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GE Sievers Innovox Operation And Maintenance Manual (270 pages)

TOC analyzer

Brand: GE | Category: Analytical Instruments | Size: 14.81 MB

Identification Records3................................................................................................................................................................

Table Of Contents4................................................................................................................................................................

List Of Tables10................................................................................................................................................................

List Of Figures11................................................................................................................................................................

Revision History15................................................................................................................................................................

Confidentiality16................................................................................................................................................................

Declaration Of Conformity17................................................................................................................................................................

Standard Limited Warranty17................................................................................................................................................................

Limitation Of Remedies And Liability18................................................................................................................................................................

Limitación De Remedios Y Responsabilidad18................................................................................................................................................................

Limites De Correction Et De Fiabilité18................................................................................................................................................................

Beschränkte Ansprüche Und Haftung18................................................................................................................................................................

Limitazione Di Rimedi E Responsabilità19................................................................................................................................................................

限定責任および救済19................................................................................................................................................................

赔偿与责任限制19................................................................................................................................................................

Warnings20................................................................................................................................................................

Chapter 1: Introduction49................................................................................................................................................................

Chapter 2: System Description51................................................................................................................................................................

System Specifications51................................................................................................................................................................

Additional System Specifications53................................................................................................................................................................

Operating Specifications53................................................................................................................................................................

Reagent Consumption54................................................................................................................................................................

Scwo Method Compliance54................................................................................................................................................................

System Overview54................................................................................................................................................................

Figure 1: Analyzer Schematic56................................................................................................................................................................

Sample Flow Path57................................................................................................................................................................

Table 1 Innovox Wetted Materials List59................................................................................................................................................................

Additional System Components60................................................................................................................................................................

System/controller And Electronics60................................................................................................................................................................

Data Outputs61................................................................................................................................................................

Sample Preparation Device Options61................................................................................................................................................................

Clean Water Sample Options61................................................................................................................................................................

Sample Preparation Options61................................................................................................................................................................

2-stream Configuration62................................................................................................................................................................

Specifications - (2-stream Or 5-stream) Clean Water Sampler62................................................................................................................................................................

2-stream High Temperature Configuration62................................................................................................................................................................

Specifications - (2-stream) High Temperature Clean Water Sampler63................................................................................................................................................................

Wastewater Sampler Option63................................................................................................................................................................

Specifications - Wastewater Sampler64................................................................................................................................................................

Mounting Stand64................................................................................................................................................................

Regenerative Air Purifier Option64................................................................................................................................................................

Carrier Gas Co 2 Scrubber Option (on-line)65................................................................................................................................................................

Fail Safe Accessory65................................................................................................................................................................

Ip5665................................................................................................................................................................

Nema 4x Cabinet65................................................................................................................................................................

Hazardous Location Enclosures65................................................................................................................................................................

Sample Filter Panel66................................................................................................................................................................

Sample Peristaltic Pump66................................................................................................................................................................

Chapter 3: Interferences67................................................................................................................................................................

Safety67................................................................................................................................................................

Reliability68................................................................................................................................................................

Analytical Performance68................................................................................................................................................................

Chapter 4: Installation71................................................................................................................................................................

Overview71................................................................................................................................................................

Step 1: Unpack And Inspect The Analyzer71................................................................................................................................................................

Additional Installation Equipment73................................................................................................................................................................

Step 2: Complete The Identification Records73................................................................................................................................................................

Step 3: Select A Location For The Analyzer73................................................................................................................................................................

Mounting Stand Installation73................................................................................................................................................................

Figure 2 Mounting Stand - Clearances74................................................................................................................................................................

Figure 3 Attaching Mounting Brackets On The Analyzer75................................................................................................................................................................

Figure 4 Mounting The Analyzer To The Stand76................................................................................................................................................................

Wall Mount Installation77................................................................................................................................................................

Step 4: Connect The Waste Lines77................................................................................................................................................................

Step 5: Fill The Gas-liquid Separator79................................................................................................................................................................

Step 6: Install Input/output, Cables, And Accessories79................................................................................................................................................................

The Gas-liquid Separator79................................................................................................................................................................

Analog Outputs (tb1)81................................................................................................................................................................

Stream Id81................................................................................................................................................................

Alarm Outputs (tb3)82................................................................................................................................................................

Table 5 Binary Input (tb2)82................................................................................................................................................................

Alarm Outputs (tb4)83................................................................................................................................................................

Installing The 4-20 Ma Connection84................................................................................................................................................................

Installing The Remote Start (binary Input) Connection84................................................................................................................................................................

