GE Sievers Innovox Manuals

Table of Contents

• • 3

    Identification Records
  • 4

    Table of Contents
  • 10

    List of Tables
  • 11

    List of Figures
  • 15

    Revision History
  • 16

    Confidentiality
  • 17

    Declaration of Conformity
  • 17

    Standard Limited Warranty
    • 18

      Limitation of Remedies and Liability
    • 18

      Limitación De Remedios Y Responsabilidad
    • 18

      Limites De Correction Et De Fiabilité
    • 18

      Beschränkte Ansprüche Und Haftung
    • 19

      Limitazione DI Rimedi E Responsabilità
    • 19

      限定責任および救済
  • 19

    赔偿与责任限制
  • 20

    Warnings

• 49

  Chapter 1: Introduction

• 51

  Chapter 2: System Description

  • 51

    System Specifications
    • 53

      Additional System Specifications
  • 53

    Operating Specifications
  • 54

    Reagent Consumption
  • 54

    SCWO Method Compliance
  • 54

    System Overview
  • 56

    Figure 1: Analyzer Schematic
  • 57

    Sample Flow Path
  • 59

    Table 1 InnovOx Wetted Materials List
  • 60

    Additional System Components
    • 60

      System/Controller and Electronics
    • 61

      Data Outputs
    • 61

      Sample Preparation Device Options
    • 61

      Clean Water Sample Options
    • 61

      Sample Preparation Options
      • 62

        2-Stream Configuration
      • 62

        Specifications - (2-Stream or 5-Stream) Clean Water Sampler
      • 62

        2-Stream High Temperature Configuration
      • 63

        Specifications - (2-Stream) High Temperature Clean Water Sampler
  • 63

    Wastewater Sampler Option
    • 63

      2-Stream Configuration
    • 64

      Specifications - Wastewater Sampler
    • 64

      Mounting Stand
    • 64

      Regenerative Air Purifier Option
    • 65

      Carrier Gas CO 2 Scrubber Option (On-line)
    • 65

      Fail Safe Accessory
    • 65

      Ip56
    • 65

      NEMA 4X Cabinet
    • 65

      Hazardous Location Enclosures
    • 66

      Sample Filter Panel
    • 66

      Sample Peristaltic Pump

• 67

  Chapter 3: Interferences

  • 67

    Safety
  • 68

    Reliability
  • 68

    Analytical Performance

• 71

  Chapter 4: Installation

  • 71

    Overview
  • 71

    Step 1: Unpack and Inspect the Analyzer
    • 73

      Additional Installation Equipment
  • 73

    Step 2: Complete the Identification Records
  • 73

    Step 3: Select a Location for the Analyzer
    • 73

      Mounting Stand Installation
      • 74

        Figure 2 Mounting Stand - Clearances
      • 75

        Figure 3 Attaching Mounting Brackets On the Analyzer
      • 76

        Figure 4 Mounting the Analyzer to the Stand
    • 77

      Wall Mount Installation
  • 77

    Step 4: Connect the Waste Lines
  • 79

    Step 5: Fill the Gas-Liquid Separator
  • 79

    Step 6: Install Input/Output, Cables, and Accessories
    • 79

      The Gas-Liquid Separator
    • 81

      Analog Outputs (TB1)
    • 81

      Stream ID
    • 82

      Alarm Outputs (TB3)
    • 82

      Table 5 Binary Input (TB2)
    • 83

      Alarm Outputs (TB4)
    • 84

      Installing the 4-20 MA Connection
    • 84

      Installing the Remote Start (Binary Input) Connection
    • 85

      Installing the Analysis Complete Output Connection
    • 85

