Agilent Technologies Infinity II 1290 User Manual
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Agilent Technologies Infinity II 1290 User Manual

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Agilent 1290 Infinity II
Flexible Pump
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  • Page 1 Agilent 1290 Infinity II Flexible Pump User Manual Agilent Technologies...
  • Page 2 Notices Warranty © Agilent Technologies, Inc. 2014 receive no greater than Restricted Rights as defined in FAR 52.227-19(c)(1-2) (June No part of this manual may be reproduced The material contained in this docu- 1987). U.S. Government users will receive in any form or by any means (including elec- ment is provided “as is,”...
  • Page 3 In This Guide... In This Guide... This manual covers the Agilent 1290 Infinity II Flexible Pump (G7104A). 1 Introduction This chapter gives an introduction to the module, instrument overview and internal connectors. 2 Site Requirements and Specifications This chapter provides information on environmental requirements, physical and performance specifications.
  • Page 4 In This Guide... 8 Parts and Materials This chapter provides information on parts for maintenance and repair. 9 Identifying Cables This chapter provides information on cables used with the modules. 10 Hardware Information This chapter describes the pump in more detail on hardware and electronics.

  • Page 5: Table Of Contents

    Contents Contents 1 Introduction Product Description Features Operating Principle Positions of the Multi Purpose Valve Leak and Waste Handling 2 Site Requirements and Specifications Site Requirements Physical Specifications Performance Specifications 3 Using the Pump Magnets Turn on/off Status Indicators Best Practices 4 How to Optimize the Performance of Your Module Delay Volume and Extra-Column Volume How to Configure the Optimum Delay Volume...
  • Page 6 Contents 7 Maintenance Introduction to Maintenance Warnings and Cautions Overview of Maintenance Cleaning the Module Install Fittings and Capillaries Remove and Install Doors Replace the Pressure Sensor Replace the Inlet Weaver Replace the Inlet Valve Replace the Outlet Valve Remove the Jet Weaver Install the Jet Weaver Replace the Seal Wash Pump Replace the Multi-Channel Gradient Valve (MCGV)
  • Page 7 Automatic configuration with Bootp Manual Configuration PC and User Interface Software Setup Setup 12 Appendix General Safety Information Waste Electrical and Electronic Equipment Directive Radio Interference Sound Emission Agilent Technologies on Internet Agilent 1290 Infinity II Flexible Pump User Manual...
  • Page 8 Contents Agilent 1290 Infinity II Flexible Pump User Manual...

  • Page 9: Introduction

    Agilent 1290 Infinity II Flexible Pump User Manual Introduction Product Description Features Operating Principle Positions of the Multi Purpose Valve Leak and Waste Handling Waste Concept This chapter gives an introduction to the module, instrument overview and internal connectors. Agilent Technologies...

  • Page 10: Product Description

    Introduction Product Description Product Description The Agilent 1290 Infinity II Flexible Pump improves your efficiency by combining the performance of a high- pressure mixing UHPLC pump with the flexibility of a low- pressure mixing UHPLC pump. The new 1290 Infinity II LC power range has a high instrument efficiency, allowing you to run any HPLC and UHPLC method.

  • Page 11: Features

    Introduction Features Features • High performance in terms of accuracy and precision for flow and composition. • High power range combining high pressure up to 1300 bar and high analytical flow rates up to 5 mL/min for high chromatographic performance. •...

  • Page 12: Operating Principle

    Introduction Operating Principle Operating Principle The pump head comprises two pump chambers in series with independent high- resolution motion control. A pressure sensor in the flow path monitors the pressure. The pump control uses this signal for minimizing the pressure ripple in order to achieve highest flow precision. A stable flow can be delivered even in case of eventual small internal leaks, which can be compensated automatically.
  • Page 13 Introduction Operating Principle Figure 2 The hydraulic path Agilent 1290 Infinity II Flexible Pump User Manual...

  • Page 14: Positions Of The Multi Purpose Valve

    Introduction Positions of the Multi Purpose Valve Positions of the Multi Purpose Valve The Multi Purpose Valve allows easy software controlled switching between different modes of operation. Normal Operating Mode Without Mixer In normal operating mode, the flow comes from the pump head, passes the pressure sensor and arrives at the central port of the Multi Purpose Valve.
  • Page 15 Introduction Positions of the Multi Purpose Valve Purge Mode In purge mode, the flow is diverted to the waste container. From pump To waste Figure 4 Valve position in purge mode Agilent 1290 Infinity II Flexible Pump User Manual...
  • Page 16 Introduction Positions of the Multi Purpose Valve Normal Operating Mode With Mixer In this mode, the flow passes an optional Jet Weaver and the inline filter. This configuration is recommended for special applications which require an increased mixing efficiency. From pump Jet Weaver To system Inline filter...
  • Page 17 Introduction Positions of the Multi Purpose Valve Filter Flush Mode This mode is used for cleaning the inline filter by back- flushing it. The flow goes to port 5, passes the inline filter in opposite direction and leaves to the waste through port 7. From pump To waste Inline filter...
  • Page 18 Introduction Positions of the Multi Purpose Valve Service Mode In service mode, the flow is diverted to port 3, where for example a restriction capillary can be installed for diagnostic tests. From pump Restriction capillary Figure 7 Valve position in service mode Agilent 1290 Infinity II Flexible Pump User Manual...

  • Page 19: Leak And Waste Handling

    Introduction Leak and Waste Handling Leak and Waste Handling The 1290 Infinity II Series has been designed for safe leak and waste handling. It is important that all security concepts are understood and instructions are carefully followed. Figure 8 Leak and waste handling concept (overview - typical stack configuration as an example) Agilent 1290 Infinity II Flexible Pump User Manual...
  • Page 20 Introduction Leak and Waste Handling The solvent cabinet is designed to store a maximum volume of 6 L solvent. The maximum volume for an individual bottle stored in the solvent cabinet should not exceed 4 L. For details, see the usage guideline for the Agilent 1200 Infinity Series Solvent Cabinets (a printed copy of the guideline has been shipped with the solvent cabinet, electronic copies are available on the Internet).
  • Page 21 Introduction Leak and Waste Handling Waste Concept Agilent recommends using the 6 L waste can with 1 Stay Safe cap GL45 with 4 ports (5043- 1221) for optimal and safe waste disposal. If you decide to use your own waste solution, make sure that the tubes don't immerse in the liquid.
  • Page 22 Introduction Leak and Waste Handling Agilent 1290 Infinity II Flexible Pump User Manual...

  • Page 23: Site Requirements And Specifications

    Agilent 1290 Infinity II Flexible Pump User Manual Site Requirements and Specifications Site Requirements Physical Specifications Performance Specifications This chapter provides information on environmental requirements, physical and performance specifications. Agilent Technologies...

  • Page 24: Site Requirements

    Site Requirements and Specifications Site Requirements Site Requirements A suitable environment is important to ensure optimal performance of the instrument. Power Considerations The module power supply has wide ranging capability. It accepts any line voltage in the range described in Table 1 on page 27.
  • Page 25 Never operate your instrumentation from a power outlet that has no ground connection. ➔ Never use a power cord other than the Agilent Technologies power cord designed for your region. Use of unsupplied cables WA R N I N G Using cables not supplied by Agilent Technologies can lead to damage of the electronic components or personal injury.
  • Page 26 Site Requirements and Specifications Site Requirements Bench Space The module dimensions and weight (see Table 1 on page 27) allow you to place the module on almost any desk or laboratory bench. It needs an additional 2.5 cm (1.0 inches) of space on either side and approximately 8 cm (3.1 inches) in the rear for air circulation and electric connections.

  • Page 27: Physical Specifications

    Site Requirements and Specifications Physical Specifications Physical Specifications Table 1 Physical Specifications Type Specification Comments Weight 16.1 kg (35.5 lbs) Dimensions 180 x 396 x 436 mm (height × width × depth) (7.1 x 15.6 x 17.2 inches) Line voltage 100 –...

  • Page 28: Performance Specifications

    Site Requirements and Specifications Performance Specifications Performance Specifications Table 2 Agilent 1290 Infinity II Flexible Pump (G7104A) Performance Specifications Feature Specification Hydraulic system Dual pistons in series pump with proprietary servo-controlled variable stroke design and smooth motion control for active damping. Pump resolution step 300 pL step size size...
  • Page 29 Site Requirements and Specifications Performance Specifications Table 2 Agilent 1290 Infinity II Flexible Pump (G7104A) Performance Specifications Feature Specification Solvent selection Internal 4-solvent gradient formation valve included. valve External 2x 12 solvent valve as option, fully integrated in the pump control interface.
  • Page 30 Site Requirements and Specifications Performance Specifications Agilent 1290 Infinity II Flexible Pump User Manual...

  • Page 31: Using The Pump

    Daily / Weekly tasks Power up / Shut-down the pump Prepare the pump How to deal with solvents Select channels for Multi-Channel Gradient Valve (MCGV) This chapter explains the operational parameters of the Agilent 1290 Infinity II Flexible Pump. Agilent Technologies...

  • Page 32: Magnets

    Using the Pump Magnets Magnets Agilent 1290 Infinity II Flexible Pump User Manual...

