Thermo Scientific dionex ic pure water Operating Instructions Manual
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Thermo Scientific dionex ic pure water Operating Instructions Manual

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Thermo Scientific
Dionex IC Pure
Water Purification
System
June 2016
50133369
Revision C

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Summary of Contents for Thermo Scientific dionex ic pure water

  • Page 1 Thermo Scientific Dionex IC Pure Water Purification System June 2016 50133369 Revision C...
  • Page 2 © 2016 Thermo Fisher Scientific Inc. All rights reserved. Thermo Fisher Scientific Inc. provides this document to its customers with a product purchase to use in the product operation. This document is copyright protected and any reproduction of the whole or any part of this document is strictly prohibited, except with the written authorization of Thermo Fisher Scientific Inc.

  • Page 3: Preface

    This document is not part of any sales contract between Thermo Fisher Scientific Inc. and a purchaser. This document shall in no way govern or modify any Terms and Conditions of Sale, which Terms and Conditions of Sale shall govern all conflicting information between the two documents. Thermo Scientific Dionex IC Pure system | iii...

  • Page 4: Legal Information

    Please consult your local sales representative for details. Warranty Thermo Electron LED GmbH warrants the operational safety and functions of the Thermo Scientific™ Dionex™ IC Pure™ Water Purification System only under the condition that: The unit is installed and operated as per the operation manual. Do not use this product for ...

  • Page 5: Explanatory Notes On The Operating Instructions

    Indicates a situation in which protective gloves or clothing must be worn. Indicates a situation in which protective goggles must be worn. Indicates a situation in which breathing protection must be used. Thermo Scientific Dionex IC Pure system | v...
  • Page 6 Additionally, the ultrapure water system is in compliance with many other international standards, regulations and directives not listed here. Should you have any questions regarding compliance with national standards, regulations and directives applicable for your country, please contact your Thermo Fisher Scientific sales organization. Dionex IC Pure system Thermo Scientific...

  • Page 7: Table Of Contents

    Table of Contents Preface............. iii Legal Information .
  • Page 8 Schematic illustration with connected suppressor ....... . 46 Dionex Integrion and Dionex ICS-2100 system ........46 Dionex ICS-4000 system.
  • Page 9 Table of Contents OEM menu ..............72 Accessing the OEM menu .

  • Page 11: Chapter 1 Transport And Packaging

    Transport and packaging Content “Examination on receipt” on page 2  “Complaints” on page 2  “Packing for return shipment” on page 2  Thermo Scientific Dionex IC Pure system | 1...

  • Page 12: Examination On Receipt

    Save the complete packaging, including the cardboard box, for a possible inspection of them  and/or return shipment of the system. Packing for return shipment If possible, use the original box and packaging material. When these are no longer available, then: Dionex IC Pure system Thermo Scientific...
  • Page 13 Prior to sending back an operated device, empty the water, dry the system and take out the  ultrapure cartridges. Plug and wrap the emptied ultrapure cartridges with a bubble wrap. Return the cartridges  together with the Dionex IC Pure system. Thermo Scientific Dionex IC Pure system | 3...
  • Page 14 Chapter 1 | Transport and packaging Dionex IC Pure system Thermo Scientific...

  • Page 15: Chapter 2 Safety Precautions

    A grounded 100-240 VAC, 50/60 Hz socket must be available (see “Electrical connections for  Dionex IC Pure system and external 20 L tank” on page 16). Access to the power supply cord and plug should never be restricted or obstructed.  Thermo Scientific Dionex IC Pure system | 5...
  • Page 16 CAUTION To avoid the risk of pinching, crushing, cutting or electrical shock, never perform maintenance on the unit without its protective housing, or while it is in operation. Maintenance work on the unit may only be performed by trained, authorized specialists. Dionex IC Pure system Thermo Scientific...
  • Page 17 Proceed as follows when the unit has a defect:  Switch the system off and unplug the unit from power outlet.  Shut off the supply of feedwater.  Contact your local service organization.  Thermo Scientific Dionex IC Pure system | 7...
  • Page 18 Chapter 2 | Safety precautions Dionex IC Pure system Thermo Scientific...