Installing The Analysis Complete Output Connection85................................................................................................................................................................

Figure 8 Wiring Option - Binary Input Using Analyzer's Internal Supply85................................................................................................................................................................

Figure 9 Wiring Option - Binary Input Using Analyzer's External Supply85................................................................................................................................................................

Installing The Alarms And System Fault Output Connection86................................................................................................................................................................

Installing The Ethernet Connection86................................................................................................................................................................

Connecting The Analyzer To A Computer86................................................................................................................................................................

Installing The Usb Connection87................................................................................................................................................................

Connecting The Analyzer To A Network87................................................................................................................................................................

Step 7: Connecting To A Power Supply88................................................................................................................................................................

Step 8: Connect The Sample Inlet System89................................................................................................................................................................

Installing The Online Sample System89................................................................................................................................................................

Installing The Wastewater Sampler90................................................................................................................................................................

To Install The Wastewater Sampler (velocity Method)91................................................................................................................................................................

Figure 16 Top Wastewater Sampler Bracket W/plate Adapter91................................................................................................................................................................

Figure 17: Lower Wastewater Sampler Bracket92................................................................................................................................................................

Velocity Method - Barb Fittings Identification92................................................................................................................................................................

Figure 19: Velocity Method - Installation93................................................................................................................................................................

Figure 20 Velocity Method - Adjusting The Sipper Tube Height93................................................................................................................................................................

To Install The Wastewater Sampler (overflow Method)94................................................................................................................................................................

Velocity Method - Failsafe Installation94................................................................................................................................................................

Figure 23 Top Wastewater Sampler Bracket W/plate Adapter95................................................................................................................................................................

Lower Wastewater Sampler Bracket95................................................................................................................................................................

Figure 25 Overflow Method - External Sample Pump Position96................................................................................................................................................................

Figure 26 Overflow Method - Barb Fittings Identification96................................................................................................................................................................

Figure 27: Overflow Method - Installation97................................................................................................................................................................

Figure 28 Overflow Method - Adjusting The Sipper Tube Height97................................................................................................................................................................

Installing The Check Standard System98................................................................................................................................................................

Overflow Method - Failsafe Installation98................................................................................................................................................................

Installing The Grab Sample System99................................................................................................................................................................

Step 9: Connect The Reagent And Dilution Water Lines99................................................................................................................................................................

Step 10: Connect The Compressed Gas100................................................................................................................................................................

Installing The Carrier Gas Supply100................................................................................................................................................................

Installing The Gas Supply For The Ip56 Accessory101................................................................................................................................................................

Specifications - Ip56 Accessory102................................................................................................................................................................

Step 11: Turn On Power And Configure Basic Settings102................................................................................................................................................................

Setting The Clock102................................................................................................................................................................

Step 12: Perform A Test Analysis102................................................................................................................................................................

Step 13: Calibrate The Analyzer104................................................................................................................................................................

Chapter 5: Calibration And Verification105................................................................................................................................................................

Handling Standards106................................................................................................................................................................

Prepare Ic Standard Solution106................................................................................................................................................................

Calibration And Verification Options107................................................................................................................................................................

Single-point Calibration107................................................................................................................................................................

Figure 31 Calibration Curve For Single-point Calibration108................................................................................................................................................................

Two-point Calibration109................................................................................................................................................................

Figure 33 Two-point Calibration (point 1 Is Reagent Water)110................................................................................................................................................................

Calibration With More Than Two Points111................................................................................................................................................................

Linear Fit Multi-point Calibration111................................................................................................................................................................

Point-to-point Multi-point Calibration112................................................................................................................................................................

Auto Dilution113................................................................................................................................................................

Blank Correction114................................................................................................................................................................

Calibration Groups114................................................................................................................................................................

Table 8 Maximum Dilution Allowed Using Auto Dilution Feature114................................................................................................................................................................

Preparing For Calibration115................................................................................................................................................................

Save System Settings115................................................................................................................................................................

Perform Maintenance Tasks116................................................................................................................................................................

Setting Up Npoc, Ic, Tc/toc Calibration116................................................................................................................................................................

Calibrating The Analyzer118................................................................................................................................................................

Table 9 Approximate Number Of Calibration Repetitions Possible118................................................................................................................................................................

Editing A Calibration119................................................................................................................................................................

Performing A Calibration Verification121................................................................................................................................................................

Reviewing Calibration And Verification History122................................................................................................................................................................

Table 10 Approximate Number Of Verification Repetitions Possible122................................................................................................................................................................