  • Page 33: Turn On/Off

    Using the Pump Turn on/off Turn on/off Power switch (1) On (2) Off Agilent 1290 Infinity II Flexible Pump User Manual...

  • Page 34: Status Indicators

    Using the Pump Status Indicators Status Indicators The module status indicator indicates one of six possible module conditions: Status indicators 1. Idle 2. Run mode 3. Not- ready. Waiting for a specific pre- run condition to be reached or completed. 4.

  • Page 35: Best Practices

    Using the Pump Best Practices Best Practices Daily / Weekly tasks Daily tasks • Replace mobile phase based on water/buffer. • Replace organic mobile phase latest every 2nd day. • Check seal wash solvent. • Run conditioning with composition of your application. Weekly tasks •...

  • Page 36: Prepare The Pump

    Using the Pump Best Practices Prepare the pump Purge Use the Purge function to: • fill the pump, • exchange a solvent, • remove air bubbles in tubes and pump heads. Condition Use the Conditioning function: • daily when starting the pump, •...

  • Page 37: How To Deal With Solvents

    Using the Pump Best Practices How to deal with solvents • Use clean bottles only. • Exchange water- based solvents daily. • Select solvent volume to be used up within 1 – 2 days. • Use only HPLC- grade solvents and water filtered through 0.2 µm filters. •...
  • Page 38 Using the Pump Best Practices Agilent 1290 Infinity II Flexible Pump User Manual...

  • Page 39: How To Optimize The Performance Of Your Module

    Your Module Delay Volume and Extra-Column Volume Delay Volume How to Configure the Optimum Delay Volume How to Achieve Higher Resolution Using Solvent Calibration Tables This chapter gives hints on how to optimize the performance or use additional devices. Agilent Technologies...

  • Page 40: Delay Volume And Extra-Column Volume

    How to Optimize the Performance of Your Module Delay Volume and Extra-Column Volume Delay Volume and Extra-Column Volume The delay volume is defined as the system volume between the point of mixing in the pump and the top of the column. The extra- column volume is defined as the volume between the injection point and the detection point, excluding the volume in the column.

  • Page 41: How To Configure The Optimum Delay Volume

    How to Optimize the Performance of Your Module How to Configure the Optimum Delay Volume How to Configure the Optimum Delay Volume The design of the 1290 Infinity Quaternary Pump offers a strongly decreased delay volume compared to standard 600 bar pressure pumps. For the 1290 Infinity Quaternary Pump, mixing is done in the multi- channel gradient valve at ambient pressure.
  • Page 42 How to Optimize the Performance of Your Module How to Configure the Optimum Delay Volume Figure 9 The Jet Weaver mixer The installation procedure is illustrated in “Install the Jet Weaver” page 97. Agilent 1290 Infinity II Flexible Pump User Manual...

  • Page 43: How To Achieve Higher Resolution

    How to Optimize the Performance of Your Module How to Achieve Higher Resolution How to Achieve Higher Resolution Increased resolution in a separation will improve the qualitative and quantitative data analysis, allow more peaks to be separated or offer further scope for speeding up the separation. This section explains how resolution can be increased by examining the following points: •...
  • Page 44 How to Optimize the Performance of Your Module How to Achieve Higher Resolution ways. N is inversely proportional to the particle size and directly proportional to the length of a column and so smaller particle size and a longer column will give a higher plate number. The pressure rises with the inverse square of the particle size and proportionally with the length of the column.
  • Page 45 How to Optimize the Performance of Your Module How to Achieve Higher Resolution • F = flow (ml/min), • V = column delay volume, • Δ%B = change in fraction of solvent B during the gradient, • S = constant (ca. 4- 5 for small molecules). This shows that k and hence resolution can be increased by having a shallower gradient (2 to 5 %/min change is a guideline), higher flow rate and a smaller volume column.

  • Page 46: Using Solvent Calibration Tables

    How to Optimize the Performance of Your Module Using Solvent Calibration Tables Using Solvent Calibration Tables Importing Solvent Calibration Tables RC.NET based Agilent graphical user interfaces (ChemStation, EZChrom Elite, OpenLab etc.) include data for most commonly used solvents in HPLC. This data contains solvent properties and is used for optimum pump control in order to ensure best flow and composition accuracy.

  • Page 47: Troubleshooting And Diagnostics

    Agilent 1290 Infinity II Flexible Pump User Manual Troubleshooting and Diagnostics User Interfaces Agilent Lab Advisor Software Overview about the troubleshooting and diagnostic features. Agilent Technologies...

  • Page 48: User Interfaces

    Troubleshooting and Diagnostics User Interfaces User Interfaces • Depending on the user interface, the available tests and the screens/reports may vary. • Preferred tool should be Agilent Lab Advisor Software, see “Agilent Lab Advisor Software” on page 49. • The Agilent OpenLab ChemStation C.01.03 and above do not include any maintenance/test functions.

  • Page 49: Agilent Lab Advisor Software

    Troubleshooting and Diagnostics Agilent Lab Advisor Software Agilent Lab Advisor Software The Agilent Lab Advisor Software is a standalone product that can be used with or without chromatographic data system. Agilent Lab Advisor helps to manage the lab for high- quality chromatographic results by providing a detailed system overview of all connected analytical instruments with instrument status, Early Maintenance Feedback counters (EMF), instrument configuration information, and diagnostic tests.
  • Page 50 Troubleshooting and Diagnostics Agilent Lab Advisor Software Agilent 1290 Infinity II Flexible Pump User Manual...

  • Page 51: Error Information

    Quaternary pump shutdown during analysis Reading the pump encoder tag failed Writing the pump encoder tag failed Pump drive blocked or encoder failed Drive current too low Drive current too high Drive timeout Overcurrent of pump drive Deliver underrun Agilent Technologies...
  • Page 52 Error Information Agilent Lab Advisor Software Defect connection between main board and pump drive encoder Pump drive encoder defect Multi Purpose Valve failed Reading of multi purpose valve tag failed Pump drive encoder rollover Drive position limit Insufficient power of drive encoder LED Drive encoder error Writing the multi purpose valve tag failed Unknown multi purpose valve type...

  • Page 53: What Are Error Messages

    Error Information What Are Error Messages What Are Error Messages Error messages are displayed in the user interface when an electronic, mechanical, or hydraulic (flow path) failure occurs which requires attention before the analysis can be continued (for example, repair, or exchange of consumables is necessary).

  • Page 54: General Error Messages

    Error Information General Error Messages General Error Messages General error messages are generic to all Agilent series HPLC modules and may show up on other modules as well. Timeout Error ID: 0062 The timeout threshold was exceeded. Probable cause Suggested actions Check the logbook for the occurrence and The analysis was completed successfully, source of a not-ready condition.

  • Page 55: Remote Timeout

    Error Information General Error Messages Probable cause Suggested actions Fix the leak in the external instrument before Leak detected in another module with a restarting the module. CAN connection to the system. Fix the leak in the external instrument before Leak detected in an external instrument restarting the module.

  • Page 56: Lost Can Partner

    Error Information General Error Messages Lost CAN Partner Error ID: 0071 During an analysis, the internal synchronization or communication between one or more of the modules in the system has failed. The system processors continually monitor the system configuration. If one or more of the modules is no longer recognized as being connected to the system, the error message is generated.

  • Page 57: Leak Sensor Open

    Error Information General Error Messages Leak Sensor Open Error ID: 0083 The leak sensor in the module has failed (open circuit). The current through the leak sensor is dependent on temperature. A leak is detected when solvent cools the leak sensor, causing the leak- sensor current to change within defined limits.

  • Page 58: Compensation Sensor Short

    Error Information General Error Messages Compensation Sensor Short Error ID: 0080 The ambient- compensation sensor (NTC) on the power switch board in the module has failed (open circuit). The resistance across the temperature compensation sensor (NTC) on the power switch board is dependent on ambient temperature. The change in resistance is used by the leak circuit to compensate for ambient temperature changes.

  • Page 59: Fan Failed

    Error Information General Error Messages Fan Failed Error ID: 0068 The cooling fan in the module has failed. The hall sensor on the fan shaft is used by the main board to monitor the fan speed. If the fan speed falls below a certain limit for a certain length of time, the error message is generated.

  • Page 60: Pump Error Messages

    Error Information Pump Error Messages Pump Error Messages These errors are pump specific. Pressure of quaternary pump above upper limit Error ID: 29163 The pressure has exceeded the upper pressure limit. • Parameter: Measured pressure Probable cause Suggested actions • Check for blockages in the LC system, e.g. purge Blockage in flow path after the pressure valve, Jet Weaver, degraded column, column frits, sensor.

  • Page 61: Target Pressure Not Reached For Quaternary Pump Degasser

    Error Information Pump Error Messages Target pressure not reached for quaternary pump degasser Error ID: 29221 The target pressure of the quaternary pump degasser has not been reached within the expected time. • Parameter: Pressure in mbar Probable cause Suggested actions Equilibrate and restart module.

  • Page 62: Waste Counter Limit Exceeded

    Error Information Pump Error Messages Waste counter limit exceeded Error ID: 29147 The counter for the waste volume has exceeded the limit, which has been set in the user interface. • Parameter: None Probable cause Suggested actions Empty waste container. The waste container is full.

