Evaluating The Results - Agilent Technologies InfinityLab LC Series User Manual

Isocratic and quaternary pumps
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7
Test Functions and Calibration
System Pressure Test

Evaluating the Results

The test fails, if the leak rate between pump and blank nut is higher than the limit
of 5 µL/min.
If the System Pressure Test fails:
Often it is only a damaged blank nut itself (poorly shaped from overtightening)
NOTE
that causes a failure of the test. Before investigating on any other possible
sources of failure make sure that the blank nut you are using is in good condition
and properly tightened!
If the test fails again, insert the blank nut at the outlet of the previous module in
the stack (e.g. autosampler outlet if TCC has been tested before), and repeat the
test. Exclude each module one by one to determine which module is leaking.
If the pump is determined to be the source of the leak, run the Pump Leak Rate
Test.
Agilent InfinityLab LC Series 1260 Infinity II Isocratic and Quaternary Pumps User Manual
Ensure that all fittings between the pump and the blank nut are tight.
Repeat the test.
116

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