Chapter 6: Analyzer Operation123................................................................................................................................................................

The Main Screen123................................................................................................................................................................

Figure 38 The Main Screen (grab Mode)124................................................................................................................................................................

The Menu Screen125................................................................................................................................................................

Setting Up Measurements (the Setup Tab)126................................................................................................................................................................

Online Measurements126................................................................................................................................................................

Continuous Measurements127................................................................................................................................................................

Operation With Multiple Streams128................................................................................................................................................................

Cycle Frequency128................................................................................................................................................................

Figure 43 Operation With Five Streams And The Check Standard128................................................................................................................................................................

Configure Online Screen129................................................................................................................................................................

Figure 44 Calculating The Run Time130................................................................................................................................................................

Online Measurement-configuration131................................................................................................................................................................

Figure 46: Stream 1 Screen132................................................................................................................................................................

Check Standards134................................................................................................................................................................

Figure 47: Check Standard Setup Screen135................................................................................................................................................................

Check Standard (setup) Screen137................................................................................................................................................................

Clean Inlet138................................................................................................................................................................

Auto Restart138................................................................................................................................................................

Daily Flush138................................................................................................................................................................

Summary139................................................................................................................................................................

Grab Measurements139................................................................................................................................................................

Figure 51 The Grab (setup) Screen140................................................................................................................................................................

Table 11 Vial Port - Repetitions Possible142................................................................................................................................................................

Rinse143................................................................................................................................................................

Measurement Settings143................................................................................................................................................................

Measure143................................................................................................................................................................

Range144................................................................................................................................................................

Auto Range144................................................................................................................................................................

Acid145................................................................................................................................................................

Oxidizer145................................................................................................................................................................

Repetitions145................................................................................................................................................................

Rejects145................................................................................................................................................................

Repeat Criteria145................................................................................................................................................................

Sparge146................................................................................................................................................................

Flush146................................................................................................................................................................

Manual Dilution146................................................................................................................................................................

Configuring Conversion Factors146................................................................................................................................................................

Figure 52: The Maintenance Tab147................................................................................................................................................................

Figure 54: Configuring The Factor Equation148................................................................................................................................................................

Configuring The Factor Units148................................................................................................................................................................

Figure 56: Configuring The Factor Name149................................................................................................................................................................

User Management150................................................................................................................................................................

Measuring The Blank151................................................................................................................................................................

Viewing And Exporting Data152................................................................................................................................................................

Viewing Data On Screen152................................................................................................................................................................

Exporting Data152................................................................................................................................................................

The Data Screen152................................................................................................................................................................

Export (data) Screen153................................................................................................................................................................

Figure 60: Export Data Screen154................................................................................................................................................................

Reviewing Exported Data155................................................................................................................................................................

Data Fields Output155................................................................................................................................................................

Setting Up Input And Output (i/o)156................................................................................................................................................................

The I/o Tab156................................................................................................................................................................

Connecting The Analyzer To A Network Via Ethernet156................................................................................................................................................................

Configuring The Analyzer's Ip Address156................................................................................................................................................................

Configuring A Personal Computer157................................................................................................................................................................

Collecting Historical And Real-time Data159................................................................................................................................................................

To Collect Real-time Data (w/ethernet Connection)159................................................................................................................................................................

Using The Ethernet Connection And Modbus160................................................................................................................................................................

Configuring Alarm Outputs160................................................................................................................................................................

Figure 62 Alarm Output Screen161................................................................................................................................................................

Changing The Alarms On Or Off Setting162................................................................................................................................................................

Resetting Alarms162................................................................................................................................................................

Printer Setup162................................................................................................................................................................

Liquid Sensor Setup163................................................................................................................................................................

To Enable A Liquid Sensor163................................................................................................................................................................

Figure 65 Liquid Sensor Location - Hazardous Location Enclosure (atex Or C1/d2)164................................................................................................................................................................

Configuring Advanced Setup165................................................................................................................................................................

The Maintenance Tab165................................................................................................................................................................

Setting Analyzer Name And Location165................................................................................................................................................................

Setting System Properties166................................................................................................................................................................

System Properties Screen166................................................................................................................................................................

Upgrade Option167................................................................................................................................................................

Gas Valve Pid Parameters167................................................................................................................................................................

Cleaning The Analyzer Screen168................................................................................................................................................................

Setting The Fail Safe Option169................................................................................................................................................................

Setting The Keyboard Options169................................................................................................................................................................

Setting The Display Options169................................................................................................................................................................

Archiving The Data History170................................................................................................................................................................