  • Page 63: Quaternary Pump Shutdown During Analysis

    Error Information Pump Error Messages Quaternary pump shutdown during analysis Error ID: 29199 The quaternary pump has been shut down by the control software or control module during an analysis. • Parameter: 0 for off, 1 for standby. Probable cause Suggested actions Restart pump.

  • Page 64: Writing The Pump Encoder Tag Failed

    Error Information Pump Error Messages Writing the pump encoder tag failed Error ID: 29200 Writing the pump encoder tag has failed. • Parameter: 1 – 2 referring to pump drive Probable cause Suggested actions Please contact your Agilent service Defect connection between encoder and representative.

  • Page 65: Drive Current Too Low

    Error Information Pump Error Messages Drive current too low Error ID: 29205 The current consumption of the pump drive is too low. • Parameter: 1 – 2 referring to pump drive Probable cause Suggested actions Please contact your Agilent service Drive motor defect.

  • Page 66: Drive Timeout

    Error Information Pump Error Messages Drive timeout Error ID: 29204 Movement of drive during initialization is blocked mechanically. • Parameter: 1 – 2 referring to pump drive Probable cause Suggested actions Remove capillary connection to system, check Blockage in flow path outlet filter, check valves, check pump head.

  • Page 67: Deliver Underrun

    Error Information Pump Error Messages Deliver underrun Error ID: 29233 Internal error. • Parameter: None Probable cause Suggested actions Please contact your Agilent service Internal error. representative. Use a minimum firmware revision of B.06.55 Firmware issue Defect connection between main board and pump drive encoder Error ID: 29208 Defect connection between main board and pump drive encoder.

  • Page 68: Pump Drive Encoder Defect

    Error Information Pump Error Messages Pump drive encoder defect Error ID: 29209 Defect pump drive encoder. • Parameter: 1 – 2 referring to pump drive Probable cause Suggested actions Please contact your Agilent service Defect encoder. representative. Multi Purpose Valve failed Error ID: 29231 Lost steps of the purge valve encoder.

  • Page 69: Reading Of Multi Purpose Valve Tag Failed

    Error Information Pump Error Messages Reading of multi purpose valve tag failed Error ID: 29240 Reading the multi purpose valve tag failed. • Parameter: None Probable cause Suggested actions Check cable connection. Reading of multi purpose valve tag failed. Replace multi purpose valve head. Multi purpose valve head tag defect or empty.

  • Page 70: Drive Position Limit

    Error Information Pump Error Messages Drive position limit Error ID: 29234 Internal error. • Parameter: 1 – 4 referring to pump drive Probable cause Suggested actions Please contact your Agilent service Internal error. representative. Insufficient power of drive encoder LED Error ID: 29235 Insufficient power of drive encoder LED.

  • Page 71: Writing The Multi Purpose Valve Tag Failed

    Error Information Pump Error Messages Writing the multi purpose valve tag failed Error ID: 29241 Writing the multi purpose valve tag failed. • Parameter: None Probable cause Suggested actions Replace multi purpose valve head. Multi purpose valve head tag defect. Please contact your Agilent service Multi purpose valve tag head reader is representative.

  • Page 72: Pump Drive Error

    Error Information Pump Error Messages Pump drive error Error ID: 29212, 29213 The pump drive failed during calibration. • Parameter: 1 – 2 referring to pump drive Probable cause Suggested actions Please contact your Agilent service Pump drive encoder is defect. representative.

  • Page 73: Pump Drive Stop Not Found

    Error Information Pump Error Messages Pump drive stop not found Error ID: 29207 The pump drive stop has not been found. • Parameter: 1 – 2 referring to pump drive Probable cause Suggested actions Please contact your Agilent service Pump drive spindle is defect. representative.

  • Page 74: Timeout: Wait For Run Volume

    Error Information Pump Error Messages Timeout: Wait for run volume Error ID: 29181 A target condition (run volume, which is the volume delivered since the method run start) has been sent to the instrument which should have been reached within an expected time frame but didn’t. Either the limit, time frame or the current value of the variable has been modified later directly or indirectly (for example the flow rate).

  • Page 75: Timeout: Wait For Flow

    Error Information Pump Error Messages Timeout: Wait for Flow Error ID: 29183 A target condition (flow rate) has been sent to the instrument which should have been reached within an expected time frame but didn’t. Either the limit, time frame or the current value of the variable has been modified later directly or indirectly.

  • Page 76: Drive Encoder Failed

    Error Information Pump Error Messages Drive Encoder failed Error ID: 29210 Drive encoder failed during pump drive calibration. Probable cause Suggested actions Contact Agilent support. Internal error. Drive phases differ too much in electric resistance Error ID: 29216 Pump drive calibration has failed due to a strong difference electric resistances for different motor phases.

  • Page 77: Degasser's Pressure Limit Violation

    Error Information Pump Error Messages Degasser's pressure limit violation Error ID: 29220 Pressure too far above the limit. Probable cause Suggested actions Please contact your Agilent service Leak in degasser chamber or degasser representative. tubing. Please contact your Agilent service Defect vacuum pump.

  • Page 78: Valve Hardware Overcurrent (Mcgv)

    Error Information Pump Error Messages Valve hardware overcurrent (MCGV) Error ID: 29227 Power consumption too high for one of the MCGV valves. Probable cause Suggested actions Replace MCGV. Cable defect. Replace MCGV. Valve defect Please contact your Agilent service Defective main board. representative.

  • Page 79: Maintenance

    Disassemble the Primary Pump Head Disassemble the Secondary Pump Head Replacing the Heat Exchanger Replace Wash Seal and Gasket Assemble the Primary and Secondary Pump Head Reassemble the Pump Head Assembly Install the Pump Head Assembly Replace the Multi Purpose Valve Agilent Technologies...
  • Page 80 Maintenance Pump Error Messages Replace Parts of the Multi Purpose Valve Replace the High Pressure Outlet Filter or Filter Frit Replace Parts of the Inline Filter Replace the Module Firmware Prepare the Pump Module for Transport This chapter describes the maintenance of the Agilent 1290 Infinity II Flexible Pump.

  • Page 81: Introduction To Maintenance

    Maintenance Introduction to Maintenance Introduction to Maintenance Figure 10 on page 81 shows the main user- accessible assemblies of the Agilent 1290 Infinity II Flexible Pump. These parts can be accessed from the front (simple repairs) and don’t require to remove the pump from the system stack.

  • Page 82: Warnings And Cautions

    Maintenance Warnings and Cautions Warnings and Cautions Toxic, flammable and hazardous solvents, samples and reagents WA R N I N G The handling of solvents, samples and reagents can hold health and safety risks. ➔ When working with these substances observe appropriate safety procedures (for example by wearing goggles, safety gloves and protective clothing) as described in the material handling and safety data sheet supplied by the vendor, and follow good laboratory practice.
  • Page 83 Maintenance Warnings and Cautions Safety standards for external equipment C A U T I O N ➔ If you connect external equipment to the instrument, make sure that you only use accessory units tested and approved according to the safety standards appropriate for the type of external equipment.

  • Page 84: Overview Of Maintenance

    Maintenance Overview of Maintenance Overview of Maintenance The following pages describe maintenance (simple repairs) of the module that can be carried out without opening the main cover. Agilent 1290 Infinity II Flexible Pump User Manual...

  • Page 85: Cleaning The Module

    Maintenance Cleaning the Module Cleaning the Module To keep the module case clean, use a soft cloth slightly dampened with water, or a solution of water and mild detergent. Liquid dripping into the electronic compartment of your module can cause shock WA R N I N G hazard and damage the module ➔...

  • Page 86: Install Fittings And Capillaries

    Maintenance Install Fittings and Capillaries Install Fittings and Capillaries Solvent can spray under high pressure. WA R N I N G ➔ Observe appropriate safety procedures (for example, goggles, safety gloves and protective clothing), when opening flow path. Deformation of fittings and seals C A U T I O N Liquid drops under high pressure up to 1200 bar act like solid parts.

  • Page 87: Remove And Install Doors

    Maintenance Remove and Install Doors Remove and Install Doors Parts required Description 5067-5745 Door Assy Infinity 180 Left 5067-5746 Door Assembly Infinity 180 Right The figures shown in this procedure exemplarily show the Infinity II Multisampler module. N O T E The principle of how to remove and/or install doors works in the same way for all Infinity II modules.

  • Page 88: Replace The Pressure Sensor

    Maintenance Replace the Pressure Sensor Replace the Pressure Sensor When No or invalid pressure signal Tools required Description 8710-2412 Hex key 2.5 mm, 15 cm long, straight handle 8710-0510 Wrench open 1/4 — 5/16 inch Screwdriver Parts required Description G7104-60001 Pressure sensor 1300 bar Preparations Turn off pump flow, switch off pump...
  • Page 89 Maintenance Replace the Pressure Sensor Carefully pull out the pressure sensor for about 2 cm. Connect the new pressure sensor to the pressure sensor Then unscrew the cable from the pressure sensor. connector. Fix the pressure sensor to the instrument chassis. Connect the capillary from the pump head outlet to the pressure sensor inlet (1).