  • Page 19: Chapter 3 Scope Of Delivery

    The following items are included with the Dionex IC Pure system: 1 x Dionex IC Pure system Item No.: 50132810 1 x Filter set for Dionex IC Pure system Item No.: 09.1006 including 1 x Assembly kit Item No.: 50133371 consisting of: Thermo Scientific Dionex IC Pure system | 9...
  • Page 20 Drain piece with tubing o.d. 8 mm (0.31 in) Dionex IC Pure system 50146268 PVDF- precision metering valve 1/8“ tube 50147490 Disinfection Adapter 50133431 Jumper cable 50145876 Control cable for 20 L tank with and without level control 50143964 Dionex IC Pure system Thermo Scientific...

  • Page 21: Chapter 4 Intended Use Of The Device

    The system must not be operated outside of the specifications as described in the operating manual. In particular, the system may not be used for production of drinking water and drug manufacturing. The system must not be used as a medical device and outside of laboratories. Thermo Scientific IC Pure | 11...
  • Page 22 Chapter 4 | Intended use of the device IC Pure Thermo Scientific...

  • Page 23: Chapter 5 Technical Specifications

    +2 - +35 °C (35.6 to 95 °F) Pressure for 1.45 - 58 psi (at a pressure > -- (not applicable) automatic filling 58 psi a pressure reducer must be installed upstream of the unit. Thermo Scientific Dionex IC Pure system | 13...
  • Page 24 485 mm (19.09 in) Base area (height x width) 340 x 483 mm (13.39 x 7.48 in) Weight of tank and filling station 7 kg (18.07 lb) Weight with full tank 27 kg (60 lb) Dionex IC Pure system Thermo Scientific...
  • Page 25 Rinse water tubing 8 mm (0.31 in) o.d. Connection to pump IC 30 psi 8 mm (0.31 in) o.d. on 1/8“coupling Connection to pump IC 3 psi 8 mm (0.31 in) o.d. on 1/8“coupling Thermo Scientific Dionex IC Pure system | 15...
  • Page 26 300 mm (11.81 in) the unit Space to the back of the unit at least 200 mm (7.87 in) Top space at least 400 mm (15.75 in) Space to front of unit Free accessibility Dionex IC Pure system Thermo Scientific...
  • Page 27 II of IEC 60364-4-443. Ventilation no special requirements no special requirements requirements Degree of pol- lution Airborne sound emission Sound pressure level 49 db(A) Thermo Scientific Dionex IC Pure system | 17...
  • Page 28 Chapter 5 | Technical specifications Dionex IC Pure system Thermo Scientific...

  • Page 29: Chapter 6 The Installation Area

    2.48 inch (DN 50 pipe). Should no such drain be available it is recommended to install a water watcher (only for European specification). Otherwise the manufacturer will not accept liability for any possible water damage. Thermo Scientific Dionex IC Pure system | 19...
  • Page 30 Ample working space must be provided around the unit for easy replacement of parts and for  ease of operation (see “Accessibility to Dionex IC Pure system and external 20 L tank” on page 16). Easy access for operation and control of the system.  Dionex IC Pure system Thermo Scientific...

  • Page 31: Chapter 7 Installation

    , Dionex ICS-5000 and  Dionex ICS-3000 system” on page 40 “Connecting the Suppressor to the Dionex IC Pure system”  “Calibrate suppressor regenerant water flow rate”  “Schematic illustration with connected suppressor”  Thermo Scientific Dionex IC Pure system | 21...

  • Page 32: Connections Of The Dionex Ic Pure System

    A = 4 pin for ion chromatogram, B= 5 pin for tube jumper, C= 6 pin for level switch for  external tank. 5. Voltage supply connector for 24V DC 6. Quick coupling connector for “to pump“ and “to suppressor“ o.d. 8 mm (0.31 in) tube Dionex IC Pure system Thermo Scientific...

  • Page 33: Connections External 20 L Tank

    11. Quick coupling connector for outlet o.d. 8 mm (0.31 in) tube - water supply from 20 L external tank to IC Pure system 12. 1/4“ thread connection for sterile vent filter Thermo Scientific Dionex IC Pure system | 23...
  • Page 34 Lift the unit and hang the back of it on the wall-mounting brackets. CAUTION Always lift and carry the unit in tandem (two people), never alone. Lift the unit at the two bottom corners. 190 mm (7.48 in) 95 mm (3.74 in) Dionex IC Pure system Thermo Scientific...