Shutting Down The Analyzer170................................................................................................................................................................

Checking The Software Version171................................................................................................................................................................

Chapter 7: Operation With The Filter Panel173................................................................................................................................................................

Operation Of The Filter Panel With A Sample Pump173................................................................................................................................................................

Control Of Filter Panel173................................................................................................................................................................

Figure 69: Blowback Pulses And Sample Flow Time174................................................................................................................................................................

Flush/blowback Screen175................................................................................................................................................................

Chapter 8: Maintenance177................................................................................................................................................................

Recommended Spare Parts178................................................................................................................................................................

Periodic Maintenance Tasks178................................................................................................................................................................

Periodic Inspections178................................................................................................................................................................

Consumables Replacement Schedule178................................................................................................................................................................

Preparing The Oxidizer Solution179................................................................................................................................................................

Figure 72 Aging Of 30% (w/v) Na 2 S 2 O 8 In Hdpe Bottles179................................................................................................................................................................

Preparing The Persulfate Oxidizing Solution180................................................................................................................................................................

To Prepare The Oxidizing Solution180................................................................................................................................................................

Preparing The Acid180................................................................................................................................................................

Adding The Dilution Water180................................................................................................................................................................

Performing A Flush180................................................................................................................................................................

Cleaning The Analyzer181................................................................................................................................................................

Cleaning The Gas-liquid Separator181................................................................................................................................................................

Figure 73 The Gas-liquid Separator182................................................................................................................................................................

Cleaning The Sparger183................................................................................................................................................................

The Sparger183................................................................................................................................................................

Lubricating The Syringe184................................................................................................................................................................

Unscrewing The Syringe Base185................................................................................................................................................................

Figure 75 Locating The Syringe Screw And Washers185................................................................................................................................................................

Figure 77 Removing The Syringe186................................................................................................................................................................

Figure 79 Removing The Stopper187................................................................................................................................................................

Consumables Replacement188................................................................................................................................................................

Replacing The Pinch Valve Tubing188................................................................................................................................................................

Figure 81 Valve Locations - Innovox On-line Toc Analyzer190................................................................................................................................................................

Replacing The Peristaltic Pump Head Tubing191................................................................................................................................................................

Replacing The Ndir Filter192................................................................................................................................................................

Entering Consumables Installation Information193................................................................................................................................................................

Other Maintenance Tasks193................................................................................................................................................................

Replacing The High Pressure Valve Seals194................................................................................................................................................................

Figure 83: The High Pressure Valve Seal - Before Removal195................................................................................................................................................................

The High Pressure Valve Seal - After Removal195................................................................................................................................................................

Table 15 2-year Maintenance Worksheet - Sievers Innovox Online Toc Analyzer196................................................................................................................................................................

Chapter 9: Troubleshooting199................................................................................................................................................................

Reviewing Warnings And Errors199................................................................................................................................................................

Analyzer Warnings And Error Messages200................................................................................................................................................................

Other Software Errors210................................................................................................................................................................

Visual Inspection210................................................................................................................................................................

Figure 85 The Fluidics Side Of The Analyzer211................................................................................................................................................................

Figure 86 The Electronics Side Of The Analyzer212................................................................................................................................................................

Figure 87 Electronics In The Top Of The Analyzer213................................................................................................................................................................

Figure 88: Analyzer Schematic214................................................................................................................................................................

External Inspection215................................................................................................................................................................

Internal Inspection215................................................................................................................................................................

Reviewing Solutions For Basic Problems216................................................................................................................................................................

The Analyzer Will Not Power On216................................................................................................................................................................

Diagnostics217................................................................................................................................................................

The Diagnostics Screen217................................................................................................................................................................

Valves218................................................................................................................................................................

Flow Control Valves218................................................................................................................................................................

The Flow Control Valve Screen218................................................................................................................................................................

Figure 93 Sampler Handler Valves Screen219................................................................................................................................................................

Gas Valves220................................................................................................................................................................

Diagnostic Result Screen220................................................................................................................................................................

Gas Valve Testing Criteria221................................................................................................................................................................

Pneumatic Valves222................................................................................................................................................................

Pneumatic Valve Screen222................................................................................................................................................................

Ndir223................................................................................................................................................................

Heater223................................................................................................................................................................

Heater Testing Criteria224................................................................................................................................................................

Liquid Flow Check225................................................................................................................................................................

Gas Leak Checks226................................................................................................................................................................

Figure 100 The Gas Leak Check Screen227................................................................................................................................................................

Figure 101 Gas Manifold Leak Check229................................................................................................................................................................

