Option169................................................................................................................................................................
Setting The Keyboard Options169................................................................................................................................................................
Setting The Display Options169................................................................................................................................................................
Archiving The Data History170................................................................................................................................................................
Shutting Down The Analyzer170................................................................................................................................................................
Checking The Software Version171................................................................................................................................................................
Chapter 7: Operation With The Filter Panel173................................................................................................................................................................
Operation Of The Filter Panel With A Sample Pump173................................................................................................................................................................
Control Of Filter Panel173................................................................................................................................................................
Figure 69: Blowback Pulses And Sample Flow Time174................................................................................................................................................................
Flush/blowback Screen175................................................................................................................................................................
Chapter 8: Maintenance177................................................................................................................................................................
Recommended Spare Parts178................................................................................................................................................................
Periodic Maintenance Tasks178................................................................................................................................................................
Periodic Inspections178................................................................................................................................................................
Consumables Replacement Schedule178................................................................................................................................................................
Preparing The Oxidizer Solution179................................................................................................................................................................
Figure 72 Aging Of 30% (w/v) Na 2 S 2 O 8 In Hdpe Bottles179................................................................................................................................................................
Preparing The Persulfate Oxidizing Solution180................................................................................................................................................................
To Prepare The Oxidizing Solution180................................................................................................................................................................
Preparing The Acid180................................................................................................................................................................
Adding The Dilution Water180................................................................................................................................................................
Performing A Flush180................................................................................................................................................................
Cleaning The Analyzer181................................................................................................................................................................
Cleaning The Gas-liquid Separator181................................................................................................................................................................
Figure 73 The Gas-liquid Separator182................................................................................................................................................................
Cleaning The Sparger183................................................................................................................................................................
The Sparger183................................................................................................................................................................
Lubricating The Syringe184................................................................................................................................................................
Unscrewing The Syringe Base185................................................................................................................................................................
Figure 75 Locating The Syringe Screw And Washers185................................................................................................................................................................
Figure 77 Removing The Syringe186................................................................................................................................................................
Figure 79 Removing The Stopper187................................................................................................................................................................
Consumables Replacement188................................................................................................................................................................
Replacing The Pinch Valve Tubing188................................................................................................................................................................
Figure 81 Valve Locations - Innovox On-line Toc Analyzer190................................................................................................................................................................
Replacing The Peristaltic Pump Head Tubing191................................................................................................................................................................
Replacing The Ndir Filter192................................................................................................................................................................
Entering Consumables Installation Information193................................................................................................................................................................
Other Maintenance Tasks193................................................................................................................................................................
Replacing The High Pressure Valve Seals194................................................................................................................................................................
Figure 83: The High Pressure Valve Seal - Before Removal195................................................................................................................................................................
The High Pressure Valve Seal - After Removal195................................................................................................................................................................
Table 15 2-year Maintenance Worksheet - Sievers Innovox Online Toc Analyzer196................................................................................................................................................................
Chapter 9: Troubleshooting199................................................................................................................................................................
Reviewing Warnings And Errors199................................................................................................................................................................
Analyzer Warnings And Error Messages200................................................................................................................................................................
Other Software Errors210................................................................................................................................................................
Visual Inspection210................................................................................................................................................................
Figure 85 The Fluidics Side Of The Analyzer211................................................................................................................................................................
Figure 86 The Electronics Side Of The Analyzer212................................................................................................................................................................
Figure 87 Electronics In The Top Of The Analyzer213................................................................................................................................................................
Figure 88: Analyzer Schematic214................................................................................................................................................................
External Inspection215................................................................................................................................................................
Internal Inspection215................................................................................................................................................................
Reviewing Solutions For Basic Problems216................................................................................................................................................................
The Analyzer Will Not Power On216................................................................................................................................................................
Diagnostics217................................................................................................................................................................
The Diagnostics Screen217................................................................................................................................................................
Valves218................................................................................................................................................................
Flow Control Valves218................................................................................................................................................................
The Flow Control Valve Screen218................................................................................................................................................................
Figure 93 Sampler Handler Valves Screen219................................................................................................................................................................
Gas Valves220................................................................................................................................................................
Diagnostic Result Screen220................................................................................................................................................................
Gas Valve Testing Criteria221................................................................................................................................................................
Pneumatic Valves222................................................................................................................................................................
Pneumatic Valve Screen222................................................................................................................................................................
Ndir223................................................................................................................................................................
Heater223................................................................................................................................................................
Heater Testing Criteria224................................................................................................................................................................
Liquid Flow Check225................................................................................................................................................................
Gas Leak Checks226................................................................................................................................................................