  • Page 35: Setting Up Ic Pure System

    Note Cartridge serial number will need to be entered in the system after power is applied. (see“Changing the ultrapure cartridge” ) Thermo Scientific Dionex IC Pure system | 25...
  • Page 36 CAUTION When using the unit without a pretreatment cartridge, only feedwater that 5 L tank has been pretreated by reverse osmosis, ion exchange or distillation is to be used. Dionex IC Pure system Thermo Scientific...
  • Page 37 On/Off button for the additional tank indicator. Screw the sterile filter supplied with the unit into the 1/4“ thread of the sampling tap. 1/4“ thread Sterile filter Thermo Scientific Dionex IC Pure system | 27...

  • Page 38: Connecting Of A Pretreatment Cartridge (Optional)

    CAUTION When using a pretreatment cartridge, the initial pressure at the connections for the IC unit must be reset. Contact the Service department at Thermo Scientific for this. Always ensure that the internal 5 L or external 20 L tank does not drain completely, as this may damage or render the optional pretreatment cartridge unusable.
  • Page 39 Attach the o.d. 8 mm (0.31 in) tube into the right connections connection of the external 20 L tank for tank overflow and route the tube with a downward slope to the drain. 20 L tank connection for tank overflow Thermo Scientific Dionex IC Pure system | 29...

  • Page 40: Connecting The External 20 L Tank With Level Control (Optional)

    If you are using a pretreatment cartridge in the Dionex IC Pure system, connect the external 20 L tank with level control to a potable water supply. Additionally, route the concentrate line directly to an atmospherically vented drain. Dionex IC Pure system Thermo Scientific...
  • Page 41 Wet end of the tube with water and insert the o.d. 8 mm (0.31 in) tube into the right connection of the external 20 L tank with level control for tank overflow. Tank Feedwater inlet/ overflow Concentrate Thermo Scientific Dionex IC Pure system | 31...
  • Page 42 Note This additional tank indicator has already been control cable calibrated at the factory. If recalibration is required refer to “Recalibration of the tank sensor for an additional tank indicator” . Additional tank indicator Dionex IC Pure system Thermo Scientific...

  • Page 43: Illustration Of Drain

    Minimum distance tubes must be located at least 20 mm (0.75 in) above 20 mm/ 0.75 inch the drain. Attach the tubes in such a manner that they remain in their position. Drain Thermo Scientific Dionex IC Pure system | 33...

  • Page 44: Mounting Of The Power Pack (Voltage Supply)

    Universal holder Universal foil Universal adapter Mains adapter Attach universal adapter to a smooth wall surface with Universal adapter supplied screws or with glue (not provided). Wall surface Dionex IC Pure system Thermo Scientific...
  • Page 45 Switch the unit on and enter the serial number of the ultrapure cartridge in the control menu (“Changing the ultrapure cartridge” ).The unit is ready for use now. Thermo Scientific Dionex IC Pure system | 35...

  • Page 46: Connecting The Control Cable From The Ic Pure System To A Dionex Integrion And Dionex Ics-2100, Dionex Ics-4000, Dionex Ics- 5000+, Dionex Ics-5000 Or Dionex Ics-3000 System

    Set up an additional ion chromatograph to the IC Pure system as shown on page 42 - 43 1 - 5 Set up of Suppressor to IC Pure system as shown on page 4 1 - 8 Dionex IC Pure system Thermo Scientific...
  • Page 47 Back side Dionex Integrion and Dionex ICS-2100/ Dionex ICS-4000 system and connect this to the back of the Dionex ICS-5000 Dionex ICS-5000 or Dionex ICS-3000 system. In this case you must then make the settings for the Thermo Scientific Dionex Chromeleon Chromatography Data System (CDS) Software, 'Relay_2'.(refer to step 8, page 39)