Figure 102: Reactor Inlet Valve Leak Check231................................................................................................................................................................

Figure 103: Reactor Bypass Leak Check233................................................................................................................................................................

Figure 104 Reactor Leak Check235................................................................................................................................................................

Figure 105 Reactor Outlet Valve Check237................................................................................................................................................................

Leak Check238................................................................................................................................................................

Analog Output239................................................................................................................................................................

Binary Output239................................................................................................................................................................

Binary Input240................................................................................................................................................................

Figure 108 Binary Input Check241................................................................................................................................................................

Pumps242................................................................................................................................................................

Export Diagnostic Data243................................................................................................................................................................

Testing The Sparger243................................................................................................................................................................

Contacting Technical Support243................................................................................................................................................................

Returning The Analyzer To Ge Analytical Instruments244................................................................................................................................................................

Appendix A: Analyzer Dimension Diagrams247................................................................................................................................................................

Analyzer Dimensions (front View)247................................................................................................................................................................

Analyzer Dimensions (right Side View)248................................................................................................................................................................

Analyzer Dimensions (left Side View)249................................................................................................................................................................

Appendix B: Acronyms And Definitions251................................................................................................................................................................

Appendix C: Importing Analyzer Data Into A Spreadsheet255................................................................................................................................................................

Importing Data Into A Spreadsheet Program255................................................................................................................................................................

Figure 114 Microsoft Excel Spreadsheet Screen — Text Import Wizard - Step 1256................................................................................................................................................................

Figure 116 Microsoft Excel Spreadsheet Program — Text Import Wizard - Step 3257................................................................................................................................................................

Appendix D: Modbus Map259................................................................................................................................................................

Index265................................................................................................................................................................

GE Sievers Innovox Operation And Maintenance Manual (238 pages)

On-Line TOC Analyzer

Brand: GE | Category: Measuring Instruments | Size: 12.08 MB

Identification Records3................................................................................................................................................................

Table Of Contents4................................................................................................................................................................

List Of Tables10................................................................................................................................................................

List Of Figures11................................................................................................................................................................

Revision History14................................................................................................................................................................

Confidentiality15................................................................................................................................................................

Declaration Of Conformity16................................................................................................................................................................

Standard Limited Warranty16................................................................................................................................................................

Limitation Of Remedies And Liability17................................................................................................................................................................

Limitación De Remedios Y Responsabilidad17................................................................................................................................................................

Limites De Correction Et De Fiabilité17................................................................................................................................................................

Beschränkte Ansprüche Und Haftung17................................................................................................................................................................

Limitazione Di Rimedi E Responsabilità18................................................................................................................................................................

限定責任および救済18................................................................................................................................................................

赔偿与责任限制18................................................................................................................................................................

Warnings19................................................................................................................................................................

Chapter 1: Introduction47................................................................................................................................................................

Chapter 2: System Description49................................................................................................................................................................

System Specifications49................................................................................................................................................................

System Overview52................................................................................................................................................................

Figure 1: Analyzer Schematic53................................................................................................................................................................

Sample Flow Path54................................................................................................................................................................

Additional System Components56................................................................................................................................................................

System/controller And Electronics56................................................................................................................................................................

Data Outputs57................................................................................................................................................................

Major Accessories And Configurations57................................................................................................................................................................

2-stream Configuration57................................................................................................................................................................

5-stream Configuration58................................................................................................................................................................

Mounting Stand58................................................................................................................................................................

Air Purifier58................................................................................................................................................................

Fail Safe Accessory58................................................................................................................................................................

Ip5658................................................................................................................................................................

Nema 4x Cabinet58................................................................................................................................................................

Sample Filter Panel59................................................................................................................................................................

Sample Peristaltic Pump59................................................................................................................................................................

Chapter 3: Interferences61................................................................................................................................................................

Safety61................................................................................................................................................................

Reliability62................................................................................................................................................................

Analytical Performance62................................................................................................................................................................

Chapter 4: Installation65................................................................................................................................................................

Overview65................................................................................................................................................................

Step 1: Unpack And Inspect The Analyzer65................................................................................................................................................................

Additional Installation Equipment66................................................................................................................................................................

Step 2: Complete The Identification Records67................................................................................................................................................................

Step 3: Select A Location For The Analyzer67................................................................................................................................................................

Mounting Stand Installation67................................................................................................................................................................

Figure 2 Mounting Stand - Clearances68................................................................................................................................................................

Figure 3 Attaching Mounting Brackets On The Analyzer69................................................................................................................................................................