  • Page 90: Replace The Inlet Weaver

    Maintenance Replace the Inlet Weaver Replace the Inlet Weaver Parts required Description G4204-81090 1290 Infinity Quaternary Pump Inlet Weaver Assembly Preparations • Switch off pump at the main power switch • Open the doors • Use an optional solvent shutoff valve or lift up solvent filters inside solvent bottles for avoiding leakages •...
  • Page 91 Maintenance Replace the Inlet Weaver Pull the Inlet Weaver out of the Inlet Valve. Insert the new inlet weaver to the inlet valve. Fix the weaver with the plastic screw. Fix the fitting of the new inlet weaver to the MCGV. Reconnect tubings between MCGV and degasser.

  • Page 92: Replace The Inlet Valve

    Maintenance Replace the Inlet Valve Replace the Inlet Valve When If Inlet valve is defective. Tools required Description Wrench, 14 mm G4220-20012 Torque wrench 2 – 25 Nm Parts required Description G4204-60022 Inlet Valve 1290 Infinity Quaternary Pump Preparations • Switch off pump at the main power switch •...

  • Page 93: Replace The Outlet Valve

    Maintenance Replace the Outlet Valve Replace the Outlet Valve When If Outlet valve is defective. Tools required Description Wrench, 14 mm G4220-20012 Torque wrench 2 – 25 Nm G4220-20041 Bit Torx 10x25 mm Parts required Description G4220-60028 Outlet valve (primary pump head) G4220-20020 Internal gold seal for Outlet Valve Preparations...
  • Page 94 Maintenance Replace the Outlet Valve A gold seal between outlet valve and heat exchanger Unscrew the outlet valve with a 14 mm wrench (1) and capillary is used for a tight connection. The seal can be remove it (2). replaced separately as needed. Insert the new outlet valve and tighten it using a torque Insert the heat exchanger capillary into the outlet of the wrench with a 14 mm bit set to 10 Nm.

  • Page 95: Remove The Jet Weaver

    Maintenance Remove the Jet Weaver Remove the Jet Weaver Tools required Description 8710-0510 Wrench open 1/4 — 5/16 inch 8710-0899 Pozidriv screwdriver Parts required Description 0100-1259 Plastic fittings Preparations • Select Do not use mixer in ChemStation. • Switch off the pump at the main power switch. Remove capillary connections from the Jet Weaver to the Open the screw which fixes the Jet Weaver to the front Multi Purpose Valve.
  • Page 96 Maintenance Remove the Jet Weaver Lift up the Jet Weaver (1) and pull it out of the front panel If no other Jet Weaver shall be installed, use plastic (2). fittings for closing unused ports of the valve and install the metal lid.

  • Page 97: Install The Jet Weaver

    Maintenance Install the Jet Weaver Install the Jet Weaver When The optional Jet Weaver 380 µL for 1290 Infinity Quaternary Pump (G4204-68000) is available for applications which require highest mixing performance, see chapter Optimizing Performance. Tools required Description Screwdriver Pozidriv #1 Parts required Description G4204-68000...
  • Page 98 Maintenance Install the Jet Weaver Insert the Jet Weaver to the opening in the front panel (1) Fix the Jet Weaver with a screw. and push it down (2). Mount both capillary connections to the Jet Weaver Connect the inlet capillary of the Jet Weaver to port 2 of observing the correct orientation.

  • Page 99: Replace The Seal Wash Pump

    Maintenance Replace the Seal Wash Pump Replace the Seal Wash Pump When In case of wear of the seal wash pump Parts required Description 5065-4445 Peristaltic pump with Pharmed tubing 5065-9978 Tubing, 1 mm i.d., 3 mm o.d., silicone, 5 m Preparations Remove the flow connections from and to the seal wash pump.

  • Page 100: Replace The Multi-Channel Gradient Valve (Mcgv)

    Maintenance Replace the Multi-Channel Gradient Valve (MCGV) Replace the Multi-Channel Gradient Valve (MCGV) Tools required Description 0100-1710 Mounting Tool for Tubing Connections 8710-0899 Pozidriv screwdriver Parts required Description G1311-67701 Multi channel gradient valve (MCGV) Preparations • Switch off pump at the main power switch •...
  • Page 101 Maintenance Replace the Multi-Channel Gradient Valve (MCGV) Disconnect the MCGV cable (1), unscrew the two screws Place the new MCGV into position. (2, 3) and remove the valve. N O T E Make sure that channel A of the MCGV is put at the bottom-right position.

  • Page 102: Release A Stuck Inlet Valve

    Maintenance Release a Stuck Inlet Valve Release a Stuck Inlet Valve Tools required Description 9301-0411 Syringe, Plastic 0100-1681 Syringe adapter luer/barb 0100-1710 Mounting Tool for Tubing Connections Beaker Pressure damages the multi-channel gradient valve (MCGV) and/or degasser C A U T I O N ➔...
  • Page 103 Maintenance Release a Stuck Inlet Valve Slightly open the black plastic screw at the bottom of the Disconnect the capillary from the pressure sensor inlet inlet valve, and rotate the inlet weaver to the front. Then and route the capillary to a small beaker. retighten the screw.

  • Page 104: Pump Head Procedures

    Maintenance Pump Head Procedures Pump Head Procedures Limitation of life time C A U T I O N The pump head assembly is an exchange part which cannot be reassembled with standard tools. Disassembling the pump head will strongly limit its life time. ➔...
  • Page 105 Maintenance Pump Head Procedures Damaged pump head C A U T I O N Disassembling or reassembling the pump head with tools other than the ones recommended can damage pump heads and significantly reduce their life time. ➔ Follow all instructions step by step. ➔...

  • Page 106: Remove The Pump Head Assembly

    Maintenance Pump Head Procedures Remove the Pump Head Assembly Tools required Description G4220-20012 Torque wrench 2 – 25 Nm G4220-20013 4 mm hex bit G4220-20041 Bit Torx 10x25 mm 8710-0510 Wrench open 1/4 — 5/16 inch Preparations Remove the pump from the stack. In Lab Advisor go to Tools >...
  • Page 107 Maintenance Pump Head Procedures Use the mounting tool for removing tubing connections Open the black plastic screw of the inlet valve at the between the degassing unit and the MCGV. bottom of the left primary pump head (1) and remove the inlet weaver by first pushing it downwards (2) and then pulling it out to the left (3).

  • Page 108: Disassemble The Pump Head Assembly

    Maintenance Pump Head Procedures Disassemble the Pump Head Assembly When If parts inside the pump head need to be replaced Tools required Description G4220-20012 Torque wrench 2 – 25 Nm G4220-20013 4 mm hex bit G4220-20014 2.5 mm Hex Bit G4220-20015 Adapter ¼...
  • Page 109 Maintenance Pump Head Procedures Place the pump head on a special holding tool. Open the 2.5 mm hex or Tx 10 screw at the top of the primary pump head, which fixes the connection capillary of the heat exchanger (1). Then lift up the capillary and remove it from the primary pump head (2).
  • Page 110 Maintenance Pump Head Procedures Remove the outlet filter at the top of the secondary pump head. Agilent 1290 Infinity II Flexible Pump User Manual...

  • Page 111: Disassemble The Primary Pump Head

    Maintenance Pump Head Procedures Disassemble the Primary Pump Head Damage of pump piston C A U T I O N The pump piston is made of ZrO -based ceramic, which is a very hard and resistant material, but it is sensitive to shearing forces from the side. ➔...
  • Page 112 Maintenance Pump Head Procedures Remove the piston from the piston housing by pushing it Check the pump pistons for scratches grooves and dents to the rear, then pull it out from the rear. Piston surface Use the steel side of the insert tool for removing the To flush out particles from the pump head, use pump seal from the pump chamber housing.
  • Page 113 Maintenance Pump Head Procedures To remove wear, use isopropanol. To dry the pump head and to remove residues, use pressurized air ((1), (2) and (3)). To clean the piston and the pump head sufrace, use the ultra fine abrasive mesh (p/n 8660-0852). If the wash seal shall be replaced by a new one, use the steel side of the insert tool for removing it.

  • Page 114: Disassemble The Secondary Pump Head

    Maintenance Pump Head Procedures Disassemble the Secondary Pump Head Damage of pump piston C A U T I O N The pump piston is made of ZrO -based ceramic, which is a very hard and resistant material, but it is sensitive to shearing forces from the side. ➔...
  • Page 115 Maintenance Pump Head Procedures Remove the piston from the piston housing by pushing it Check the pump pistons for scratches, grooves and dents to the rear, then pull it out from the rear. when changing the piston seals. N O T E Damaged pistons cause micro leaks and will decrease the lifetime of the seals.
  • Page 116 Maintenance Pump Head Procedures To remove wear, use isopropanol. To dry the pump head and to remove residues, use pressurized air ((1), (2) and (3)). To clean the piston and the pump head sufrace, use the ultra fine abrasive mesh (p/n 8660-0852). If the wash seal shall be replaced by a new one, use the steel side of the insert tool for removing it.