  • Page 48: Ics-5000 Or Dionex Ics-3000 System

    The other end of the 1/8“ tube is connecting to the “Degas in“ connection from the Degas module on the Dionex Integrion and Dionex ICS-2100, Dionex ICS-4000, Dionex ICS-5000 Dionex ICS-5000 or Dionex ICS-3000 system. (see “Schematic illustration with connected suppressor” ) Union nut Dionex IC Pure system Thermo Scientific...
  • Page 49 Dionex ICS-2100“ or “Dionex ICS-4000 system“ and right-click on the entry you need. Note If you are using an Dionex ICS-5000 , Dionex ICS-5000 or Dionex ICS-3000 system you must go to the tab 'Relays' under the pump settings. Thermo Scientific Dionex IC Pure system | 39...
  • Page 50 Save your settings and exit the configuration settings. The Dionex Integrion and Dionex ICS-2100, Dionex ICS-4000, Dionex ICS-5000 Dionex ICS-5000 or Dionex ICS-3000 system will then pump pure water from the Dionex IC Pure system. Dionex IC Pure system Thermo Scientific...

  • Page 51: Sample Chromeleon Cds Software Settings For Dionex Ics-2100, Dionex Ics-4000 System

    Installation | Chapter 7 Sample Chromeleon CDS Software settings for Dionex ICS-2100, Dionex ICS-4000 system Dionex ICS-4000 system Thermo Scientific Dionex IC Pure system | 41...

  • Page 52: Sample Chromeleon Cds Software Settings For Dionex Ics-5000 Dionex Ics-5000 And Dionex Ics-3000 System

    Action Figure Switch off the Dionex IC Pure system and stop pumping of pure water for the IC system using the Chromeleon CDS software. Take the T piece and unscrew all three union nuts. Dionex IC Pure system Thermo Scientific...

  • Page 53: Connecting The Suppressor To The Dionex Ic Pure System

    Reducing adapter Union nut Note Ensure that the cutting ring and taper coupling that fit inside the union nut are not lost when you unscrew the union nut. Thermo Scientific Dionex IC Pure system | 43...
  • Page 54 This tube is suppressor” connecting to the „“Regen In“ connection of the suppressor from the Dionex Integrion and Dionex ICS-2100, Dionex ICS-4000, Dionex ICS-5000 , Dionex ICS-5000 or Dionex ICS-3000 system. Dionex IC Pure system Thermo Scientific...
  • Page 55 Note If external water regeneration mode will not be used, the suppressor supply connection must be closed off. Therefore, disconnect the reducing adapter from the ‘to Suppressor‘ connection on the Dionex IC Pure system. Thermo Scientific Dionex IC Pure system | 45...

  • Page 56: Schematic Illustration With Connected Suppressor

    Chapter 7 Installation Schematic illustration with connected suppressor Dionex Integrion and Dionex ICS-2100 system Dionex IC Pure system Thermo Scientific...
  • Page 57 Installation | Chapter 7 Thermo Scientific Dionex IC Pure system | 47...

  • Page 58: Dionex Ics-4000 System

    Chapter 7 Installation Dionex ICS-4000 system Dionex IC Pure system Thermo Scientific...
  • Page 59 Installation | Chapter 7 Thermo Scientific Dionex IC Pure system | 49...

  • Page 60: Dionex Ics-5000+ System

    Chapter 7 Installation Dionex ICS-5000 system Dionex IC Pure system Thermo Scientific...
  • Page 61 Installation | Chapter 7 Thermo Scientific Dionex IC Pure system | 51...
  • Page 62 Chapter 7 Installation Dionex IC Pure system Thermo Scientific...

  • Page 63: Chapter 8 Flow Chart

    Dionex IC Pure system with 5 L tank Pure water ASTM Type II Drain Dionex IC Pure system with pretreatment and 20 L tank Ultrapure water ASTM Type I Tap water Drain Thermo Scientific Dionex IC Pure system | 53...
  • Page 64 S1 Sterile overflow (optional) LIS 103 Float switch (optional) P1 Pressure pump UV1 UV lamp QIA 300 Feedwater conductivity measuring cell QIA 301/TIA500 Ultrapure water conductivity measuring cell + Temperature sensor QI 302 TOC conductivity measuring cell Dionex IC Pure system Thermo Scientific...