Figure 4 Mounting The Analyzer To The Stand70................................................................................................................................................................

Wall Mount Installation71................................................................................................................................................................

Step 4: Connect The Waste Lines71................................................................................................................................................................

Step 5: Fill The Gas-liquid Separator73................................................................................................................................................................

The Gas-liquid Separator73................................................................................................................................................................

Step 6: Install Input/output, Cables, And Accessories74................................................................................................................................................................

Table 1 Analog Outputs (tb1)75................................................................................................................................................................

Alarm Outputs (tb3)76................................................................................................................................................................

Table76................................................................................................................................................................

Alarm Outputs (tb4)77................................................................................................................................................................

Installing The 4-20 Ma Connection78................................................................................................................................................................

Installing The Remote Start (binary Input) Connection78................................................................................................................................................................

Installing The Analysis Complete Output Connection79................................................................................................................................................................

Figure 8 Wiring Option - Binary Input Using Analyzer's Internal Supply79................................................................................................................................................................

Figure 9 Wiring Option - Binary Input Using Analyzer's External Supply79................................................................................................................................................................

Installing The Alarms And System Fault Output Connection80................................................................................................................................................................

Installing The Ethernet Connection80................................................................................................................................................................

Connecting The Analyzer To A Computer80................................................................................................................................................................

Installing The Usb Connection81................................................................................................................................................................

Connecting The Analyzer To A Network81................................................................................................................................................................

Step 7: Connecting To A Power Supply82................................................................................................................................................................

Step 8: Connect The Sample Inlet System83................................................................................................................................................................

Installing The Online Sample System83................................................................................................................................................................

Installing The Check Standard System84................................................................................................................................................................

Installing The Grab Sample System84................................................................................................................................................................

Step 9: Connect The Reagent And Dilution Water Lines84................................................................................................................................................................

Step 10: Connect The Compressed Gas85................................................................................................................................................................

Installing The Carrier Gas Supply85................................................................................................................................................................

Installing The Gas Supply For The Ip56 Accessory86................................................................................................................................................................

Step 11: Turn On Power And Configure Basic Settings86................................................................................................................................................................

Setting The Clock87................................................................................................................................................................

Step 12: Perform A Test Analysis87................................................................................................................................................................

Step 13: Calibrate The Analyzer88................................................................................................................................................................

Chapter 5: Calibration And Verification89................................................................................................................................................................

Handling Standards90................................................................................................................................................................

Prepare Ic Standard Solution90................................................................................................................................................................

Calibration And Verification Options91................................................................................................................................................................

Single-point Calibration91................................................................................................................................................................

Two-point Calibration92................................................................................................................................................................

Two-point Calibration (point 1 Is Standard)93................................................................................................................................................................

Two-point Calibration (point 1 Is Reagent Water)94................................................................................................................................................................

Calibration With More Than Two Points95................................................................................................................................................................

Linear Fit Multi-point Calibration95................................................................................................................................................................

Point-to-point Multi-point Calibration96................................................................................................................................................................

Auto Dilution97................................................................................................................................................................

Blank Correction98................................................................................................................................................................

Calibration Groups98................................................................................................................................................................

Table 5 Maximum Dilution Allowed Using Auto Dilution Feature98................................................................................................................................................................

Preparing For Calibration99................................................................................................................................................................

Save System Settings99................................................................................................................................................................

Perform Maintenance Tasks100................................................................................................................................................................

Setting Up Npoc, Ic, Tc/toc Calibration100................................................................................................................................................................

Calibrating The Analyzer102................................................................................................................................................................

Table 6 Approximate Number Of Calibration Repetitions Possible102................................................................................................................................................................

Editing A Calibration104................................................................................................................................................................

Performing A Calibration Verification105................................................................................................................................................................

Reviewing Calibration And Verification History106................................................................................................................................................................

Table 7 Approximate Number Of Verification Repetitions Possible106................................................................................................................................................................

Chapter 6: Analyzer Operation107................................................................................................................................................................

The Main Screen108................................................................................................................................................................

The Menu Screen109................................................................................................................................................................

Setting Up Measurements (the Setup Tab)110................................................................................................................................................................

Online Measurements111................................................................................................................................................................

Continuous Measurements111................................................................................................................................................................

Operation With Multiple Streams112................................................................................................................................................................

Cycle Frequency113................................................................................................................................................................

Figure 25 Operation With Five Streams And The Check Standard113................................................................................................................................................................

Figure 26 Calculating The Run Time114................................................................................................................................................................

Configuring Online Measurements115................................................................................................................................................................