  • Page 117: Replacing The Heat Exchanger

    Maintenance Pump Head Procedures Replacing the Heat Exchanger Tools required Description Wrench, 19 mm Parts required Description G4220-81013 Heat Exchanger (secondary pump head only) G4220-20028 Headless screw for 1290 Infinity pump heads G4220-20001 Spacer Fitting Preparations • Remove the pump head assembly from the pump •...
  • Page 118 Maintenance Pump Head Procedures Remove the 2.5 mm hex screw at the bottom of the pump Lift out the heat exchanger. head. Do not drop the golden spacer fitting. Hex screw If removed, first insert the spacer fitting. Then insert the Use the 19 mm screw for fixing the front plate.
  • Page 119 Maintenance Pump Head Procedures Insert and fix the 2.5 mm hex screw. Hex screw Agilent 1290 Infinity II Flexible Pump User Manual...

  • Page 120: Replace Wash Seal And Gasket

    Maintenance Pump Head Procedures Replace Wash Seal and Gasket To remove the wash seal use the steel side of the insert Use the soft plastic side of the insert tool for inserting the tool. wash seal into the support ring. Wash seal N O T E Clean seals before Reinstallation or use new ones.
  • Page 121 Maintenance Pump Head Procedures Put the gasket into the support ring and insert the seal holder. Agilent 1290 Infinity II Flexible Pump User Manual...

  • Page 122: Assemble The Primary And Secondary Pump Head

    Maintenance Pump Head Procedures Assemble the Primary and Secondary Pump Head This procedure describes how to assemble the secondary pump head using the pump head alignment tool. Assembling the primary pump head can be done accordingly. The secondary pump head has the heat exchanger capillary, which must fit into the openings of the alignment tool, whereas the primary pump head does not have a heat exchanger.
  • Page 123 Maintenance Pump Head Procedures Damage of the pump head assembly C A U T I O N When installing the pump head assembly, the pump drives need to be in maintenance position, where they are retracted. Using the pump drive in default position will damage the pump head assembly.
  • Page 124 Maintenance Pump Head Procedures Assemble the pump head by putting the pump chamber Loosely close the 4 screws at the rear of the pump head. housing on top of the support ring. Observe correct The screws will be fixed tightly later. orientation of the pin.
  • Page 125 Maintenance Pump Head Procedures Insert the alignment piston of the pump head alignment C A U T I O N tool. Damage to the pump head. ➔ Using the alignment tool is mandatory. Alignment piston ➔ Not using will break the pump head. Insert the pump head to the pump head alignment tool, which is included to the 1290 Infinity Service Kit p/n 5067-4699.
  • Page 126 Maintenance Pump Head Procedures Close the tool by closing the 3 screws at the connection C A U T I O N ring. Damage to the pump head Using a wrong torque will damage the pump head. Heat exchanger capillary ➔...
  • Page 127 Maintenance Pump Head Procedures Open the 3 screws which have closed the pump head C A U T I O N alignment tool and take out the aligned pump head. In case the pump head sticks inside the alignment tool, you Damage to the pump head can use the handle and insert it to the rear of the tool for Using a wrong torque will damage the pump head.
  • Page 128 Maintenance Pump Head Procedures C A U T I O N C A U T I O N Damage to the pump head Damage to the pump head Using a wrong torque will damage the pump head. Using a wrong torque will damage the pump head. ➔...
  • Page 129 Maintenance Pump Head Procedures Remove the alignment piston. Insert the pump piston. Piston Agilent 1290 Infinity II Flexible Pump User Manual...

  • Page 130: Reassemble The Pump Head Assembly

    Maintenance Pump Head Procedures Reassemble the Pump Head Assembly Insert both pump heads to the link plate and make sure C A U T I O N that the clips snap in that fix the pump heads. Damage to the pump head Using a wrong torque will damage the pump head.

  • Page 131: Install The Pump Head Assembly

    Maintenance Pump Head Procedures Install the Pump Head Assembly Bring the pump drive to the maintenance position using C A U T I O N the Lab Advisor user interface: Go to Tools > Remove/Install Pump Head and follow instructions Damage to the pump head given on the screen.
  • Page 132 Maintenance Pump Head Procedures Insert the new inlet weaver to the inlet valve (1, 2). Fix Reconnect solvent tubes for channels A-D from the the weaver with the plastic screw to the inlet valve (3). MCGV to the degasser outlets. Connect the capillary from the outlet filter adapter on the Connect the seal wash tubes.

  • Page 133: Replace The Multi Purpose Valve

    Maintenance Replace the Multi Purpose Valve Replace the Multi Purpose Valve Tools required Description 5023-0240 Hex driver, ¼", slitted Parts required Description 0100-1259 Blank nut (plastic) 01080-83202 Blank nut (stainless steel) 5067-4237 Multi Purpose Valve Head Preparations Remove all capillary connections from the Multi Purpose Valve. Remove the clamp with the inline filter.
  • Page 134 Maintenance Replace the Multi Purpose Valve Put the new valve head onto the valve drive such that the lobe fits to the groove. Screw the valve head onto the valve drive using the union nut. The central (C) port is connected to the outlet of the pressure sensor. •...

  • Page 135: Replace Parts Of The Multi Purpose Valve

    Maintenance Replace Parts of the Multi Purpose Valve Replace Parts of the Multi Purpose Valve Tools required Description 8710-2394 9/64 inch hex key Parts required Description 1535-4045 Bearing ring 5068-0202 Rotor seal, Multi Purpose Valve, 1300 bar 5068-0120 Stator ring 5068-0001 Stator head 1535-4857...

  • Page 136: Replace The High Pressure Outlet Filter Or Filter Frit

    Maintenance Replace the High Pressure Outlet Filter or Filter Frit Replace the High Pressure Outlet Filter or Filter Frit When For removing blockages and leaks in the high pressure filter assembly. The outlet filter should be replaced as required depending on the system usage. Other parts are covered by the Agilent Preventive Maintenance (PM) Service.
  • Page 137 Maintenance Replace the High Pressure Outlet Filter or Filter Frit Unscrew the high pressure outlet filter. Replace the filter frit. Mount the high pressure outlet filter using a torque Reinstall the high pressure outlet filter to the filter holder. wrench set to 16 Nm. Mount the capillary connection to the pressure sensor (1) and to the Multipurpose valve (2).

  • Page 138: Replace Parts Of The Inline Filter

    Maintenance Replace Parts of the Inline Filter Replace Parts of the Inline Filter Tools required Description 8710-0510 Wrench open 1/4 — 5/16 inch Parts required Description 5067-5407 In-Line Filter Assembly for 1290 Infinity Quaternary Pump 5067-4748 Capillary ST, 0.17 mm x 90 mm Multi Purpose Valve to inline filter 5023-0271 Frit 0.3 µm for inline filter, 5/pk...
  • Page 139 Maintenance Replace Parts of the Inline Filter Use two 5/16 wrenches for opening the inline filter. Replace the filter frit and reassemble the inline filter. Put the inline filter to the clamp and install its capillaries. The integrated capillary is connected to port 5 of the Multi Purpose Valve.

  • Page 140: Replace The Module Firmware

    Maintenance Replace the Module Firmware Replace the Module Firmware When The installation of newer firmware might be necessary • if a newer version solves problems of older versions or • to keep all systems on the same (validated) revision. The installation of older firmware might be necessary •...

  • Page 141: Prepare The Pump Module For Transport

    Maintenance Prepare the Pump Module for Transport Prepare the Pump Module for Transport When If the module shall be transported or shipped. Parts required Description 9301-0411 Syringe; Plastic 9301-1337 Syringe adapter G7104-44000 Transport protection foam Mechanical damage C A U T I O N ➔...
  • Page 142 Maintenance Prepare the Pump Module for Transport Reconnect the degasser outlet tubings to the MCGV. You may keep internal tubing and capillary connections. Remove the degasser inlet tubings. Next Steps: Carefully insert the protective foam to the front part of the instrument.

  • Page 143: Parts And Materials

    Overview of Main Assemblies Flow Connections Pump Head Assembly Parts Primary Pump Head Parts Secondary Pump Head Parts Multi Purpose Valve Cover Parts Accessory Kit Tool Kit Tools This chapter provides information on parts for maintenance and repair. Agilent Technologies...

  • Page 144: Overview Of Main Assemblies

    Parts and Materials Overview of Main Assemblies Overview of Main Assemblies Figure 11 Overview of main assemblies Agilent 1290 Infinity II Flexible Pump User Manual...
  • Page 145 Parts and Materials Overview of Main Assemblies Item Description 5067-5407 In-Line Filter Assembly for 1290 Infinity Quaternary Pump 5023-0271 Frit 0.3 µm for inline filter, 5/pk G4204-40000 Clamp for In-Line Filter 5067-4237 Multi Purpose Valve Head G4204-60022 Inlet Valve 1290 Infinity Quaternary Pump G4204-81090 1290 Infinity Quaternary Pump Inlet Weaver Assembly G1311-67701...

  • Page 146: Flow Connections

    Parts and Materials Flow Connections Flow Connections Figure 12 Flow connections of the pump Agilent 1290 Infinity II Flexible Pump User Manual...
  • Page 147 Parts and Materials Flow Connections Item Description G4220-60035 Tubing kit 140 mm, 2/pk Degasser to MCGV G7120-60007 Bottle Head Assembly 5067-5760 Solvent Cabinet Kit (not shown) 5065-9978 Tubing, 1 mm i.d., 3 mm o.d., silicone, 5 m 5065-4445 Peristaltic pump with Pharmed tubing 5067-4656 Capillary ST, 0.25 mm x 80 mm Pressure Sensor to Outlet Filter, to Pump Head, and to Multi...