  • Page 65: Chapter 9 Functional Description

    0.2 µm final filter and 2. automatic dispensing from two points on Dionex IC Pure system to an external IC system. The unit is designed such that water can be taken from both sampling points simultaneously. Thermo Scientific Dionex IC Pure system | 55...

  • Page 66: Dionex Ic Pure System With External 20 L Tank And Level Control (Optional)

    1. manually through main dispenser and 0.2 µm final filter and 2. automatic dispensing from two points on Dionex IC Pure system to an external IC system. The unit is designed such that water can be taken from both sampling points simultaneously. Dionex IC Pure system Thermo Scientific...

  • Page 67: Chapter 10 Initial Start Up

    Initial start up Content “Putting the system into operation” on page 58  “Dispensing water from the Dispensing valve” on page 59  “Venting the 0.2 µm final filter” on page 59  Thermo Scientific Dionex IC Pure system | 57...

  • Page 68: Putting The System Into Operation

    Use this 'NONSTOP'-key to switch the system to the “Nonstop“ operating mode. When the unit has successfully reached the pure water value specified, return the unit to the “Interval“ mode automatically or by pressing the “INTERVAL“ button while it is in the “Nonstop“ mode. Dionex IC Pure system Thermo Scientific...

  • Page 69: Dispensing Water From The Dispensing Valve

    0.2 µm final filter, open the white knurled screw. 0.2 µm final filter Knurled screw Do not close the knurled screw until pure water runs out of the opening at the knurled screw continuously. Thermo Scientific Dionex IC Pure system | 59...
  • Page 70 Chapter 10 | Initial start up Dionex IC Pure system Thermo Scientific...

  • Page 71: Chapter 11 Operating Elements

    Operating elements Contents "Description of control display" on page 62  “Control menu flow diagram” on page 63  Thermo Scientific IC Pure | 61...

  • Page 72: Description Of Control Display

    Mode menu. values in the menu UV-Lamp operating time  Cartridge number and maintenance interval  Rinsing  Disinfection  Display of error storage  Unlocking of the factory deerror settings using a  password 62 | IC Pure Thermo Scientific...

  • Page 73: Control Menu Flow Diagram

    Press enter Hours 11 Min. 21 OEM Menu OEM Menu Temp. comp. Send interval Code 01:00 h:min Press enter OEM Menu OEM Menu  Language µS/cm - M ·cm English µS/cm SW Version 4.1 Thermo Scientific IC Pure | 63...
  • Page 74 Chapter | Operating elements 64 | IC Pure Thermo Scientific...

  • Page 75: Chapter 12 System Control

    UV is shown on the display when the UV light in on. TC is showed if temperature compensation is on. In the event of an error, the fourth line of display will display most current error. Failure message Thermo Scientific Dionex IC Pure system | 65...

  • Page 76: Nonstop Mode

    The display shows: Picture shows Nonstop mode with error Picture shows Analyser mode when IC in the fourth line. Normally 3 lines are system cable is connected on the Dionex displayed IC Pure system. Dionex IC Pure system Thermo Scientific...

  • Page 77: Uv Lamp

    "Feed.limit" in the fourth line of the display if the purity has dropped below acceptable limits. Note: the setting range is in conductivity Measuring range, feedwater: 10 – 0.01 M·cm Setting range, limiting value:0.1- 50.0 µS/cm Basic setting: 0.2 µS/cm (5.0 M·cm) Thermo Scientific Dionex IC Pure system | 67...

  • Page 78: Ultra Pure Water Limiting Value

    In this menu, the operating hours of the UV-lamp are displayed. When the maximum operating time is reached, the “UV-time“ error message is triggered. The determination of UV-intensity is not possible for the Dionex IC Pure system. Therefore the display remains permanently as “UV-intensity - - -“. Dionex IC Pure system Thermo Scientific...

  • Page 79: Ultrapure Cartridge Serial Number

    OEM menu. (see “Set the interval rinse time” on page 74). Step Action Figure Press the “Menu“ key five times. The display shows: Confirm rinse by pressing the “Enter“ button. The rinsing is started for 30 sec. Thermo Scientific Dionex IC Pure system | 69...

  • Page 80: Disinfection Procedure

    (see “Disinfection” on page 82). Confirm with “Enter“. The Disinfec- tion is started for 30 min, indicating the remaining time. Note The completely process is described in the section “Disinfection” on page 82. Dionex IC Pure system Thermo Scientific...