Configure Online Screen115................................................................................................................................................................

Stream 1 Screen116................................................................................................................................................................

Check Standards118................................................................................................................................................................

Figure 29: Check Standard Setup Screen119................................................................................................................................................................

Check Standard (setup) Screen121................................................................................................................................................................

Clean Inlet122................................................................................................................................................................

Auto Restart122................................................................................................................................................................

Daily Flush122................................................................................................................................................................

Summary123................................................................................................................................................................

Grab Measurements123................................................................................................................................................................

Table 8 Vial Port - Repetitions Possible126................................................................................................................................................................

Rinse127................................................................................................................................................................

Measurement Settings127................................................................................................................................................................

Measure127................................................................................................................................................................

Range128................................................................................................................................................................

Auto Range128................................................................................................................................................................

Acid128................................................................................................................................................................

Table 9 Ranges In The Innovox Online Toc Analyzer128................................................................................................................................................................

Oxidizer129................................................................................................................................................................

Repetitions129................................................................................................................................................................

Rejects129................................................................................................................................................................

Repeat Criteria129................................................................................................................................................................

Sparge129................................................................................................................................................................

Flush130................................................................................................................................................................

Manual Dilution130................................................................................................................................................................

Conversion Factors130................................................................................................................................................................

User Management131................................................................................................................................................................

Measuring The Blank132................................................................................................................................................................

Viewing And Exporting Data133................................................................................................................................................................

Viewing Data On Screen133................................................................................................................................................................

The Data Screen133................................................................................................................................................................

Exporting Data134................................................................................................................................................................

Export (data) Screen134................................................................................................................................................................

Figure 36: Export Data Screen135................................................................................................................................................................

Reviewing Exported Data136................................................................................................................................................................

Data Fields Output136................................................................................................................................................................

Setting Up Input And Output (i/o)137................................................................................................................................................................

Connecting The Analyzer To A Network Via Ethernet137................................................................................................................................................................

Configuring The Analyzer's Ip Address137................................................................................................................................................................

Configuring A Personal Computer138................................................................................................................................................................

Collecting Real-time Data140................................................................................................................................................................

Using The Ethernet Connection And Modbus140................................................................................................................................................................

Configuring Alarm Outputs140................................................................................................................................................................

Resetting Alarms141................................................................................................................................................................

Printing Data141................................................................................................................................................................

Figure 39 Print Data Screen142................................................................................................................................................................

Configuring Advanced Setup143................................................................................................................................................................

Setting Analyzer Name And Location143................................................................................................................................................................

Setting System Properties144................................................................................................................................................................

System Properties Screen144................................................................................................................................................................

Upgrade Option145................................................................................................................................................................

Cleaning The Analyzer Screen145................................................................................................................................................................

Setting The Fail Safe Option145................................................................................................................................................................

Setting The Keyboard Options146................................................................................................................................................................

Setting The Display Options146................................................................................................................................................................

Archiving The Data History146................................................................................................................................................................

Shutting Down The Analyzer147................................................................................................................................................................

Chapter 7: Operation With The Filter Panel149................................................................................................................................................................

Operation Of Filter Panel With Sample Pump149................................................................................................................................................................

Control Of Filter Panel149................................................................................................................................................................

Figure 42: Blowback Pulses And Delay150................................................................................................................................................................

Flush/blowback Screen151................................................................................................................................................................

Chapter 8: Maintenance153................................................................................................................................................................

Consumables Replacement Schedule153................................................................................................................................................................

Recommended Spare Parts154................................................................................................................................................................

Periodic Maintenance Tasks154................................................................................................................................................................

Periodic Inspections154................................................................................................................................................................

Preparing The Oxidizer Solution154................................................................................................................................................................

Figure 45 Aging Of 30% (w/v) Na155................................................................................................................................................................

Preparing The Acid156................................................................................................................................................................

Adding The Dilution Water156................................................................................................................................................................

Performing A Flush156................................................................................................................................................................

Cleaning The Analyzer157................................................................................................................................................................

Cleaning The Gas-liquid Separator157................................................................................................................................................................

Cleaning The Sparger158................................................................................................................................................................

The Sparger158................................................................................................................................................................

Figure 47 The Sparger159................................................................................................................................................................

Lubricating The Syringe160................................................................................................................................................................

Figure 49 Unscrewing The Syringe Base161................................................................................................................................................................

Figure 51 Pulling Out The Plunger162................................................................................................................................................................

Consumables Replacement163................................................................................................................................................................

