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Agilent Technologies 1100 Series Manuals
Manuals and User Guides for Agilent Technologies 1100 Series. We have
19
Agilent Technologies 1100 Series manuals available for free PDF download: Reference Manual, Service Manual, User Manual, System Manual, Quick Start Manual, Manual
Agilent Technologies 1100 Series Reference Manual (346 pages)
Fluorescence Detector
Brand:
Agilent Technologies
| Category:
Security Sensors
| Size: 6.18 MB
Table of Contents
Series FD Reference Manual
3
Table of Contents
5
1 Installing the Fluorescence Detector
14
Site Requirements
14
Physical Specifications
16
Unpacking the Detector
17
Detector Accessory Kit Contents
18
Optimizing the Stack Configuration
20
Installing the Detector
20
Flow Connections to the Detector
24
2 First Steps with the Fluorescence Detector
28
Before You Start
28
Optimization Overview
29
Getting Started and Checkout
31
Starting Your Detector
31
Setting the Chromatographic Conditions
32
Observe the Maxima Via the Isoabsorbance Plot
34
Method Development
35
Step 1: Check the LC System for Impurities
36
Step 2: Optimize Limits of Detection and Selectivity
37
Step 3: Set up Routine Methods
46
Example: Optimization for Multiple Compounds
50
3 Optimizing the Fluorescence Detector
59
Optimization Overview
60
Design Features Help Optimization
61
Check Performance before You Start
61
Finding the Best Wavelengths
62
A Real Example
63
Finding the Best Signal Amplification
64
Changing the Xenon Flash Lamp Frequency
65
Lamp Life Savings
66
Selecting the Best Response Time
67
Reducing Stray Light
69
4 Troubleshooting and Test Functions
72
Overview of the Detector's Indicators and Test Functions
72
Status Indicators
73
Power Supply Indicator
73
Detector Status Indicator
74
Error Messages
75
Time-Out
76
Shutdown
77
Remote Time-Out
78
Synchronization Lost
79
Leak
80
Leak Sensor Open
82
Leak Sensor Short
83
Compensation Sensor Open
84
Compensation Sensor Short
85
Fan Failed
86
Motor Errors
87
Lamp Cover Open
89
FLF Board Not Found
90
ADC Not Calibrated
91
A/D Overflow
92
Flash Lamp Current Overflow
93
Flash Trigger Lost
94
Wavelength Calibration Failed
95
Wavelength Calibration Lost
96
Flow Cell Removed
97
No Peaks
98
Wavelength Verification and Calibration
99
Check of Raman Band of Water
102
The Wavelength Calibration Procedure
108
Preparation of the Glycogen Calibration Sample
108
Preparation of the Flow Cell
109
Wavelength Calibration
110
Verification
111
Test Functions
112
Lamp Intensity Test
113
Lamp Intensity History
114
Dark-Current Test
115
Excitation and Emission Grating Resistance History
116
Raman ASTM Signal-To-Noise Test
117
Using the Built-In Test Chromatogram
122
Using the Built-In DAC Test
125
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Agilent Technologies 1100 Series Reference Manual (334 pages)
Fluorescence Detector
Brand:
Agilent Technologies
| Category:
Security Sensors
| Size: 4.85 MB
Table of Contents
Table of Contents
5
1 Installing the Fluorescence Detector
14
Site Requirements
14
Physical Specifications
17
Unpacking the Detector
18
Detector Accessory Kit Contents
19
Optimizing the Stack Configuration
20
Installing the Detector
23
Flow Connections to the Detector
26
2 First Steps with the Fluorescence Detector
31
Before You Start
32
Optimization Overview
33
Getting Started and Checkout
34
Setting the Chromatographic Conditions
35
Starting Your Detector
35
Observe the Maxima Via the Isoabsorbance Plot
36
Method Development
37
Step 1: Check the LC System for Impurities
38
Step 2: Optimize Limits of Detection and Selectivity
39
Column Temperature
48
Flow Rate
48
Gradient
48
Injection Volume
48
FLD Settings
49
Step 3: Set up Routine Methods
49
Example: Optimization for Multiple Compounds
53
First Steps with the Fluorescence Detector 2
55
3 Optimizing the Fluorescence Detector