  • Page 81: Error History

    Note When you press the “Menu“ button you will exit the user menu and the unit automatically resumes its last operating mode (“Nonstop/ Interval“ or “Analyser“ mode) Thermo Scientific Dionex IC Pure system | 71...

  • Page 82: Unlocking Code

    To simplify changing settings, press the “UV“ button to select the individual number in the numerical value which you want to change. Now use the “Arrow“ buttons to enter the wanted number from 0 to 9 at that selected position. The display shows: Dionex IC Pure system Thermo Scientific...

  • Page 83: Set The Limiting Value For Temperature

    Basic setting: 30 minutes Setting range: 15 - 90 minutes After entering the OEM menu, press the “Menu“ button three times. The display shows: Thermo Scientific Dionex IC Pure system | 73...

  • Page 84: Set The Interval Pump Time

    Basic setting: The actual date Setting range: 1 - 12 month; 1 - 31 day; 0 - 24 h; 0 - 60 min. After entering the OEM menu, press the “Menu“ button six times. The display shows: Dionex IC Pure system Thermo Scientific...

  • Page 85: Set The Sending Interval

    After entering the OEM menu, press the “Menu“ button eight times. The display shows: Select units, conductivity/resistance Basic setting: Resistance M · Setting range: Resistance M cm, Conductivity µS/cm · After entering the OEM menu, press the “Menu“ button nine times. The display shows: Thermo Scientific Dionex IC Pure system | 75...

  • Page 86: Switch Temperature Compensation On/Off

    After accessing the OEM menu, press the “Menu“ button eleven times. The display shows: Note The system is factory adjusted in the system control. In this section it is not necessary to be carried out changes of value for operating with an IC system. Dionex IC Pure system Thermo Scientific...

  • Page 87: Chapter 13 Maintenance

    Calibration of the conductivity sensor may only be performed by a service technician authorized by the manufacturer. Thermo Scientific Dionex IC Pure system | 77...

  • Page 88: Maintenance Intervals

    (optional) Please note that the lifetime of the wear parts is a direct function of the quality of the feedwater and the daily volume of water that is used. Dionex IC Pure system Thermo Scientific...
  • Page 89 Note The quick-connectors are attached to the unit in such a manner so as to prevent any confusion (switching). Ultrapure cartridge Put the cover for the ultrapure cartridge back in place and switch the unit on. Thermo Scientific Dionex IC Pure system | 79...

  • Page 90: Replacing The Pretreament Cartridge (Optional)

    Note The pretreatment cartridge should only be replaced when the maximum limit for the feedwater has been exceeded, when you cannot extract any water from the sampling tap, or when the replacement interval is due. Dionex IC Pure system Thermo Scientific...
  • Page 91 Note The quick-connectors are attached to the unit in such a manner so as to prevent any confusion Pretreatment (switching) cartridge Put the cover back in place and switch the unit on. Thermo Scientific Dionex IC Pure system | 81...

  • Page 92: Disinfection

    CAUTION If your skin should come into contact with a chlorine product, immediately rinse it with ample, fresh water. If your eyes come into contact with the disinfecting agent, immediately rinse them with ample, fresh water and immediately contact a physician. Dionex IC Pure system Thermo Scientific...
  • Page 93 Quick-connectors adapter for and center on in the tube jumper. When you hear an audible disinfection click here you can be sure that the quick-action fasteners have been inserted correctly. Quick-connectors Tube jumper Thermo Scientific Dionex IC Pure system | 83...
  • Page 94 The display shows “Disinfection cartridge“. Press “Enter“ to confirm that Disinfection cartridge or Disinfection adapter has been installed. c. The disinfection process is then started. Note Disinfection is completed after 30 minutes. The remaining time is displayed. Dionex IC Pure system Thermo Scientific...
  • Page 95 Switch the unit back on and dispense around 10 L of water from the external tank at the sampling tap. Note To dispense the amount of 10 L of water, the Dionex IC Pure system must be in the Nonstop mode. Drain fitting Thermo Scientific Dionex IC Pure system | 85...