Figure 100 The Gas Leak Check Screen227................................................................................................................................................................
Figure 101 Gas Manifold Leak Check229................................................................................................................................................................
Figure 102: Reactor Inlet Valve Leak Check231................................................................................................................................................................
Figure 103: Reactor Bypass Leak Check233................................................................................................................................................................
Figure 104 Reactor Leak Check235................................................................................................................................................................
Figure 105 Reactor Outlet Valve Check237................................................................................................................................................................
Leak Check238................................................................................................................................................................
Analog Output239................................................................................................................................................................
Binary Output239................................................................................................................................................................
Binary Input240................................................................................................................................................................
Figure 108 Binary Input Check241................................................................................................................................................................
Pumps242................................................................................................................................................................
Export Diagnostic Data243................................................................................................................................................................
Testing The Sparger243................................................................................................................................................................
Contacting Technical Support243................................................................................................................................................................
Returning The Analyzer To Ge Analytical Instruments244................................................................................................................................................................
Appendix A: Analyzer Dimension Diagrams247................................................................................................................................................................
Analyzer Dimensions (front View)247................................................................................................................................................................
Analyzer Dimensions (right Side View)248................................................................................................................................................................
Analyzer Dimensions (left Side View)249................................................................................................................................................................
Appendix B: Acronyms And Definitions251................................................................................................................................................................
Appendix C: Importing Analyzer Data Into A Spreadsheet255................................................................................................................................................................
Importing Data Into A Spreadsheet Program255................................................................................................................................................................
Figure 114 Microsoft Excel Spreadsheet Screen — Text Import Wizard - Step 1256................................................................................................................................................................
Figure 116 Microsoft Excel Spreadsheet Program — Text Import Wizard - Step 3257................................................................................................................................................................
Appendix D: Modbus Map259................................................................................................................................................................
Index265................................................................................................................................................................

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GE Sievers Innovox Operation And Maintenance Manual

GE Sievers Innovox Operation And Maintenance Manual (238 pages)

On-Line TOC Analyzer  
Brand: GE | Category: Measuring Instruments | Size: 12.08 MB
Table of contents
Identification Records3................................................................................................................................................................
Table Of Contents4................................................................................................................................................................
List Of Tables10................................................................................................................................................................
List Of Figures11................................................................................................................................................................
Revision History14................................................................................................................................................................
Confidentiality15................................................................................................................................................................
Declaration Of Conformity16................................................................................................................................................................
Standard Limited Warranty16................................................................................................................................................................
Limitation Of Remedies And Liability17................................................................................................................................................................
Limitación De Remedios Y Responsabilidad17................................................................................................................................................................
Limites De Correction Et De Fiabilité17................................................................................................................................................................
Beschränkte Ansprüche Und Haftung17................................................................................................................................................................
Limitazione Di Rimedi E Responsabilità18................................................................................................................................................................
限定責任および救済18................................................................................................................................................................
赔偿与责任限制18................................................................................................................................................................
Warnings19................................................................................................................................................................
Chapter 1: Introduction47................................................................................................................................................................
Chapter 2: System Description49................................................................................................................................................................
System Specifications49................................................................................................................................................................
System Overview52................................................................................................................................................................
Figure 1: Analyzer Schematic53................................................................................................................................................................
Sample Flow Path54................................................................................................................................................................
Additional System Components56................................................................................................................................................................
System/controller And Electronics56................................................................................................................................................................
Data Outputs57................................................................................................................................................................
Major Accessories And Configurations57................................................................................................................................................................
2-stream Configuration57................................................................................................................................................................
5-stream Configuration58................................................................................................................................................................
Mounting Stand58................................................................................................................................................................
Air Purifier58................................................................................................................................................................
Fail Safe Accessory58................................................................................................................................................................
Ip5658................................................................................................................................................................
Nema 4x Cabinet58................................................................................................................................................................
Sample Filter Panel59................................................................................................................................................................
Sample Peristaltic Pump59................................................................................................................................................................
Chapter 3: Interferences61................................................................................................................................................................
Safety61................................................................................................................................................................
Reliability62................................................................................................................................................................
Analytical Performance62................................................................................................................................................................
Chapter 4: Installation65................................................................................................................................................................
Overview65................................................................................................................................................................
Step 1: Unpack And Inspect The Analyzer65................................................................................................................................................................
Additional Installation Equipment66................................................................................................................................................................
Step 2: Complete The Identification Records67................................................................................................................................................................
Step 3: Select A Location For The Analyzer67................................................................................................................................................................
Mounting Stand Installation67................................................................................................................................................................