  • Page 148: Pump Head Assembly Parts

    Parts and Materials Pump Head Assembly Parts Pump Head Assembly Parts Agilent 1290 Infinity II Flexible Pump User Manual...
  • Page 149 Parts and Materials Pump Head Assembly Parts Item Description G4220-81013 Heat Exchanger (secondary pump head only) Channel A G4220-60022 Inlet valve (primary pump head) G4220-60028 Outlet valve (primary pump head) G4220-20020 Internal gold seal for Outlet Valve Adapter Agilent 1290 Infinity II Flexible Pump User Manual...

  • Page 150: Primary Pump Head Parts

    Parts and Materials Primary Pump Head Parts Primary Pump Head Parts Figure 13 Primary pump head parts Agilent 1290 Infinity II Flexible Pump User Manual...
  • Page 151 Parts and Materials Primary Pump Head Parts Primary Head G4204- 60060 Item Description 0515-1218 Screw M5, 40 mm long G4204-60033 PH Body prim 0905-1719 Metering seal 100 µL 5023-2513 Distance sheet G4220-60016 Seal holder including backup ring 01018-07102 Gasket (Seal wash) 0905-1718 Backup Seal PE (Seal Wash) G4220-63010...

  • Page 152: Secondary Pump Head Parts

    Parts and Materials Secondary Pump Head Parts Secondary Pump Head Parts Figure 14 Secondary pump head parts Agilent 1290 Infinity II Flexible Pump User Manual...
  • Page 153 Parts and Materials Secondary Pump Head Parts Secondary Head G4204- 60061 Item Description 0515-1218 Screw M5, 40 mm long G4220-20003 Pump Head Screw G4220-20000 G4220-81013 Heat Exchanger G2404-25213 PH Body sec G4220-20028 Headless screw for 1290 Infinity pump heads (not shown) G4220-20001 Spacer Fitting (not shown)

  • Page 154: Multi Purpose Valve

    Parts and Materials Multi Purpose Valve Multi Purpose Valve Figure 15 Multi Purpose Valve parts Item Description 1535-4857 Stator screws, 10/Pk 5068-0001 Stator head 5068-0120 Stator ring 5068-0202 Rotor seal, Multi Purpose Valve, 1300 bar 1535-4045 Bearing ring Agilent 1290 Infinity II Flexible Pump User Manual...

  • Page 155: Cover Parts

    Parts and Materials Cover Parts Cover Parts Description G4224-60200 Side Cover Right 200 G4224-60201 Side Cover Left 200 5043-0286 Base Cover 5067-5908 Top Cover 5067-5767 Door assy 200 left IF II 5067-5768 Door assy 200 right IF II Agilent 1290 Infinity II Flexible Pump User Manual...

  • Page 156: Accessory Kit

    Parts and Materials Accessory Kit Accessory Kit G7104-68705 Description 0100-1816 Fitting Waste Tube to Purge Valve 0890-2207 Tubing/Sleeving-Flex 5023-0271 Frit 0.3 µm for inline filter, 5/pk 5043-1013 Tubing Clip 5063-6527 Tubing assembly, i.d. 6 mm, o.d. 9 mm, 1.2 m (to waste) 5067-4670 SST cap.

  • Page 157: Tool Kit

    Parts and Materials Tool Kit Tool Kit Description 8720-0025 Wrench, 1/2 inch & 9/16 inch 8710-1924 Wrench open 14 mm 8710-2409 Wrench open end, 5/16 – 3/8 inch 8710-0510 Wrench open 1/4 — 5/16 inch 5023-2500 Wrench 8710-1534 Wrench, 4 mm both ends, open end 5043-1361 Hex Key Set Driver 5023-2499...

  • Page 158: Tools

    Parts and Materials Tools Tools Item Description 5067-4699 1290 Infinity pump service kit 5067-5688 Torque wrench 1 – 25 Nm with 14 mm wrench G4220-20013 4 mm hex bit G4220-20014 2.5 mm Hex Bit G4220-20015 Adapter ¼ in square to hex 5067-5691 Wrench open, 19 mm G4220-20041...
  • Page 159 Parts and Materials Tools Alignment piston Tool handle Figure 17 Replacement kit for 1290 Infinity pump head alignment tool (piston/handle) Figure 18 HPLC System Tool Kit-Infinity-II Agilent 1290 Infinity II Flexible Pump User Manual...
  • Page 160 Parts and Materials Tools Agilent 1290 Infinity II Flexible Pump User Manual...

  • Page 161: Identifying Cables

    Agilent 1290 Infinity II Flexible Pump User Manual Identifying Cables Cable Overview Analog Cables Remote Cables CAN/LAN Cables Agilent Module to PC USB Cables This chapter provides information on cables used with the modules. Agilent Technologies...

  • Page 162: Cable Overview

    Identifying Cables Cable Overview Cable Overview Never use cables other than the ones supplied by Agilent Technologies to ensure proper N O T E functionality and compliance with safety or EMC regulations. Analog cables Description 35900-60750 Agilent 35900A A/D converter...
  • Page 163 Identifying Cables Cable Overview LAN cables Description 5023-0203 Cross-over network cable, shielded, 3 m (for point to point connection) 5023-0202 Twisted pair network cable, shielded, 7 m (for point to point connection) RS-232 cables (not for FUSION Description board) G1530-60600 RS-232 cable, 2 m RS232-61601 RS-232 cable, 2.5 m...

  • Page 164: Analog Cables

    Identifying Cables Analog Cables Analog Cables One end of these cables provides a BNC connector to be connected to Agilent modules. The other end depends on the instrument to which connection is being made. Agilent Module to 35900 A/D converters p/n 35900-60750 35900 Pin Agilent...
  • Page 165 Identifying Cables Analog Cables Agilent Module to BNC Connector p/n 8120-1840 Pin BNC Pin Agilent Signal Name module Shield Shield Analog - Center Center Analog + Agilent Module to General Purpose p/n 01046-60105 Pin Agilent Signal Name module Not connected Black Analog - Analog +...

  • Page 166: Remote Cables

    Identifying Cables Remote Cables Remote Cables ERI (Enhanced Remote Interface) 5188- 8029 ERI to general purpose p/n 5188-8029 Enhanced Remote Classic Remote START REQUEST STOP READY POWER ON NOT USED SHUT DOWN START PREPARE 1wire DATA DGND +5V ERI out PGND PGND +24V ERI out...
  • Page 167 Identifying Cables Remote Cables Table 3 5188-8044 ERI to ERI p/n 5188-8044 Pin (ERI) Signal Pin (ERI) Start Request Stop Ready Power on Future Shut Down Start Prepare Ground Cable Shielding Connection 5188- 8045 ERI to APG (Connector D_Subminiature 15 pin (ERI), Connector D_Subminiature 9 pin (APG)) p/n 5188-8045 Pin (ERI)
  • Page 168 Identifying Cables Remote Cables One end of these cables provides a Agilent Technologies APG (Analytical Products Group) remote connector to be connected to Agilent modules. The other end depends on the instrument to be connected to. Agilent Module to Agilent 35900 A/D Converters...
  • Page 169 Identifying Cables Remote Cables Agilent Module to General Purpose p/n 01046-60201 Wire Color Pin Agilent Signal Name Active module (TTL) White Digital ground Brown Prepare run Gray Start Blue Shut down Pink connected Yellow Power on High Ready High Green Stop Black Start request...

  • Page 170: Can/Lan Cables

    Identifying Cables CAN/LAN Cables CAN/LAN Cables Both ends of this cable provide a modular plug to be connected to Agilent modules CAN or LAN connectors. CAN Cables Description 5181-1516 CAN cable, Agilent module to module, 0.5 m 5181-1519 CAN cable, Agilent module to module, 1 m LAN Cables Description 5023-0203...

  • Page 171: Agilent Module To Pc

    Identifying Cables Agilent Module to PC Agilent Module to PC Description G1530-60600 RS-232 cable, 2 m RS232-61601 RS-232 cable, 2.5 m Instrument to PC, 9-to-9 pin (female). This cable has special pin-out, and is not compatible with connecting printers and plotters. It's also called "Null Modem Cable"...

  • Page 172: Usb Cables

    Identifying Cables USB Cables USB Cables To connect a USB Flash Drive use a USB OTG cable with Mini- B plug and A socket. Description 5188-8050 USB A M-USB Mini B 3 m (PC-Module) 5188-8049 USB A F-USB Mini B M OTG (Module to Flash Drive) Agilent 1290 Infinity II Flexible Pump User Manual...

  • Page 173: Hardware Information

    Firmware Description Electrical Connections Serial Number Information Rear View of the Module Interfaces Overview Interfaces Setting the 8-bit Configuration Switch Special Settings Early Maintenance Feedback Instrument Layout This chapter describes the pump in more detail on hardware and electronics. Agilent Technologies...

