Teledyne CombiFlash EZ Prep Manuals

Manuals and User Guides for Teledyne CombiFlash EZ Prep. We have 1 Teledyne CombiFlash EZ Prep manual available for free PDF download: User Manual

Teledyne CombiFlash EZ Prep User Manual

Teledyne CombiFlash EZ Prep User Manual (245 pages)

Brand: Teledyne | Category: Laboratory Equipment | Size: 3.4 MB

Table of Contents

Table of Contents
3
1 Introduction

9
- Documentation Overview
  9
- Product Overview
  9
- Operating Overview
  16
  - Multiple Control Possibilities
    16
  - File Storage
    16
  - Specifications
    17
  - Controls, Indicators, and Features of the Combiflash Rf
    26
  - Safety
    33
    
    Hazard Severity Levels
    34
    
    Hazard Symbols
    34
  - For Additional Information
    36
2 Preparation

37
- Rf + , Rf + Lumen, Rf+ Purion, and EZ Prep Systems
  37
- Unpacking the Unit
  37
- Instrument Location
  39
- Connect Power
  39
- Connect Solvent Lines (Excludes EZ Prep)
  40
- Connect Waste Lines (Excludes EZ Prep)
  42
- EZ Prep Plumbing Connections
  45
- External Gas
  46
  - Combiflash Rf , Rf Lumen, and EZ Prep
    46
  - Combiflash Rf
    47
  - Lumen or EZ Prep with ELSD
    47
  - Connect and Route Drain Lines
    47
    
    Only
    47
  - Position the System
    50
- Install Collection Tube Racks
  51
- External Detector (Optional)
  53
- Turn on Power
  54
- Configure the System
  54
  - Solvents
    54
  - Enable Automatic Phase Change (EZ Prep Only)
    55
  - General Settings
    56
  - Set Date/Time
    56
  - Vapor Limit
    56
  - Set Default Tube Volumes
    57
  - User Preferences
    57
  - Prep HPLC Tab
    60
  - Restart the System
    61
- Prime the Solvent Lines
  62
- System Verification
  63
- Installation Qualification Checklist
  64
3 Preparation: Rf 150 Systems

66
- Unpacking the Unit
  66
- Instrument Location
  68
- Connect Power
  68
- Connect Solvent Lines
  69
- Connect Waste Lines
  71
- Connect and Route Drain Lines
  72
- Position the System
  74
- Install Collection Tube Racks
  75
- Turn on Power
  77
- Configure the System
  77
  - Solvents
    78
  - General Settings
    78
  - Set Date/Time
    78
  - Vapor Limit (Optional)
    78
  - Set Default Tube Volumes
    79
  - User Preferences
    79
  - Restart the System
    82
- Prime the Solvent Lines
  83
- System Verification
  83
- Installation Qualification Checklist
  84
4 Preparation: Optional 4X Module

86
- Unpacking the Unit
  86
- Instrument Location
  87
- Connect Power
  87
- Connect Solvent Lines
  88
  - Connecting the Combiflash Rf with 4X Module
    88
  - And Purion
    89
  - Connect Waste Lines
    90
  - Control Connection
    98
  - Position the System
    98
  - Remove Shipping Hardware
    98
  - Turn on Power
    99
- Prime the Solvent Lines
  100
- System Verification
  101
- Installation Qualification Checklist
  102
5 Operation

104
- Flash Sample Preparation
  104
  - Liquid Sample Injection
    104
  - Solid Samples
    104
  - Pre-Loading on Column
    108
  - Loading a Redisep Rf Column
    108
  - Start a Default Method
    109
  - During the Run
    113
    
    Run Control Buttons
    113
    
    Bypassing the Solid Load Cartridge
    116
    
    About Solvent Level Detection
    117
  - EZ Prep Operation
    119
    
    Column Mounting
    119
    
    Sample Preparation
    120
    
    Starting the Separation
    121
6 User Help Reference

122
- Peaktrak Window Elements
  122
- Method File
  123
- Run File
  124
- How to Get Peaktrak Help
  124
- File
  124
- Method Editor
  128
- Tools
  129
- Help
  131
- Main Window
  132
- Method Editor
  138
- Gradient Optimizer
  146
- Column Data
  146
- Batch
  147
- Files
  148
- Set Data Path
  149
- MS Method Development
  150
- MS Manual Control
  152
- Ionization Settings
  152
- Auto Prime/Valve Wash
  155
- Manual Control
  155
- Configuration
  157
- Set Administrator Password
  162
- User Management
  162
- Calibrate Touchscreen
  163
  - Starting a Run Using Default Settings
    164
  - Editing a Method
    167
  - Alternative Ways to Create Method Files
    173
  - Editing a Default Method
    174
  - Defining a Gradient
    175
  - Real-Time Gradient Editing
    175
  - Bypassing the Solid Load Cartridge
    176
  - Bypassing the Injection Loop
    177
  - Monitoring the Purity Measure
    178
  - Viewing Runs
    179
  - Manual Control of the Combiflash Rf
    182
  - Setting the Vapor Limit
    183
7 Remote Interfaces

186
- Network Configuration
  186
  - Network PC Access
    187
  - Network Printing
    188
  - Network File Save Configuration
    188
  - Apple Mobile Digital Devices
    189
  - Install and Configure the Peaktrak App
    189
- Direct Connection
  189
  - Windows 7 Settings
    190
  - Windows Vista Settings
    192
  - Windows XP Settings
    194
  - Windows 2000 Settings
    196
  - Completing the Direct Connection
    198
- Direct Printing
  198
8 Maintenance

200
- System Standby and Shut down
  200
- Preventive Maintenance
  201
- Cleaning
  201
  - Collection Rack and Tray Cleaning
    203
- Tubing Inspection
  203
- Flow Cell Cleaning
  205
  - Post Separation
    205
  - Quick Cleaning When Recommended
    206
  - Monthly Flow Cell Cleaning
    210
- Purion Maintenance
  210
  - Removing ESI Probe
    210
  - ESI Probe Replacement
    211
  - APCI Probe Removal
    212
  - APCI Probe Replacement
    213
  - Removal of Ion Source Housing
    213
    
    ESI and APCI Replacement from Purion S and Purion L
    214
    
    Cleaning the Ionization Source Capillary
    214
    
    Replacement of Ion Source Housing
    215
    
    Overpressure Error
    215
    
    Check Valve Cleaning
    216
    
    Replacing Check Valves
    217
  - Injection Valve Maintenance
    218
  - Electrical Troubleshooting
    218

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