Figure 2 Mounting Stand - Clearances68................................................................................................................................................................
Figure 3 Attaching Mounting Brackets On The Analyzer69................................................................................................................................................................
Figure 4 Mounting The Analyzer To The Stand70................................................................................................................................................................
Wall Mount Installation71................................................................................................................................................................
Step 4: Connect The Waste Lines71................................................................................................................................................................
Step 5: Fill The Gas-liquid Separator73................................................................................................................................................................
The Gas-liquid Separator73................................................................................................................................................................
Step 6: Install Input/output, Cables, And Accessories74................................................................................................................................................................
Table 1 Analog Outputs (tb1)75................................................................................................................................................................
Alarm Outputs (tb3)76................................................................................................................................................................
Table76................................................................................................................................................................
Alarm Outputs (tb4)77................................................................................................................................................................
Installing The 4-20 Ma Connection78................................................................................................................................................................
Installing The Remote Start (binary Input) Connection78................................................................................................................................................................
Installing The Analysis Complete Output Connection79................................................................................................................................................................
Figure 8 Wiring Option - Binary Input Using Analyzer's Internal Supply79................................................................................................................................................................
Figure 9 Wiring Option - Binary Input Using Analyzer's External Supply79................................................................................................................................................................
Installing The Alarms And System Fault Output Connection80................................................................................................................................................................
Installing The Ethernet Connection80................................................................................................................................................................
Connecting The Analyzer To A Computer80................................................................................................................................................................
Installing The Usb Connection81................................................................................................................................................................
Connecting The Analyzer To A Network81................................................................................................................................................................
Step 7: Connecting To A Power Supply82................................................................................................................................................................
Step 8: Connect The Sample Inlet System83................................................................................................................................................................
Installing The Online Sample System83................................................................................................................................................................
Installing The Check Standard System84................................................................................................................................................................
Installing The Grab Sample System84................................................................................................................................................................
Step 9: Connect The Reagent And Dilution Water Lines84................................................................................................................................................................
Step 10: Connect The Compressed Gas85................................................................................................................................................................
Installing The Carrier Gas Supply85................................................................................................................................................................
Installing The Gas Supply For The Ip56 Accessory86................................................................................................................................................................
Step 11: Turn On Power And Configure Basic Settings86................................................................................................................................................................
Setting The Clock87................................................................................................................................................................
Step 12: Perform A Test Analysis87................................................................................................................................................................
Step 13: Calibrate The Analyzer88................................................................................................................................................................
Chapter 5: Calibration And Verification89................................................................................................................................................................
Handling Standards90................................................................................................................................................................
Prepare Ic Standard Solution90................................................................................................................................................................
Calibration And Verification Options91................................................................................................................................................................
Single-point Calibration91................................................................................................................................................................
Two-point Calibration92................................................................................................................................................................
Two-point Calibration (point 1 Is Standard)93................................................................................................................................................................
Two-point Calibration (point 1 Is Reagent Water)94................................................................................................................................................................
Calibration With More Than Two Points95................................................................................................................................................................
Linear Fit Multi-point Calibration95................................................................................................................................................................
Point-to-point Multi-point Calibration96................................................................................................................................................................
Auto Dilution97................................................................................................................................................................
Blank Correction98................................................................................................................................................................
Calibration Groups98................................................................................................................................................................
Table 5 Maximum Dilution Allowed Using Auto Dilution Feature98................................................................................................................................................................
Preparing For Calibration99................................................................................................................................................................
Save System Settings99................................................................................................................................................................
Perform Maintenance Tasks100................................................................................................................................................................
Setting Up Npoc, Ic, Tc/toc Calibration100................................................................................................................................................................
Calibrating The Analyzer102................................................................................................................................................................
Table 6 Approximate Number Of Calibration Repetitions Possible102................................................................................................................................................................
Editing A Calibration104................................................................................................................................................................
Performing A Calibration Verification105................................................................................................................................................................
Reviewing Calibration And Verification History106................................................................................................................................................................
Table 7 Approximate Number Of Verification Repetitions Possible106................................................................................................................................................................
Chapter 6: Analyzer Operation107................................................................................................................................................................
The Main Screen108................................................................................................................................................................
The Menu Screen109................................................................................................................................................................
Setting Up Measurements (the Setup Tab)110................................................................................................................................................................
Online Measurements111................................................................................................................................................................
Continuous Measurements111................................................................................................................................................................
Operation With Multiple Streams112................................................................................................................................................................
Cycle Frequency113................................................................................................................................................................
Figure 25 Operation With Five Streams And The Check Standard113................................................................................................................................................................