  • Page 174: Firmware Description

    Hardware Information Firmware Description Firmware Description The firmware of the instrument consists of two independent sections: • a non- instrument specific section, called resident system • an instrument specific section, called main system Resident System This resident section of the firmware is identical for all Agilent 1100/1200/1220/1260/1290 series modules.
  • Page 175 Hardware Information Firmware Description Firmware Updates Firmware updates can be done using the following tools (latest version should be used): • Agilent Lab Advisor software with files on the hard disk • Firmware Update Tool with local files on the hard disk •...
  • Page 176 Hardware Information Firmware Description Figure 19 Firmware Update Mechanism Some modules are limited in downgrading due to their main board version or their initial N O T E firmware revision. For example, a G1315C DAD SL cannot be downgraded below firmware revision B.01.02 or to a A.xx.xx.

  • Page 177: Electrical Connections

    There are no externally accessible fuses, because automatic electronic fuses are implemented in the power supply. Never use cables other than the ones supplied by Agilent Technologies to ensure proper N O T E functionality and compliance with safety or EMC regulations.

  • Page 178: Serial Number Information

    Hardware Information Electrical Connections Serial Number Information The serial number information on the instrument labels provide the following information: CCYWWSSSSS Format country of manufacturing • DE = Germany • JP = Japan • CN = China year and week of last major manufacturing change, e.g. 820 could be week 20 of 1998 or 2008 SSSSS real serial number...

  • Page 179: Interfaces

    Hardware Information Interfaces Interfaces The Agilent 1200 Infinity Series II modules provide the following interfaces: Table 4 Agilent 1200 Infinity II Series Interfaces Module RS-232 Analog Special (on-board) (A) / ERI (E) Pumps G7104A Flexible Pump G7120A High Speed Pump Samplers G7129A/B ALS G7167A/B Multisampler...

  • Page 180: Overview Interfaces

    Hardware Information Interfaces • CAN connectors as interface to other modules • LAN connector as interface to the control software • RS- 232C as interface to a computer • USB (Universal Series Bus) as interface to a computer • REMOTE connector as interface to other Agilent products •...
  • Page 181 Hardware Information Interfaces RS-232C (Serial) The RS- 232C connector is used to control the module from a computer through RS- 232C connection, using the appropriate software. This connector can be configured with the configuration switch module at the rear of the module. Refer to Communication Settings for RS- 232C. There is no configuration possible on main boards with on-board LAN.
  • Page 182 APG Remote The APG Remote connector may be used in combination with other analytical instruments from Agilent Technologies if you want to use features as common shut down, prepare, and so on. Remote control allows easy connection between single instruments or systems to ensure coordinated analysis with simple coupling requirements.
  • Page 183 Hardware Information Interfaces • standard TTL levels (0 V is logic true, + 5.0 V is false), • fan- out is 10, • input load is 2.2 kOhm against + 5.0 V, and • output are open collector type, inputs/outputs (wired- or technique). All common TTL circuits operate with a 5 V power supply.

  • Page 184: Setting The 8-Bit Configuration Switch

    Hardware Information Setting the 8-bit Configuration Switch Setting the 8-bit Configuration Switch The 8- bit configuration switch is located at the rear of the module. Switch settings provide configuration parameters for LAN, serial communication protocol and instrument specific initialization procedures. All modules with on- board LAN: •...
  • Page 185 Hardware Information Setting the 8-bit Configuration Switch To perform any LAN configuration, SW1 and SW2 must be set to OFF. For details on the N O T E LAN settings/configuration refer to chapter LAN Configuration. Table 7 8-bit Configuration Switch (with on-board LAN) Mode Function SW 1...

  • Page 186: Special Settings

    Hardware Information Setting the 8-bit Configuration Switch Special Settings The special settings are required for specific actions (normally in a service case). The tables include both settings for modules – with on-board LAN and without on-board N O T E LAN.

  • Page 187: Early Maintenance Feedback

    Hardware Information Early Maintenance Feedback Early Maintenance Feedback Maintenance requires the exchange of components which are subject to wear or stress. Ideally, the frequency at which components are exchanged should be based on the intensity of usage of the module and the analytical conditions, and not on a predefined time interval.

  • Page 188: Instrument Layout

    Hardware Information Instrument Layout Instrument Layout The industrial design of the module incorporates several innovative features. It uses Agilent’s E- PAC concept for the packaging of electronics and mechanical assemblies. This concept is based upon the use of expanded polypropylene (EPP) layers of foam plastic spacers in which the mechanical and electronic boards components of the module are placed.

  • Page 189: Lan Configuration

    Changing the IP Address of an Instrument Using the Agilent BootP Service Manual Configuration With Telnet PC and User Interface Software Setup Setup PC Setup for Local Configuration User Interface Software Setup This chapter provides information on connecting the module to the controller software. Agilent Technologies...

  • Page 190: What You Have To Do First

    LAN Configuration What You Have To Do First What You Have To Do First The module has an on- board LAN communication interface. 1 Note the MAC (Media Access Control) address for further reference. The MAC or hardware address of the LAN interfaces is a world wide unique identifier.

  • Page 191: Tcp/Ip Parameter Configuration

    LAN Configuration TCP/IP Parameter Configuration TCP/IP Parameter Configuration To operate properly in a network environment, the LAN interface must be configured with valid TCP/IP network parameters. These parameters are: • IP address • Subnet Mask • Default Gateway The TCP/IP parameters can be configured by the following methods: •...

  • Page 192: Configuration Switch

    LAN Configuration Configuration Switch Configuration Switch The configuration switch can be accessed at the rear of the module. Figure 25 Location of Configuration Switch The module is shipped with all switches set to OFF, as shown above. To perform any LAN configuration, SW1 and SW2 must be set to OFF. N O T E Table 10 Factory Default Settings...

  • Page 193: Initialization Mode Selection

    LAN Configuration Initialization Mode Selection Initialization Mode Selection The following initialization (init) modes are selectable: Table 11 Initialization Mode Switches SW 6 SW 7 SW 8 Init Mode Bootp Bootp & Store Using Stored Using Default DHCP Requires firmware B.06.40 or above. Modules without LAN on board, see G1369C LAN Interface Card Bootp When the initialization mode Bootp is selected, the module tries to download the parameters from a Bootp Server.
  • Page 194 LAN Configuration Initialization Mode Selection Bootp & Store When Bootp & Store is selected, the parameters obtained from a Bootp Server become the active parameters immediately. In addition, they are stored to the non- volatile memory of the module. Thus, after a power cycle they are still available.
  • Page 195 LAN Configuration Initialization Mode Selection Using Stored When initialization mode Using Stored is selected, the parameters are taken from the non- volatile memory of the module. The TCP/IP connection will be established using these parameters. The parameters were configured previously by one of the described methods. Figure 28 Using Stored (Principle) Using Default...
  • Page 196 LAN Configuration Initialization Mode Selection Since the default IP address is a so- called local address, it will not be routed by any network device. Thus, the PC and the module must reside in the same subnet. The user may open a Telnet session using the default IP address and change the parameters stored in the non- volatile memory of the module.

  • Page 197: Dynamic Host Configuration Protocol (Dhcp)

    LAN Configuration Dynamic Host Configuration Protocol (DHCP) Dynamic Host Configuration Protocol (DHCP) General Information (DHCP) The Dynamic Host Configuration Protocol (DHCP) is an auto configuration protocol used on IP networks. The DHCP functionality is available on all Agilent HPLC modules with on- board LAN Interface or LAN Interface Card, and “B”- firmware (B.06.40 or above).

  • Page 198: Setup (Dhcp)

    LAN Configuration Dynamic Host Configuration Protocol (DHCP) Setup (DHCP) Software required The modules in the stack must have at least firmware from set A.06.34 and the above mentioned modules B.06.40 or above (must from the same firmware set). 1 Note the MAC address of the LAN interface (provided with G1369C LAN Interface Card or Main Board).
  • Page 199 LAN Configuration Dynamic Host Configuration Protocol (DHCP) Table 14 LC Modules inclusive 1120/1220 (configuration switch at rear of the instru- ment) SW 6 SW 7 SW 8 Initialization Mode DHCP 3 Turn on the module that hosts the LAN interface. 4 Configure your Control Software (e.g.

  • Page 200: Link Configuration Selection

    LAN Configuration Link Configuration Selection Link Configuration Selection The LAN interface supports 10 or 100 Mbps operation in full- or half- duplex modes. In most cases, full- duplex is supported when the connecting network device - such as a network switch or hub - supports IEEE 802.3u auto- negotiation specifications.

  • Page 201: Automatic Configuration With Bootp

    LAN Configuration Automatic configuration with Bootp Automatic configuration with Bootp All examples shown in this chapter will not work in your environment. You need your own N O T E IP-, Subnet-Mask- and Gateway addresses. Assure that the detector configuration switch is set properly. The setting should be either N O T E BootP or BootP &...

  • Page 202: How Bootp Service Works

    LAN Configuration Automatic configuration with Bootp How BootP Service Works When an instrument is powered on, an LAN Interface in the instrument broadcasts a request for an IP address or host name and provides its hardware MAC address as an identifier. The Agilent BootP Service answers this request and passes a previously defined IP address and host name associated with the hardware MAC address to the requesting instrument.