      Figure 8 Wiring Option - Binary Input Using Analyzer's Internal Supply
    • 85

      Figure 9 Wiring Option - Binary Input Using Analyzer's External Supply
    • 86

      Installing the Alarms and System Fault Output Connection
    • 86

      Installing the Ethernet Connection
  • 86

    Connecting the Analyzer to a Computer
    • 87

      Installing the USB Connection
    • 87

      Connecting the Analyzer to a Network
  • 88

    Step 7: Connecting to a Power Supply
  • 89

    Step 8: Connect the Sample Inlet System
    • 89

      Installing the Online Sample System
    • 90

      Installing the Wastewater Sampler
      • 91

        To Install the Wastewater Sampler (Velocity Method)
      • 91

        Figure 16 Top Wastewater Sampler Bracket W/Plate Adapter
      • 92

        Figure 17: Lower Wastewater Sampler Bracket
  • 92

    Velocity Method - Barb Fittings Identification
    • 93

      Figure 19: Velocity Method - Installation
    • 93

      Figure 20 Velocity Method - Adjusting the Sipper Tube Height
    • 94

      To Install the Wastewater Sampler (Overflow Method)
    • 94

      Velocity Method - Failsafe Installation
    • 95

      Figure 23 Top Wastewater Sampler Bracket W/Plate Adapter
  • 95

    Lower Wastewater Sampler Bracket
    • 96

      Figure 25 Overflow Method - External Sample Pump Position
    • 96

      Figure 26 Overflow Method - Barb Fittings Identification
    • 97

      Figure 27: Overflow Method - Installation
    • 97

      Figure 28 Overflow Method - Adjusting the Sipper Tube Height
    • 98

      Installing the Check Standard System
  • 98

    Overflow Method - Failsafe Installation
  • 99

    Installing the Grab Sample System
  • 99

    Step 9: Connect the Reagent and Dilution Water Lines
  • 100

    Step 10: Connect the Compressed Gas
    • 100

      Installing the Carrier Gas Supply
    • 101

      Installing the Gas Supply for the IP56 Accessory
      • 102

        Specifications - IP56 Accessory
  • 102

    Step 11: Turn On Power and Configure Basic Settings
    • 102

      Setting the Clock
  • 102

    Step 12: Perform a Test Analysis
  • 104

    Step 13: Calibrate the Analyzer

• 105

  Chapter 5: Calibration and Verification

  • 105

    Overview
  • 106

    Handling Standards
    • 106

      Prepare IC Standard Solution
  • 107

    Calibration and Verification Options
    • 107

      Single-Point Calibration
    • 108

      Figure 31 Calibration Curve for Single-Point Calibration
    • 109

      Two-Point Calibration
    • 110

      Figure 33 Two-Point Calibration (Point 1 Is Reagent Water)
    • 111

      Calibration With More Than Two Points
      • 111

        Linear Fit Multi-Point Calibration
      • 112

        Point-to-Point Multi-Point Calibration
    • 113

      Auto Dilution
    • 114

      Blank Correction
    • 114

      Calibration Groups
    • 114

      Table 8 Maximum Dilution Allowed Using Auto Dilution Feature
  • 115

    Preparing for Calibration
    • 115

      Save System Settings
    • 116

      Perform Maintenance Tasks
  • 116

    Setting Up NPOC, IC, TC/TOC Calibration
  • 118

    Calibrating the Analyzer
    • 118

      Table 9 Approximate Number of Calibration Repetitions Possible
    • 119

      Editing a Calibration