61
Optimization Overview
62
Design Features Help Optimization
63
Check Performance before You Start
63
Finding the Best Wavelengths
63
A Real Example
64
Finding the Best Signal Amplification
65
Changing the Xenon Flash Lamp Frequency
67
Lamp Life Savings
67
Selecting the Best Response Time
69
Reducing Stray Light
70
Status Indicators
73
Status Indicators
74
Detector Status Indicator
75
Power Supply Indicator
75
Error Messages
76
Time-Out
77
Remote Time-Out
78
Shutdown
78
Leak
79
Synchronization Lost
79
Leak Sensor Open
81
Leak Sensor Short
82
Compensation Sensor Open
83
Compensation Sensor
84
Fan Failed
85
Motor Errors
86
Lamp Cover Open
88
FLF Board Not Found
89
ADC Not Calibrated
90
A/D Overflow
91
4 Troubleshooting and Test Functions
73
Flash Lamp Current Overflow
91
Flash Trigger Lost
93
Wavelength Calibration Failed
94
Wavelength Calibration Lost
94
Flow Cell Removed 103 no
95
Peaks
96
Wavelength Verification and Calibration
96
Check of Raman Band of Water
99
The Wavelength Calibration Procedure
105
Preparation of the Flow Cell
105
Preparation of the Glycogen Calibration Sample
105
Wavelength Calibration
106
Verification
107
Test Functions
107
Lamp Intensity Test
108
Lamp Intensity History
109
Dark-Current Test
110
Excitation and Emission Grating Resistance History
111
Raman ASTM Signal-To-Noise Test
112
Using the Built-In Test Chromatogram
114
Using the Built-In DAC Test
116
Agilent Technologies 1100 Series Reference Manual (318 pages)
Diode Array and Multiple Wavelength Detectors
Brand:
Agilent Technologies
| Category:
Security Sensors
| Size: 7.43 MB
Table of Contents
Table of Contents
5
Installing the Detector
13
Site Requirements
14
Physical Specifications
16
Unpacking the Detector
17
Damaged Packaging
17
Delivery Checklist
17
Optimizing the Stack Configuration
20
Installing the Detector
22
Flow Connections to the Detector
25
How to Optmize the Detector
30
Optimizing the Detector Performance
30
Optimization Overview
31
Optimizing for Sensitivity, Selectivity, Linearity and Dispersion
33
Flow Cell Path Length
33
Peak Width (Response Time)
35
Sample and Reference Wavelength and Bandwidth
36
Slit Width
39
Optimizing Spectral Acquisition (DAD Only)
42
Margin for Negative Absorbance
43
Optimizing Selectivity
44
Quantifying Coeluting Peaks by Peak Suppression
44
Ratio Qualifiers for Selective Detection of Compound Classes
46
Troubleshooting and Test Functions
50
Overview of the Detector's Indicators and Test Functions
50
Status Indicators
51
Power Supply Indicator
51
Detector Status Indicator
51
Error Messages
53
Timeout
54
Shutdown
55
Remote Timeout
56
Synchronization Lost
57
Leak
58
Leak Sensor Open
60
Leak Sensor Short
61
Compensation Sensor Open
62
Compensation Sensor Short
63
Fan Failed
64
Open Cover
65
Cover Violation
66
Visible Lamp Current
67
Visible Lamp Voltage
68
Communication Error
69
Calibration Values Invalid
70
Diode Current Leakage
71
Holmium Oxide Test Failed
72
UV Lamp Current
73
UV Lamp Voltage
74
UV Ignition Failed
75
UV Heater Current
76
New Messages with the G1315B and G1365B Detectors
77
Module Type Changed
78
Illegal Value from Temperature Sensor Mounted on the Fan Assembly
80
Illegal Value from „Air Inlet" Temperature Sensor
81
Heater Failed
82
Heater Power at Limit
83
Wavelength Recalibration
84
Test Functions
85
Holmium Oxide Test
86
Intensity Test
88
Cell Test
90
Dark-Current Test
91
Filter Test
93
Repairing the Detector
96
Introduction into Repairing the Detector
96
Using the ESD Strap
98
Overview of the Repairing of the Detector
99
Simple Repairs
101
Exchanging a Lamp
102
Exchanging a Flow Cell
105
Repairing the Standard or Semi-Micro Flow Cell
108
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Agilent Technologies 1100 Series Service Manual (288 pages)
Nano Pump
Brand:
Agilent Technologies
| Category:
Water Pump
| Size: 6.81 MB