  • Page 203: Installation Of Bootp Service

    LAN Configuration Automatic configuration with Bootp Installation of BootP Service Before installing and configuring the Agilent BootP Service, be sure to have the IP addresses of the computer and instruments on hand. 1 Log on as Administrator or other user with Administrator privileges. 2 Close all Windows programs.
  • Page 204 LAN Configuration Automatic configuration with Bootp 11 Files load; when finished, the BootP Settings screen appears. Figure 32 BootP Settings screen 12 In the Default Settings part of the screen, if known, you can enter the subnet mask and gateway. Defaults can be used: •...

  • Page 205: Two Methods To Determine The Mac Address

    LAN Configuration Automatic configuration with Bootp Two Methods to Determine the MAC Address Enabling logging to discover the MAC address using BootP If you want to see the MAC address, select the Do you want to log BootP requests? check box. 1 Open BootP Settings from Start >...

  • Page 206: Assigning Ip Addresses Using The Agilent Bootp Service

    LAN Configuration Automatic configuration with Bootp Determining the MAC address directly from the LAN Interface card label 1 Turn off the instrument. 2 Read the MAC address from the label and record it. The MAC address is printed on a label on the rear of the module. 3 Read the MAC address from the label and record it.
  • Page 207 LAN Configuration Automatic configuration with Bootp 4 The Error means the MAC address has not been assigned an IP address and the Tab File does not have this entry. The MAC address is saved to the Tab File when an IP address is assigned. 5 Close the log file before turning on another instrument.
  • Page 208 LAN Configuration Automatic configuration with Bootp 5 Make these entries for the instrument: • MAC address • Host name, Enter a Hostname of your choice. The Host Name must begin with "alpha" characters (i.e. LC1260) • IP address • Comment (optional) •...

  • Page 209: Changing The Ip Address Of An Instrument Using The Agilent Bootp Service

    LAN Configuration Automatic configuration with Bootp Changing the IP Address of an Instrument Using the Agilent BootP Service Agilent BootP Service starts automatically when your PC reboots. To change Agilent BootP Service settings, you must stop the service, make the changes, and then restart the service.
  • Page 210 LAN Configuration Automatic configuration with Bootp 3 Press Edit BootP Addresses… to edit the Tab File. Figure 36 Edit BootP Adresses screen 4 In the Edit BootP Addresses... screen press Add... to create a new entry or select an existing line from the table and press Modify... or Delete to change the IP address, comment, subnet mask, for example, in the Tab File.

  • Page 211: Manual Configuration

    LAN Configuration Manual Configuration Manual Configuration Manual configuration only alters the set of parameters stored in the non- volatile memory of the module. It never affects the currently active parameters. Therefore, manual configuration can be done at any time. A power cycle is mandatory to make the stored parameters become the active parameters, given that the initialization mode selection switches are allowing it.

  • Page 212: With Telnet

    LAN Configuration Manual Configuration With Telnet Whenever a TCP/IP connection to the module is possible (TCP/IP parameters set by any method), the parameters may be altered by opening a Telnet session. 1 Open the system (DOS) prompt window by clicking on Windows START button and select “Run...”.
  • Page 213 LAN Configuration Manual Configuration 3 Type ? and press enter to see the available commands. Figure 40 Telnet Commands Table 16 Telnet Commands Value Description displays syntax and descriptions of commands displays current LAN settings ip <x.x.x.x> sets new ip address sm <x.x.x.x>...
  • Page 214 LAN Configuration Manual Configuration information about the LAN interface MAC address, initialization mode Initialization mode is Using Stored active TCP/IP settings TCP/IP status - here ready connected to PC with controller software (e.g. Agilent ChemStation), here not connected Figure 41 Telnet - Current settings in "Using Stored"...
  • Page 215 LAN Configuration Manual Configuration 7 When you have finished typing the configuration parameters, type exit and press Enter to exit with storing parameters. Figure 43 Closing the Telnet Session If the Initialization Mode Switch is changed now to “Using Stored” mode, the instrument N O T E will take the stored settings when the module is re-booted.

  • Page 216: Pc And User Interface Software Setup Setup

    LAN Configuration PC and User Interface Software Setup Setup PC and User Interface Software Setup Setup PC Setup for Local Configuration This procedure describes the change of the TCP/IP settings on your PC to match the module’s default parameters in a local configuration (see also “Initialization Mode Selection”...

  • Page 217: User Interface Software Setup

    LAN Configuration PC and User Interface Software Setup Setup User Interface Software Setup Install you user interface software according the provided User Interface Software Setup Guide. Agilent 1290 Infinity II Flexible Pump User Manual...
  • Page 218 LAN Configuration PC and User Interface Software Setup Setup Agilent 1290 Infinity II Flexible Pump User Manual...

  • Page 219: Appendix

    Do Not Remove the Instrument Cover Do Not Modify the Instrument In Case of Damage Solvents Safety Symbols Waste Electrical and Electronic Equipment Directive Radio Interference Sound Emission Agilent Technologies on Internet This chapter provides additional information on safety, legal and web. Agilent Technologies...

  • Page 220: General Safety Information

    Agilent Technologies assumes no liability for the customer’s failure to comply with these requirements. Ensure the proper usage of the equipment.

  • Page 221: Before Applying Power

    Verify that the voltage range and frequency of your power distribution matches to the power specification of the individual instrument. ➔ Never use cables other than the ones supplied by Agilent Technologies to ensure proper functionality and compliance with safety or EMC regulations. ➔...

  • Page 222: Do Not Operate In An Explosive Atmosphere

    Appendix General Safety Information Do Not Operate in an Explosive Atmosphere Presence of flammable gases or fumes WA R N I N G Explosion hazard ➔ Do not operate the instrument in the presence of flammable gases or fumes. Do Not Remove the Instrument Cover Instrument covers removed WA R N I N G Electrical shock...

  • Page 223: Solvents

    Appendix General Safety Information Solvents Toxic, flammable and hazardous solvents, samples and reagents WA R N I N G The handling of solvents, samples and reagents can hold health and safety risks. ➔ When working with these substances observe appropriate safety procedures (for example by wearing goggles, safety gloves and protective clothing) as described in the material handling and safety data sheet supplied by the vendor, and follow good laboratory practice.

  • Page 224: Safety Symbols

    Appendix General Safety Information Safety Symbols Table 17 Symbols The apparatus is marked with this symbol when the user should refer to the instruction manual in order to protect risk of harm to the operator and to protect the apparatus against damage. Indicates dangerous voltages.
  • Page 225 Appendix General Safety Information Table 17 Symbols Pacemaker Magnets could affect the functioning of pacemakers and implanted heart defibrillators. A pacemaker could switch into test mode and cause illness. A heart defibrillator may stop working. If you wear these devices keep at least 55 mm distance to magnets.

  • Page 226: Waste Electrical And Electronic Equipment Directive

    Appendix Waste Electrical and Electronic Equipment Directive Waste Electrical and Electronic Equipment Directive Abstract The Waste Electrical and Electronic Equipment (WEEE) Directive (2002/96/EC), adopted by EU Commission on 13 February 2003, is introducing producer responsibility on all electric and electronic appliances starting with 13 August 2005.

  • Page 227: Radio Interference

    Appendix Radio Interference Radio Interference Cables supplied by Agilent Technologies are screened to provide optimized protection against radio interference. All cables are in compliance with safety or EMC regulations. Test and Measurement If test and measurement equipment is operated with unscreened cables, or...

  • Page 228: Sound Emission

    Appendix Sound Emission Sound Emission Manufacturer’s Declaration This statement is provided to comply with the requirements of the German Sound Emission Directive of 18 January 1991. This product has a sound pressure emission (at the operator position) < 70 dB. •...

  • Page 229: Agilent Technologies On Internet

    Appendix Agilent Technologies on Internet Agilent Technologies on Internet For the latest information on products and services visit our worldwide web site on the Internet at: http://www.agilent.com Agilent 1290 Infinity II Flexible Pump User Manual...
  • Page 230 Index Index install remove 8-bit configuration switch cable drive current too high on-board LAN drive current too low drive encoder error overview drive encoder failed RS-232 Agilent Lab Advisor software drive phases differ too much in electric cables Agilent Lab Advisor resistance analog Agilent...
  • Page 231 Index insufficient power of drive encoder valve hardware overcurrent (MCGV) release if stuck replace leak sensor open waste counter limit exceeded stuck leak sensor short writing the multi purpose valve tag inlet weaver failed leak replace writing the pump encoder tag lost CAN partner inline filter failed...
  • Page 232 Index manual configuration disassemble PC and User Interface Software parts non-operating altitude Setup product description non-operating temperature TCP/IP parameter configuration pump drive blocked or encoder failed using default pump drive encoder defect using stored pump drive encoder error leak sensor open operating Altitude pump drive encoder rollover leak sensor short...
  • Page 233 Index inlet valve specifications inlet weaver performance wash seal MCGV replace multi channel gradient valve waste counter limit exceeded multi purpose valve target pressure not reached for quaternary waste outlet valve pump degasser electrical and electronic pressure sensor TCP/IP parameter configuration equipment seal wash pump telnet...
  • Page 234 • using and optimizing, • troubleshooting and diagnostic, • error information, • test functions, • maintenance, • parts identification, • hardware information, • safety and related information. © Agilent Technologies 2014 Printed in Germany 12/2014 *G7104-90000* *G7104-90000* G7104-90000 Rev. B Agilent Technologies...

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