    • 120

      Editing a Calibration
  • 121

    Performing a Calibration Verification
  • 122

    Reviewing Calibration and Verification History
  • 122

    Table 10 Approximate Number of Verification Repetitions Possible

• 123

  Chapter 6: Analyzer Operation

  • 123

    Overview
    • 123

      The Main Screen
    • 124

      Figure 38 the Main Screen (Grab Mode)
    • 125

      The Menu Screen
  • 126

    Setting Up Measurements (The Setup Tab)
    • 126

      Online Measurements
      • 127

        Continuous Measurements
      • 128

        Operation With Multiple Streams
      • 128

        Cycle Frequency
      • 128

        Figure 43 Operation With Five Streams and the Check Standard
  • 129

    Configure Online Screen
    • 130

      Figure 44 Calculating the Run Time
    • 131

      Online Measurement-Configuration
      • 131

        Operation With Multiple Streams
      • 132

        Figure 46: Stream 1 Screen
      • 134

        Check Standards
      • 135

        Figure 47: Check Standard Setup Screen
  • 137

    Check Standard (Setup) Screen
    • 138

      Clean Inlet
    • 138

      Auto Restart
    • 138

      Daily Flush
    • 139

      Summary
    • 139

      Grab Measurements
      • 140

        Figure 51 the Grab (Setup) Screen
      • 142

        Table 11 Vial Port - Repetitions Possible
    • 143

      Rinse
    • 143

      Measurement Settings
      • 143

        Measure
      • 144

        Range
      • 144

        Auto Range
      • 145

        Acid
      • 145

        Oxidizer
      • 145

        Repetitions
      • 145

        Rejects
      • 145

        Repeat Criteria
      • 146

        Sparge
      • 146

        Flush
      • 146

        Manual Dilution
      • 146

        Configuring Conversion Factors
      • 147

        Figure 52: the Maintenance Tab
      • 148

        Figure 54: Configuring the Factor Equation
  • 148

    Configuring the Factor Units
    • 149

      Figure 56: Configuring the Factor Name
    • 150

      User Management
      • 150

        Blank Correction
      • 151

        Measuring the Blank
  • 152

    Viewing and Exporting Data
    • 152

      Viewing Data On Screen
    • 152

      Exporting Data
  • 152

    The Data Screen
  • 153

    Export (Data) Screen
    • 154

      Figure 60: Export Data Screen
    • 155

      Reviewing Exported Data
  • 155

    Data Fields Output
  • 156

    Setting Up Input and Output (I/O)
    • 156

      The I/O Tab
    • 156

      Connecting the Analyzer to a Network Via Ethernet
      • 156

        Configuring the Analyzer's IP Address
      • 157

        Configuring a Personal Computer
    • 159

      Collecting Historical and Real-Time Data
      • 159

        To Collect Real-time Data (W/ethernet Connection)
      • 160

        Using the Ethernet Connection and Modbus
      • 160

        Configuring Alarm Outputs
      • 161

        Figure 62 Alarm Output Screen
      • 162

        Changing the Alarms On or Off Setting
      • 162

        Resetting Alarms
    • 162

      Printer Setup
    • 163

      Liquid Sensor Setup
      • 163

        To Enable a Liquid Sensor
      • 164

        Figure 65 Liquid Sensor Location - Hazardous Location Enclosure (ATEX or C1/D2)
    • 165