Table of Contents
Table of Contents
5
1 Installing the Pump
14
Site Requirements
14
Power Consideration
14
Power Cords
14
Bench Space
15
Environment
15
Unpacking the Nano Pump
17
Optimizing the Stack Configuration
19
Installing the Nano Pump
24
Installing the Nano Pump
25
Install the Degasser (G1379A)
27
Install the Solvent Cabinet
27
Get the System Ready for the First Injection
29
Manually Priming the Solvent Channels
29
Purging the Pump
30
2 Troubleshooting and Test Functions
33
Pump
34
Status Indicators
35
Power Supply Indicator
35
Instrument Status Indicator
36
Error Messages - Indication
36
Error Messages
37
Time-Out
39
Troubleshooting and Test Functions
39
Shutdown
40
Remote Time-Out
41
Synchronization Lost
42
Leak
43
Leak Sensor Open
44
Leak Sensor Short
45
Compensation Sensor Open
46
Compensation Sensor Short
47
Fan Failed
48
Open Cover
49
Restart Without Cover
50
Zero Solvent Counter
51
Pressure above Upper Limit
52
Pressure below Lower Limit
53
Pressure Signal Missing
54
Valve Failed
55
Missing Pressure Reading
56
Pump Configuration
57
Valve Fuse
58
Inlet-Valve Fuse
59
Temperature out of Range
60
Temperature Limit Exceeded
61
Motor-Drive Power
62
Encoder Missing
63
Inlet-Valve Missing
64
Electro-Magnetic-Proportional-Valve (EMPV) Missing
65
Flow Sensor Missing
66
Unsupported Flow Sensor
67
Leak Sensor Missing
68
Servo Restart Failed
69
Pump Head Missing
70
Index Limit
71
Index Adjustment
72
Index Missing
73
Stroke Length
74
Initialization Failed
75
Wait Time-Out
76
Testing Your Nano Pump
77
Micro Mode Pressure Test
77
Normal Mode Pressure Test
80
Leak Test
85
EMPV Test
96
Evaluating the Results
97
Flow Sensor Accuracy Calibration
98
EMPV Cleaning
103
Basic System Troubleshooting
104
System Pressure Abnormally Low
105
System Pressure Abnormally High
106
EMPV Failed to Initialize (Micro Mode Only)
107
Unstable Column Flow And/Or System Pressure
108
Poor Peak Shape
110
Failure to Produce Peaks, or Abnormally Small Peaks, after Injection
111
Wandering Detector Baseline
112
User Interface Displays Error Messages for Specific Modules
113
Agilent Technologies 1100 Series Reference Manual (302 pages)
Diode Array and Multiple Wavelength Detectors
Brand:
Agilent Technologies
| Category:
Security Sensors
| Size: 4.43 MB
Table of Contents
Table of Contents
4
1 Installing the Detector
13
Site Requirements
14
Physical Specifications
16
Unpacking the Detector
17
Damaged Packaging
17
Delivery Checklist
17
Optimizing the Stack Configuration
20
Installing the Detector
22
Flow Connections to the Detector
25
2 How to Optmize the Detector
30
Optimizing the Detector Performance
30
Optimization Overview
31
Optimizing for Sensitivity, Selectivity, Linearity and Dispersion
33
Flow Cell Path Length
33
Peak Width (Response Time)
35
Sample and Reference Wavelength and Bandwidth
36
Slit Width
39
Optimizing Spectral Acquisition (DAD Only)
41
Margin for Negative Absorbance
42
Optimizing Selectivity
43
Quantifying Coeluting Peaks by Peak Suppression
43
Ratio Qualifiers for Selective Detection of Compound Classes
44
3 Troubleshooting and Test Functions
46
O E Ie of the Dete to 'S I DI Ato S a D Test Fu Tio S
46
Status Indicators
47
Power Supply Indicator
48
Detector Status Indicator
48
Error Messages
49
Timeout
50
Shutdown
51
Remote Timeout
51
Synchronization Lost
52
Leak
52
Leak Sensor Open
54
Leak Sensor Short
55
Compensation Sensor Open
56
Compensation Sensor
57
Fan Failed
58
Open Cover
59
Cover Violation
60
Visible Lamp Current
61
Visible Lamp Voltage
61
Communication Error
62
Calibration Values Invalid
63
Diode Current Leakage
64
Holmium Oxide Test Failed
65
UV Lamp Current
65
UV Lamp Voltage
66
UV Ignition Failed
67
UV Heater Current
67
New Messages with the G1315B and G1365B Detectors
68
Module Type Changed
69
Illegal Value from Temperature Sensor Mounted on the Fan
71
Assembly
71
Heater Failed
73