Replacing The Pinch Valve Tubing163................................................................................................................................................................

Figure 54 Valve Locations - Innovox On-line Toc Analyzer165................................................................................................................................................................

Replacing The Peristaltic Pumps166................................................................................................................................................................

Replacing The Ndir Filter166................................................................................................................................................................

Figure 55: Replacing The Ndir Filter167................................................................................................................................................................

Entering Consumables Installation Information168................................................................................................................................................................

Other Maintenance Tasks168................................................................................................................................................................

Replacing The High Pressure Valve Seals168................................................................................................................................................................

Figure 56: The High Pressure Valve Seal - Before Removal169................................................................................................................................................................

The High Pressure Valve Seal - After Removal169................................................................................................................................................................

Table 12 2-year Maintenance Worksheet - Sievers Innovox Online Toc Analyzer170................................................................................................................................................................

Chapter 9: Troubleshooting173................................................................................................................................................................

Reviewing Warnings And Errors173................................................................................................................................................................

Analyzer Warnings And Error Messages174................................................................................................................................................................

Other Software Errors182................................................................................................................................................................

Visual Inspection182................................................................................................................................................................

Figure 58 The Fluidics Side Of The Analyzer183................................................................................................................................................................

Figure 59 The Electronics Side Of The Analyzer184................................................................................................................................................................

Figure 60 Electronics In The Top Of The Analyzer185................................................................................................................................................................

Figure 61: Analyzer Schematic186................................................................................................................................................................

External Inspection187................................................................................................................................................................

Internal Inspection187................................................................................................................................................................

Figure 62 Connections To The Gas-liquid Separator188................................................................................................................................................................

Reviewing Solutions For Basic Problems189................................................................................................................................................................

The Analyzer Will Not Power On189................................................................................................................................................................

Diagnostics189................................................................................................................................................................

The Diagnostics Screen189................................................................................................................................................................

Pinch Valves190................................................................................................................................................................

Gas Valves191................................................................................................................................................................

Ndir192................................................................................................................................................................

The Temperatures Display On The Ndir Screen192................................................................................................................................................................

Heater193................................................................................................................................................................

Liquid Flow194................................................................................................................................................................

Gas Leak Checks195................................................................................................................................................................

Gas Manifold Leak Check195................................................................................................................................................................

Figure 70: Gas Manifold Leak Check197................................................................................................................................................................

Reactor Inlet Valve Leak Check198................................................................................................................................................................

Figure 71: Reactor Inlet Valve Leak Check199................................................................................................................................................................

Reactor Bypass Leak Check200................................................................................................................................................................

Figure 72: Reactor Bypass Leak Check201................................................................................................................................................................

Reactor Leak Check202................................................................................................................................................................

Figure 73: Reactor Leak Check203................................................................................................................................................................

Reactor Outlet Valve Leak Check204................................................................................................................................................................

Figure 74 Reactor Valve Outlet Check205................................................................................................................................................................

Gas Liquid Separator, Ndir Filter, Ndir Sample Path And Sparger Leak Check206................................................................................................................................................................

Pneumatic Valves206................................................................................................................................................................

Pneumatic Valve Check206................................................................................................................................................................

Analog Output207................................................................................................................................................................

Binary Output207................................................................................................................................................................

Binary Input208................................................................................................................................................................

Sample Pumps209................................................................................................................................................................

Export Diagnostic Data210................................................................................................................................................................

Contacting Technical Support210................................................................................................................................................................

Returning The Analyzer To Ge Analytical Instruments210................................................................................................................................................................

Appendix A: Analyzer Dimension Diagrams213................................................................................................................................................................

Analyzer Dimensions (front View)213................................................................................................................................................................

Analyzer Dimensions (right Side View)214................................................................................................................................................................

Analyzer Dimensions (left Side View)215................................................................................................................................................................

Appendix B: Acronyms And Definitions217................................................................................................................................................................

Appendix C: Transferring Data To A Pc221................................................................................................................................................................

Using Hyperterminal221................................................................................................................................................................

Figure 84 Entering Connection Information222................................................................................................................................................................

Figure 85 Saving Data On Hyperterminal223................................................................................................................................................................

Importing Data Into A Spreadsheet Program224................................................................................................................................................................

Figure 87 Microsoft Excel Spreadsheet Screen — Text Import Wizard - Step 1225................................................................................................................................................................

Figure 89 Microsoft Excel Spreadsheet Program — Text Import Wizard - Step 3226................................................................................................................................................................

Appendix D: Modbus Map227................................................................................................................................................................

Index233................................................................................................................................................................