      Configuring Advanced Setup
      • 165

        The Maintenance Tab
      • 165

        Setting Analyzer Name and Location
      • 166

        Setting System Properties
    • 166

      System Properties Screen
    • 167

      Setting the Clock
    • 167

      Upgrade Option
    • 167

      Gas Valve PID Parameters
    • 168

      Cleaning the Analyzer Screen
    • 169

      Setting the Fail Safe Option
    • 169

      Setting the Keyboard Options
    • 169

      Setting the Display Options
    • 170

      Archiving the Data History
  • 170

    Shutting Down the Analyzer
  • 171

    Checking the Software Version

• 173

  Chapter 7: Operation With the Filter Panel

  • 173

    Operation of the Filter Panel With a Sample Pump
  • 173

    Control of Filter Panel
    • 174

      Figure 69: Blowback Pulses and Sample Flow Time
    • 175

      Flush/Blowback Screen

• 177

  Chapter 8: Maintenance

  • 178

    Recommended Spare Parts
  • 178

    Periodic Maintenance Tasks
    • 178

      Periodic Inspections
  • 178

    Consumables Replacement Schedule
    • 179

      Preparing the Oxidizer Solution
    • 179

      Figure 72 Aging of 30% (W/V) Na 2 S 2 O 8 in HDPE Bottles
    • 180

      Preparing the Persulfate Oxidizing Solution
      • 180

        To Prepare the Oxidizing Solution
    • 180

      Preparing the Acid
    • 180

      Adding the Dilution Water
    • 180

      Performing a Flush
    • 181

      Cleaning the Analyzer
    • 181

      Cleaning the Gas-Liquid Separator
    • 182

      Figure 73 the Gas-Liquid Separator
    • 183

      Cleaning the Sparger
  • 183

    The Sparger
    • 184

      Lubricating the Syringe
  • 185

    Unscrewing the Syringe Base
    • 185

      Figure 75 Locating the Syringe Screw and Washers
    • 186

      Figure 77 Removing the Syringe
    • 187

      Figure 79 Removing the Stopper
  • 188

    Consumables Replacement
    • 188

      Replacing the Pinch Valve Tubing
    • 190

      Figure 81 Valve Locations - InnovOx On-Line TOC Analyzer
    • 191

      Replacing the Peristaltic Pump Head Tubing
    • 192

      Replacing the NDIR Filter
    • 193

      Entering Consumables Installation Information
  • 193

    Other Maintenance Tasks
  • 193

    Replacing the NDIR Filter
    • 194

      Replacing the High Pressure Valve Seals
    • 195

      Figure 83: the High Pressure Valve Seal - before Removal
  • 195

    The High Pressure Valve Seal - After Removal
  • 196

    Table 15 2-Year Maintenance Worksheet - Sievers InnovOx Online TOC Analyzer

• 199

  Chapter 9: Troubleshooting

  • 199

    Overview
  • 199

    Reviewing Warnings and Errors
    • 200

      Analyzer Warnings and Error Messages
    • 210

      Other Software Errors
  • 210

    Visual Inspection
    • 211

      Figure 85 the Fluidics Side of the Analyzer
    • 212

      Figure 86 the Electronics Side of the Analyzer
    • 213

      Figure 87 Electronics in the Top of the Analyzer
    • 214

      Figure 88: Analyzer Schematic
    • 215

      External Inspection
    • 215

      Internal Inspection
  • 216

    Reviewing Solutions for Basic Problems
    • 216

      The Analyzer Will Not Power On
  • 217

    Diagnostics
  • 217

    The Diagnostics Screen
    • 218

      Valves
      • 218

        Flow Control Valves
  • 218

    The Flow Control Valve Screen
    • 219

      Figure 93 Sampler Handler Valves Screen
    • 220

      Gas Valves
  • 220

    Diagnostic Result Screen
    • 221

      Gas Valve Testing Criteria
    • 222

      Pneumatic Valves
    • 222

      Pneumatic Valve Screen
    • 223

      Ndir
    • 223

      Heater
      • 224

        Heater Testing Criteria
    • 225

      Liquid Flow Check
    • 226

      Gas Leak Checks
      • 227

        Figure 100 the Gas Leak Check Screen
      • 229

        Figure 101 Gas Manifold Leak Check
      • 231

        Figure 102: Reactor Inlet Valve Leak Check
      • 233

        Figure 103: Reactor Bypass Leak Check
      • 235

        Figure 104 Reactor Leak Check
      • 237

        Figure 105 Reactor Outlet Valve Check
      • 238

        Leak Check
    • 239

      Analog Output
    • 239

      Binary Output
    • 240

      Binary Input
    • 241

      Figure 108 Binary Input Check
    • 242

      Pumps
    • 243

      Export Diagnostic Data
    • 243

      Testing the Sparger
  • 243

    Contacting Technical Support
  • 244

    Returning the Analyzer to GE Analytical Instruments

• 247

  Appendix A: Analyzer Dimension Diagrams

  • 247

    Analyzer Dimensions (Front View)
  • 248

    Analyzer Dimensions (Right Side View)
  • 249

    Analyzer Dimensions (Left Side View)

• 251

  Appendix B: Acronyms and Definitions

• 255

  Appendix C: Importing Analyzer Data Into a Spreadsheet

  • 255

    Importing Data Into a Spreadsheet Program
    • 256

      Figure 114 Microsoft Excel Spreadsheet Screen — Text Import Wizard - Step 1
    • 257

      Figure 116 Microsoft Excel Spreadsheet Program — Text Import Wizard - Step 3

• 259

  Appendix D: Modbus Map

  • 265

    Index