Heater Power at Limit
74
Wavelength Recalibration
75
Test Functions
75
Holmium Oxide Test
76
Intensity Test
78
Cell Test
80
Dark-Current Test
81
Filter Test
83
Agilent Technologies 1100 Series Reference Manual (278 pages)
Binary Pump
Brand:
Agilent Technologies
| Category:
Laboratory Equipment
| Size: 6.28 MB
Table of Contents
Table of Contents
5
1 Installing the Pump
13
How to Install the Binary Pump
13
Site Requirements
14
Unpacking the Binary Pump
17
Optimizing the Stack Configuration
19
Installing the Binary Pump
21
Flow Connections of the Binary Pump with Solvent Selection Valve
24
Flow Connections of the Binary Pump Without Solvent Selection Valve
27
Priming and Purging the System
30
2 Optimizing Performance
33
How to Optimize the Binary Pump to Achieve Best Chromatographic Results
33
Hints for Successful Use of the Binary Pump
34
Solvent Information
36
Prevent Blocking of Solvent Filters
37
When to Use a Vacuum Degasser
39
When to Use the Continuous Seal Wash Option
40
When to Use Alternative Seals
41
When to Remove the Static Mixer
42
How to Optimize the Compressibility Compensation Setting
43
3 Troubleshooting and Test Functions
46
Status Indicators
48
Power Supply Indicator
49
Instrument Status Indicator
49
Error Messages
50
Timeout
51
Shutdown
52
Remote Timeout
53
Synchronization Lost
54
Leak
55
Leak Sensor Open
56
Leak Sensor Short
57
Compensation Sensor Open
58
Compensation Sensor Short
59
Fan Failed
60
Open Cover
61
Restart Without Cover
62
Zero Solvent Counter
63
Pressure above Upper Limit
64
Pressure below Lower Limit
65
Pressure Signal Missing
66
Valve Failed
67
Missing Pressure Reading
68
Pump Configuration
69
Valve Fuse
70
Inlet-Valve Fuse
71
Temperature out of Range
72
Temperature Limit Exceeded
73
Motor-Drive Power
74
Encoder Missing
75
Inlet-Valve Missing
76
Servo Restart Failed
77
Pump Head Missing
78
Index Limit
79
Index Adjustment
80
Index Missing
81
Stroke Length
82
Initialization Failed
83
Wait Timeout
84
Pressure Test
85
Running the Pressure Test
87
Evaluating the Results
89
Leak Test
91
Description
92
Running the Leak Test
94
Evaluating the Results
96
Agilent Technologies 1100 Series Reference Manual (272 pages)
Quaternary Pump
Brand:
Agilent Technologies
| Category:
Laboratory Equipment
| Size: 6.09 MB
Table of Contents
Table of Contents
5
1 Installing the Pump
13
How to Install the Quaternary Pump
13
Site Requirements
14
Unpacking the Quaternary Pump
17
Optimizing the Stack Configuration
20
Installing the Quaternary Pump
22
Flow Connections of the Quaternary Pump
25
Priming and Purging the System
28
2 Optimizing Performance
31
How to Optimize the Quaternary Pump to Achieve Best Chromatographic Results
31
Hints for Successful Use of the Quaternary Pump
32
Solvent Information
34
Prevent Blocking of Solvent Filters
35
Operational Hints for the Vacuum Degasser
36
Operational Hints for the Multi Channel Gradient Valve (MCGV)
37
When to Use the Continuous Seal Wash Option
38
When to Use Alternative Seals
39
Optimize the Compressibility Compensation Setting
40
3 Troubleshooting and Test Functions
43
The Quaternary Pump's Built-In Troubleshooting and Test Functions
43
Status Indicators
45
Power Supply Indicator
46
Pump Status Indicator
46
Error Messages
47
Timeout
48
Shut-Down
49
Remote Timeout
50
Synchronization Lost
51
Leak
52
Leak Sensor Open
53
Leak Sensor Short
54
Compensation Sensor Open
55
Compensation Sensor Short
56
Fan Failed
57
Open Cover
58
Restart Without Cover
59
Zero Solvent Counter
60
Pressure above Upper Limit
61
Pressure below Lower Limit
62
Pressure Signal Missing
63
Missing Pressure Reading
64
Pump Configuration
65
Valve Fuse
66
Inlet-Valve Fuse
67
Valve Failed
68
Motor-Drive Power
69
Encoder Missing
70
Inlet-Valve Missing
71
Temperature out of Range
72
Temperature Limit Exceeded
73
Servo Restart Failed
74
Pump Head Missing
75
Index Limit