  • Page 96: Changing The Ultrafilter

    Changing the ultrafilter Note You will need the following tools for replacing the ultra-filter: Open-end wrench, size 17, Phillips screwdriver and Teflon strip Step Action Figure Switch the system off and unplug from power supply Dionex IC Pure system Thermo Scientific...
  • Page 97 Mark the position of the fittings before removing them. Use Mounting bracket the open-end wrench size 17 mm (0.67 in) to unscrew the top and bottom fittings on the ultrafilter. Ultrafilter UV lamp Luerlock Ultrafilter Fitting Open-end wrench Ultrafilter Thermo Scientific Dionex IC Pure system | 87...
  • Page 98 Replace the cover on the unit, open the supply of the feedwater once the unit has been connected to the 20 L tank filling station and switch the unit on. Dispense 5 L of water and activate three rinses for the UF. Dionex IC Pure system Thermo Scientific...

  • Page 99: Uv-Reactor Assembly

    These stoppers are located in the UV lamp casing Stopper Item No.: 21.5008 Replacing the UV lamp CAUTION Never look directly into a UV lamp when it is on. It could damage your sight. Thermo Scientific Dionex IC Pure system | 89...
  • Page 100 UV lamp out by about 1 cm while still plugged in. a. Carefully unplug the plug for the UV lamp. b. Now, carefully pull the UV lamp up while turning it slightly in UV-lamp a clockwise direction at the same time. UV- lamp casing Dionex IC Pure system Thermo Scientific...
  • Page 101 You can then reattach the plug to the UV lamp and retighten UV lamp the UV assembly on the mounting plate using the two UV lamp retaining brackets and the two screws that you removed casing previously. UV lamp UV lamp casing Thermo Scientific Dionex IC Pure system | 91...

  • Page 102: Replacing The 0.2 Μm Final Filter

    Rotate the exhausted or clogged sterile filter in a clockwise position to remove it. 1/4“ thread 0.2 µm final filter Unpack the new sterile filter and screw it into the bottom 1/4“ thread on the sampling tap. Dionex IC Pure system Thermo Scientific...

  • Page 103: Autoclaving The 0.2 Μm Final Filter

    “Troubleshooting” on page 99, or replace the sterile filter back into the 1/4“ thread on the sampling tap filter with a new one. (see “Replacing the 0.2 µm final filter” on page 92). Thermo Scientific Dionex IC Pure system | 93...

  • Page 104: Recalibration Of The Tank Sensor For An Additional Tank Indicator

    90%. Dionex IC Pure system Setting screw d. Stop the rotating of the setting screw as soon as it reaches 100% on the tank indicator Control case display. Sensor, external 20 L tank Dionex IC Pure system Thermo Scientific...

  • Page 105: Draining The Internal 5 L And External 20 L Tank

    Therefore, at a filling level of 30% the tank water needs to be changed to prevent the shortening of the ultrapure cartridge lifetime. Thermo Scientific Dionex IC Pure system | 95...
  • Page 106 20 L tank, reattach the tube jumper to the Dionex IC Pure system and manually refill the internal 5 L or external 20 L tank completely. b. Switch the system on. Dionex IC Pure system Thermo Scientific...

  • Page 107: Chapter 14 Waste Disposal

    Only specially trained personal can take the system out of operation and dispose it properly. If you have a used or broken UV-lamp, contact your local Thermo Scientific service organization or waste disposal company.
  • Page 108 Chapter 14 | Waste disposal Dionex IC Pure system Thermo Scientific...

  • Page 109: Chapter 15 Troubleshooting

    Check and seal the tubing   connection Feedwater pressure > 600 kPa  (87 psi) (external tank filling Install a pressure reducer  station only) Contact the Thermo Fisher  Scientific service department Thermo Scientific Dionex IC Pure system | 99...
  • Page 110 Internal pressure too low  Readjust pressure reducer  Dispensed water flow rate out of  the tolerance range Contact Thermo Scientific for  calibration 0.2 µm final filter is clogged  Replace the 0.2 µm final filter  Air look in unit ...
  • Page 111 Replace measuring cell   “Measuring cell Temp.“ System control defect Replace system control   Error message: Ultrapure cartridge operating Replace with new ultrapure   “New ultrapure cartridge“ time has expired cartridge Thermo Scientific Dionex IC Pure system | 101...
  • Page 112 Chapter 15 | Troubleshooting Dionex IC Pure system Thermo Scientific...