Figure 26 Calculating The Run Time114................................................................................................................................................................
Configuring Online Measurements115................................................................................................................................................................
Configure Online Screen115................................................................................................................................................................
Stream 1 Screen116................................................................................................................................................................
Check Standards118................................................................................................................................................................
Figure 29: Check Standard Setup Screen119................................................................................................................................................................
Check Standard (setup) Screen121................................................................................................................................................................
Clean Inlet122................................................................................................................................................................
Auto Restart122................................................................................................................................................................
Daily Flush122................................................................................................................................................................
Summary123................................................................................................................................................................
Grab Measurements123................................................................................................................................................................
Table 8 Vial Port - Repetitions Possible126................................................................................................................................................................
Rinse127................................................................................................................................................................
Measurement Settings127................................................................................................................................................................
Measure127................................................................................................................................................................
Range128................................................................................................................................................................
Auto Range128................................................................................................................................................................
Acid128................................................................................................................................................................
Table 9 Ranges In The Innovox Online Toc Analyzer128................................................................................................................................................................
Oxidizer129................................................................................................................................................................
Repetitions129................................................................................................................................................................
Rejects129................................................................................................................................................................
Repeat Criteria129................................................................................................................................................................
Sparge129................................................................................................................................................................
Flush130................................................................................................................................................................
Manual Dilution130................................................................................................................................................................
Conversion Factors130................................................................................................................................................................
User Management131................................................................................................................................................................
Measuring The Blank132................................................................................................................................................................
Viewing And Exporting Data133................................................................................................................................................................
Viewing Data On Screen133................................................................................................................................................................
The Data Screen133................................................................................................................................................................
Exporting Data134................................................................................................................................................................
Export (data) Screen134................................................................................................................................................................
Figure 36: Export Data Screen135................................................................................................................................................................
Reviewing Exported Data136................................................................................................................................................................
Data Fields Output136................................................................................................................................................................
Setting Up Input And Output (i/o)137................................................................................................................................................................
Connecting The Analyzer To A Network Via Ethernet137................................................................................................................................................................
Configuring The Analyzer's Ip Address137................................................................................................................................................................
Configuring A Personal Computer138................................................................................................................................................................
Collecting Real-time Data140................................................................................................................................................................
Using The Ethernet Connection And Modbus140................................................................................................................................................................
Configuring Alarm Outputs140................................................................................................................................................................
Resetting Alarms141................................................................................................................................................................
Printing Data141................................................................................................................................................................
Figure 39 Print Data Screen142................................................................................................................................................................
Configuring Advanced Setup143................................................................................................................................................................
Setting Analyzer Name And Location143................................................................................................................................................................
Setting System Properties144................................................................................................................................................................
System Properties Screen144................................................................................................................................................................
Upgrade Option145................................................................................................................................................................
Cleaning The Analyzer Screen145................................................................................................................................................................
Setting The Fail Safe Option145................................................................................................................................................................
Setting The Keyboard Options146................................................................................................................................................................
Setting The Display Options146................................................................................................................................................................
Archiving The Data History146................................................................................................................................................................
Shutting Down The Analyzer147................................................................................................................................................................
Chapter 7: Operation With The Filter Panel149................................................................................................................................................................
Operation Of Filter Panel With Sample Pump149................................................................................................................................................................
Control Of Filter Panel149................................................................................................................................................................
Figure 42: Blowback Pulses And Delay150................................................................................................................................................................
Flush/blowback Screen151................................................................................................................................................................
Chapter 8: Maintenance153................................................................................................................................................................
Consumables Replacement Schedule153................................................................................................................................................................
Recommended Spare Parts154................................................................................................................................................................
Periodic Maintenance Tasks154................................................................................................................................................................
Periodic Inspections154................................................................................................................................................................
Preparing The Oxidizer Solution154................................................................................................................................................................
Figure 45 Aging Of 30% (w/v) Na155................................................................................................................................................................
Preparing The Acid156................................................................................................................................................................
Adding The Dilution Water156................................................................................................................................................................
Performing A Flush156................................................................................................................................................................
Cleaning The Analyzer157................................................................................................................................................................
Cleaning The Gas-liquid Separator157................................................................................................................................................................
Cleaning The Sparger158................................................................................................................................................................
The Sparger158................................................................................................................................................................
Figure 47 The Sparger159................................................................................................................................................................
Lubricating The Syringe160................................................................................................................................................................
Figure 49 Unscrewing The Syringe Base161................................................................................................................................................................
Figure 51 Pulling Out The Plunger162................................................................................................................................................................
Consumables Replacement163................................................................................................................................................................
