Thermo Scientific 108004-00 Manuals

Manuals and User Guides for Thermo Scientific 108004-00. We have 1 Thermo Scientific 108004-00 manual available for free PDF download: Instruction Manual

Thermo Scientific 108004-00 Instruction Manual

Thermo Scientific 108004-00 Instruction Manual (254 pages)

Brand: Thermo Scientific | Category: Laboratory Equipment | Size: 12 MB

Table of Contents

Table of Contents
11
Chapter 1 Introduction

23
- Figure 1-1. Omni FTIR Multi Gas CEMS
  24
- System Overview
  25
- Figure 1-2. Omni FTIR Multi Gas CEMS System Overview
  25
- Sample Probe
  26
- Sample Line
  26
- Temperature Controller
  26
- Sample Conditioning
  26
- Ftir
  26
- Data Logger
  27
- Data Communications
  28
- Typical System Flow
  28
- System Power Distribution
  28
- Specifications
  28
- Measuring Components with Minimum Measuring Range and Required MDL
  29
- Performance
  29
- Table 1-1. FTIR Compounds
  29
- Table 1-2. FTIR Performance Specifications
  29
- Connections
  30
- Power Requirements
  30
- Pneumatics
  31
- Cabinet
  31
- Other Manuals
  32
Chapter 2 System Installation, Start up and Shut down

33
- Unpacking and Inspection
  33
- Site Requirements
  34
- Ambient Temperature Instrument Air
  34
- Power Requirements
  34
- Rack Dimensions
  34
- Weight
  34
- Flange Requirements
  34
- Remove Shipping Restraint
  34
- Installing the FTIR Analyzer into the Rack
  35
- Figure 2-1. Removing the Shipping Screws
  35
- Figure 2-2. Analyzer Installation
  36
- Figure 2-3. Purge and Power Connections
  37
- Connect the Purge Lines to the FTIR
  38
- Connect the Power to the FTIR
  38
- Figure 2-4. Connecting to the FTIR Unit
  38
- Connecting the Computer Cable to the FTIR
  39
- Connect the Pressure Transducer Cable to the FTIR
  39
- Connect the Cell Heater Cable to the FTIR
  39
- Connect Sample Lines to the Heated Pump/Valve Assembly
  39
- Hydrator
  39
- External System Connections
  40
- Connect the Sample Line to the FTIR Analyzer Cabinet and Heated Sample Box
  40
- Figure 2-5. Rear Panel Terminal Blocks
  40
- Instrument Air
  41
- Exhaust Line
  41
- Calibration Gases
  41
- Communications
  41
- Ethernet
  41
- Serial
  41
- Analog
  42
- Digital
  42
- System Startup
  42
- Turn Power on
  42
- Adjust/Confirm Flow and Heat Settings
  43
- Air Flow
  43
- Figure 2-6. Pneumatic Panel Rear View
  43
- Heat
  44
- Imacc
  44
- Autostart
  44
- Maintenance Switch
  45
- System Shut down
  46
- Operation
  47
- Software Description
  47
- Imacc FTIR Software Suite (IFSS)
  48
- Monitor
  48
- Figure 3-1. Component Relational Diagram
  48
- Concentrations Pane
  50
- Processstatus
  51
- Concentrationplot/Spectrum Plot
  52
- Display Tab
  52
- Timespan Tab
  53
- Datasource Tab
  54
- Data Files
  54
- Remote Control
  56
- Server
  56
- Script Engine
  56
- Omnic
  57
- Result
  59
- Ni-Daq
  59
- Calgrafix
  59
- CDM-USB Driver
  59
- Data Server Software
  59
- Imacccurrentloop
  59
- Configure
  60
- Analog Output Board
  61
- Table 3-1. Analog Current Channel Assignments
  61
Chapter 4 Calibration

65
Chapter 5 Preventive Maintenance and Servicing

85
Chapter 7 System Component Description

192
- Sample Probe
  192
- Figure 7-1. FTIR Multi Gas CEMS System Component Layout
  192
- Temperature Controller
  193
- Heated Sample Line
  193
- Figure 7-2. Sample Probe
  193
- Heated Pump/Valve Assembly
  194
- Hydrator
  194
- Pneumatic Panel
  194
- Sample Mode
  195
- Blowback
  195
- Instrument Background Scan and Flowback
  195
- Figure 7-3. Pneumatic Panel
  195
- Check Zero
  196
- Check Spike
  196
- Check Span
  196
- Figure 7-4. Sample and Calibration Gas Flow Diagram
  196
- Ftir
  197
- Figure 7-5. FTIR Analyzer
  197
- Figure 7-6. FTIR Flow Schematic
  198
- Optical Components
  199
- Source
  199
- Figure 7-7. Spectrometer Compartment
  199
- Interferometer
  200
- Laser
  200
- Mirrors
  200
- Aperture
  200
- Detector
  201
- Gas Cell
  201
- Gas Cell Heating Jacket
  201
- Figure 7-8. Major System Components
  201
- Temperature Sensor
  202
- Pressure Sensor
  202
- Gas Cell Interface
  202
- Computer Interface
  202
- Humidity Control
  202
- Air Purifier
  202
- Industrial PC
  203
- Figure 7-9. FTIR Purge Gas Generator
  203
- Figure 7-10. FTIR PC
  203
- I/O Boards
  204
- Console
  204
- Datalogger
  204
- Electrical Panel Assembly
  204
- AC Power Input
  205
- Figure 7-11. Electrical Panel
  205
- Figure 7-12. AC Mains
  205
Appendix A Warranty

207
Appendix B Modbus Protocol

209
- Serial Communication Parameters
  209
- TCP Communication Parameters
  209
- Application Data Unit Definition
  210
- Slave Address
  210
- MBAP Header
  210
- Function Code
  211
- Data
  211
- Error Check
  211
- Function Codes
  211
- (0X03) Read Holding Registers
  211
- Modbus Parameters Supported
  213
- Table B-1. Modbus Read Registers
  213
- Table B-2. Modbus Write Registers
  214
- Table B-3. System Command Values
  214
- Table B-4. System Flag Bits
  215
Appendix C Interfacing a DCS/PLC with the Omni FTIR Multi Gas CEMS

217
- Introduction
  217
- Connecting a DCS/PLC to the Omni FTIR Multi Gas CEMS
  218
- Figure C-1. Rear Panel Terminal Connectors
  218
- Establishing Communications
  219
- Analog Outputs
  219
- Table C-1. Analog Output Connections
  219
- Digital I/O
  220
- Figure C-2. Analog Outputs
  220
- Figure C-3. Digital I/O - Rear Panel Terminals
  221
- Table C-2. Digital I/O Connections
  221
- Solid-State Relays (SSR
  222
- SSR Rail
  222
- Figure C-4. SSR Rail
  222
- Figure C-5. SSR Indicator Light Configurations
  222
Appendix D Calogix Setup

223
- Hardware Description
  223
- Figure D-1. Base Unit and Four Controllers
  223
- Finding the Correct COM Port
  224
- Figure D-2. Temperature Controller Connection
  224
- Setting the Virtual COM Port
  226
- Programming the Controllers and Setting Parameters
  228
- Creating Ramp Programs
  229
- Inputting Controller Values
  231
- Table D-1. Controller Values
  232
Appendix Eimacc Script Setting

235
- Cems_Samplemode
  235
- Modbus Control Version
  244
Appendix F Concentration Data Transfer Using a Web Server

251

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