76
Index Adjustment
77
Index Missing
78
Stroke Length
79
Initialization Failed
80
Wait Timeout
81
Pressure Test
82
Running the Pressure Test
84
Evaluating the Results
86
Leak Test
88
Running the Leak Test
90
Evaluating the Results
92
Agilent Technologies 1100 Series Reference Manual (247 pages)
Variable Wavelength Detector
Brand:
Agilent Technologies
| Category:
Laboratory Equipment
| Size: 3.87 MB
Table of Contents
Table of Contents
5
1 Installing the Variable Wavelength Detector
12
Site Requirements
12
Physical Specifications
15
Unpacking the Detector
16
Optimizing the Stack Configuration
18
Installing the Detector
19
Flow Connections to the Detector
23
2 How to Optimize the Detector
29
Optimizing the Detector Performance
29
Optimizing the Detector Performance
30
The Detector Parameters
33
3 Troubleshooting and Test Functions
36
Overview of the Detector's Indicators and Test Functions
36
Status Indicators
38
Power Supply Indicator
39
Detector Status Indicator
39
Error Messages
41
Timeout
42
Remote Timeout
43
Shutdown
43
Sychronization Lost
44
Leak
44
Leak Sensor Open
45
Leak Sensor Short
46
Compensation Sensor Open
47
Compensation Sensor Short
48
Fan Failed
49
Open Cover
50
Lamp Current Missing
51
Lamp Voltage Missing
51
Lamp Ignition Failed
53
Heater Current Missing
53
Calibration Failed
54
Holmium Oxide Test Failed
55
Test Failed
56
Wavelength Check Failed
57
Filter Check Failed
58
Wavelength Calibration
59
When to Calibrate the
59
Zero-Order Calibration
60
Calibration Procedure
61
656-Nm Wavelength
61
Calibration Calibration Procedure
61
Test Functions
62
Lamp-On Routine
63
Checking the Photocurrent
63
Holmium Oxide Test
64
Intensity Test
66
Dark Current Test
68
DAC Test
70
Grating Motor Test
71
Filter Motor Test
72
Test Chromatogram
73
Diagnostic Signal Output
75
Service Dialog
77
Signal Descriptions
79
Agilent Technologies 1100 Series System Manual (189 pages)
Capillary LC System
Brand:
Agilent Technologies
| Category:
Laboratory Equipment
| Size: 2.4 MB
Table of Contents
Table of Contents
5
Installing Your Capillary LC System
11
Site Requirements
12
Physical Specifications
13
System Installation Process
15
Installing a Capillary LC System with a Non-Thermostatted Sampler
16
Install the Diode Array Detector (DAD) (G1315B)
16
Install the Thermostatted Column Compartment (TCC) (G1316A)
17
Install the Micro Well-Plate Sampler (G1377A)
19
Install the Capillary Pump (G1376A)
20
Install the Micro Vacuum Degasser (G1379A)
21
Install the Solvent Cabinet
23
Installing a Capillary LC System with a Thermostatted Micro Sampler
24
Install the Thermostat for 1100 Samplers (G1330B)
24
Install the Micro Sampler (G1387A Micro Autosampler (ALS), or G1378A Micro Well-Plate Sampler)
25
Install the Thermostatted Column Compartment (TCC) (G1316A)
26
Install the Diode Array Detector (DAD) (G1315B)
27
Install the Capillary Pump (G1376A)
28
Install the Micro Vacuum Degasser (G1379A)
29
Install the Solvent Cabinet
29
Get the System Ready for the First Injection
31
Manually Priming the Solvent Channels
32
Conditioning the System under Method Conditions
34
Inject the Check-Out Sample
35
Procedure
36
Typical Chromatogram
36
Optimizing Performance
39
Hints for Successful Use of the Capillary Pump
40
Pump Issues
40
Fused Silica Capillary Issues
41
Sampler Issues
41
Column Thermostat Issues
42
DAD Issues
42
Solvent Information
42
Prevent Blocking of Solvent Inlet Filters
42
Cleaning the Solvent Filters
43
Hints for the Micro Vacuum Degasser
45
When to Use Alternative Seals
45
How to Choose the Primary Flow
46
Static Mixer and Filter
47
The Standard Static Mixer 40 the Standard Filter
47
How to Optimize the Compressibility Compensation Setting
48
The Fast Composition Change/Reconditioning Function
50
Purpose
50
How the Function Works
50
Capillaries and Fittings
52
Capillary Flow Diagram
53