  • Page 113: Chapter 16 Dionex Ic Pure System Spare Parts

    Keyboard foil 2. 50132289 Display front part 3. 50134036 Display holder 4. 50142984 Tank indicator 5. 17.0147 Display back part 6. 50134032 Rotary knob 7. 26.0025 Control display part 8. 50133988 Dispensing valve Thermo Scientific Dionex IC Pure system | 103...
  • Page 114 Connector 15. 50149264 Pressure pump 16. 50142981 Sensor for tank indicator 17. 50131190 Solenoid valve 18. 50142246 Pressure hold valve 19. 16.0126 Feedwater measuring cell 20. 50133979 Fuseholder with fuse 21. 50150598 Check valve Dionex IC Pure system Thermo Scientific...
  • Page 115 Sensor for tank indicator 27. 50148086 Float switch 28. 50148086 Float switch 29. 50145876 Wire jumper (not shown) 30. 50143964 Connecting wire 20 L tank (not shown) Taple top power supply (not shown) 31. 50149597 Thermo Scientific Dionex IC Pure system | 105...
  • Page 116 Chapter 16 | Dionex IC Pure system spare parts Dionex IC Pure system Thermo Scientific...

  • Page 117: Chapter 17 Consumables

    (if using pretreatment cartridge only - if experiencing short pre- treatment life) Pretreatment cartridge 09.2012 Wall-mounting bracket 09.2212 External 20 L tank 50146376 External 20 L tank with level control 50146378 Cleaning Solution, 1 syringe CMX25 Thermo Scientific Dionex IC Pure system | 107...
  • Page 118 Chapter 17 | Consumables Dionex IC Pure system Thermo Scientific...

  • Page 119: Chapter 18 Terminal Assignment

    Terminal assignment Thermo Scientific Dionex IC Pure system | 109...
  • Page 120 Chapter 18 | Terminal assignment Dionex IC Pure system Thermo Scientific...

  • Page 121: Chapter 19 Maintenance Record

    / Notes Signature volume flow cartridge disinfection [l/h] The following points must be observed in order to ensure the quality of the system. 1x / Weekly, enter measured values. Thermo Scientific Dionex IC Pure system | 111...
  • Page 122 Chapter 19 | Maintenance record Dionex IC Pure system Thermo Scientific...

  • Page 123: Chapter 20 Thermo Fisher Scientific Contact Information

    Thermo Fisher Scientific contact information Contact address for service: Overview of Thermo Scientific international sales organization Postal address in USA: Thermo Scientific 275 Aiken Road Asheville, NC 28804 Inquiries from USA/Canada Sales: +1 866 984 3766 Service: +1 800 438 4851...
  • Page 124 2016 Thermo Fisher Scientific Inc. All rights reserved. All trademarks are the property of Thermo Fisher Scientific Inc. and its subsidiaries. Specifications, terms and pricing are subject to change. Not all products are available in all countries. Please consult your local sales representative for details. Dionex IC Pure system Thermo Scientific...
  • Page 125 Dionex ICPure without pretreatment OFF mode 67 cartridge 55 Operating elements 61 Disinfection procedure 70 Operating Modes 65 Dispensing water from the Dispensing valve 59 Draining the internal 5L and external 20L tank 95 Thermo Scientific IC Pure | 115...
  • Page 126 69 Unlocking code 72 UV lamp 67 UV-reactor assembly 89 Venting the sterile filter 59 Wall Mounting 24 Waste disposal 97 Water connections DIONEX IC Pure system 15 Water connections for external 20L tank 16 IC Pure Thermo Scientific...
  • Page 127 Thermo Scientific IC Pure | 117...
  • Page 128 thermoscientific.com © 2016 Thermo Fisher Scientific Inc. All rights reserved. All trademarks are the property of Thermo Fisher Scientific Inc. and its subsidiaries. Specifications, terms and pricing are subject to change. Not all products are available in all countries. Please consult your local sales representative for details. Thermo Fisher Scientific 1214 Oakmead Parkway Building 10...

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