Replacing The Pinch Valve Tubing163................................................................................................................................................................
Figure 54 Valve Locations - Innovox On-line Toc Analyzer165................................................................................................................................................................
Replacing The Peristaltic Pumps166................................................................................................................................................................
Replacing The Ndir Filter166................................................................................................................................................................
Figure 55: Replacing The Ndir Filter167................................................................................................................................................................
Entering Consumables Installation Information168................................................................................................................................................................
Other Maintenance Tasks168................................................................................................................................................................
Replacing The High Pressure Valve Seals168................................................................................................................................................................
Figure 56: The High Pressure Valve Seal - Before Removal169................................................................................................................................................................
The High Pressure Valve Seal - After Removal169................................................................................................................................................................
Table 12 2-year Maintenance Worksheet - Sievers Innovox Online Toc Analyzer170................................................................................................................................................................
Chapter 9: Troubleshooting173................................................................................................................................................................
Reviewing Warnings And Errors173................................................................................................................................................................
Analyzer Warnings And Error Messages174................................................................................................................................................................
Other Software Errors182................................................................................................................................................................
Visual Inspection182................................................................................................................................................................
Figure 58 The Fluidics Side Of The Analyzer183................................................................................................................................................................
Figure 59 The Electronics Side Of The Analyzer184................................................................................................................................................................
Figure 60 Electronics In The Top Of The Analyzer185................................................................................................................................................................
Figure 61: Analyzer Schematic186................................................................................................................................................................
External Inspection187................................................................................................................................................................
Internal Inspection187................................................................................................................................................................
Figure 62 Connections To The Gas-liquid Separator188................................................................................................................................................................
Reviewing Solutions For Basic Problems189................................................................................................................................................................
The Analyzer Will Not Power On189................................................................................................................................................................
Diagnostics189................................................................................................................................................................
The Diagnostics Screen189................................................................................................................................................................
Pinch Valves190................................................................................................................................................................
Gas Valves191................................................................................................................................................................
Ndir192................................................................................................................................................................
The Temperatures Display On The Ndir Screen192................................................................................................................................................................
Heater193................................................................................................................................................................
Liquid Flow194................................................................................................................................................................
Gas Leak Checks195................................................................................................................................................................
Gas Manifold Leak Check195................................................................................................................................................................
Figure 70: Gas Manifold Leak Check197................................................................................................................................................................
Reactor Inlet Valve Leak Check198................................................................................................................................................................
Figure 71: Reactor Inlet Valve Leak Check199................................................................................................................................................................
Reactor Bypass Leak Check200................................................................................................................................................................
Figure 72: Reactor Bypass Leak Check201................................................................................................................................................................
Reactor Leak Check202................................................................................................................................................................
Figure 73: Reactor Leak Check203................................................................................................................................................................
Reactor Outlet Valve Leak Check204................................................................................................................................................................
Figure 74 Reactor Valve Outlet Check205................................................................................................................................................................
Gas Liquid Separator, Ndir Filter, Ndir Sample Path And Sparger Leak Check206................................................................................................................................................................
Pneumatic Valves206................................................................................................................................................................
Pneumatic Valve Check206................................................................................................................................................................
Analog Output207................................................................................................................................................................
Binary Output207................................................................................................................................................................
Binary Input208................................................................................................................................................................
Sample Pumps209................................................................................................................................................................
Export Diagnostic Data210................................................................................................................................................................
Contacting Technical Support210................................................................................................................................................................
Returning The Analyzer To Ge Analytical Instruments210................................................................................................................................................................
Appendix A: Analyzer Dimension Diagrams213................................................................................................................................................................
Analyzer Dimensions (front View)213................................................................................................................................................................
Analyzer Dimensions (right Side View)214................................................................................................................................................................
Analyzer Dimensions (left Side View)215................................................................................................................................................................
Appendix B: Acronyms And Definitions217................................................................................................................................................................
Appendix C: Transferring Data To A Pc221................................................................................................................................................................
Using Hyperterminal221................................................................................................................................................................
Figure 84 Entering Connection Information222................................................................................................................................................................
Figure 85 Saving Data On Hyperterminal223................................................................................................................................................................
Importing Data Into A Spreadsheet Program224................................................................................................................................................................
Figure 87 Microsoft Excel Spreadsheet Screen — Text Import Wizard - Step 1225................................................................................................................................................................
Figure 89 Microsoft Excel Spreadsheet Program — Text Import Wizard - Step 3226................................................................................................................................................................
Appendix D: Modbus Map227................................................................................................................................................................
Index233................................................................................................................................................................

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