Connecting Capillaries for the Capillary LC System
53
Fittings and Ferrules
60
Instructions to Connect a Capillary
61
Hints for Successful Use of Capillaries and Fittings
62
Basic System Troubleshooting
64
System Pressure Abnormally Low
64
System Pressure Abnormally High
64
EMPV Failed to Initialize (Micro Mode Only)
65
Unstable Column Flow And/Or System Pressure
66
Poor Peak Shape
68
Failure to Produce Peaks, or Abnormally Small Peaks, after Injection
69
Wandering Detector Baseline
70
User Interface Displays Error Messages for Specific Modules
71
Agilent Technologies 1100 Series Reference Manual (214 pages)
Thermostatted Column Compartment
Brand:
Agilent Technologies
| Category:
Laboratory Equipment
| Size: 5.04 MB
Table of Contents
Table of Contents
5
1 Installing the Column Compartment
12
Site Requirements
12
Physical Specifications
14
Unpacking the Column Compartment
15
Optimizing the Stack Configuration
17
Installing the Column Compartment
19
Flow Connections of the Column Compartment
21
2 How to Optimize the Column Compartment
25
Optimizing the Column Compartment
26
3 Troubleshooting and Test Functions
28
Overview of the Column Department's Indicators and Test Functions
28
Status Indicators
29
Power Supply Indicator
30
Instrument Status Indicator
30
Error Messages
31
Timeout
32
Shutdown
33
Remote Timeout
34
Synchronization Lost
35
Leak
36
Leak Sensor Open
37
Leak Sensor Short
38
Compensation Sensor Open
39
Compensation Sensor Short
40
Left Fan Failed
41
Right Fan Failed
42
Open Cover
43
Cover Violation
44
Left Temperature Timeout
45
Right Temperature Timeout
46
Defective Temperature Sensor
47
Heater Profile
48
Valve Failed
49
Column Temperature
50
Heatsink Temperature
51
Defective Heater Circuit
52
Thermostat Function Test
53
Temperature Calibration
55
Temperature Calibration Procedure
56
Calibration Problems
57
Installing the Temperature Sensor
58
4 Repairing the Column Compartment
62
Introduction into Repairing the Column Compartment
62
Overview of the Repairing the Column Compartment
65
Simple Repairs
66
Changing Column Identification Tags
67
Replacing Head Parts of Column Switching Valve
70
Correcting Leaks
72
Exchanging Internal Parts
73
Removing the Top Cover and Foam
75
Removing the Column Switching Valve
78
Installing the Column Switching Valve
81
Exchanging the Column Compartment Main (CCM) Board
84
Replacing the Column Identification Module (CID) Board
88
Exchanging the Fan
89
Removing the Heat Exchanger Assemblies
91
Unscrew the Z-Panel
92
Press against the Rear of the Z-Panel to Release the Metal
92
Plate from the Guide and Pull It Carefully Upwards
92
Lift the Z-Panel Together with the Top Plastic Panel
92
Locate the Ambient Temperature Sensor in the Top Plastic
93
Installing the Heat Exchanger Assemblies
94
Exchanging the Power Supply
97
Replacing the Leak Sensor or Leak Base
100
Replacing Status Light Pipe
105
Installing the Foam and the Top Cover
106
Assembling the Main Cover
109
Replacing the Column Compartment's Firmware
110
Agilent Technologies 1100 Series User Manual (214 pages)
Diode Array and Multiple Wavelength Detector SL
Brand:
Agilent Technologies
| Category:
Security Sensors
| Size: 5.17 MB
Table of Contents
Table of Contents
5
Site Requirements and Specifications
12
Site Requirements
12
Physical Specifications
15
Performance Specifications
16
Installing the Detector
19
Unpacking the Detector
20
Damaged Packaging
20
Delivery Checklist
20
Optimizing the Stack Configuration
22
Installing the Detector
24
Flow Connections to the Detector
27
Setting up the LAN Access
30
LAN Configuration
31
What You Have to Do First
32
TCP/IP Parameter Configuration
33
Configuration Switches
34
Initialization Mode Selection
35
Link Configuration Selection
39
Automatic Configuration with Bootp
40
Configuring the Agilent Bootp Service Program
40
Storing the Settings Permanently with Bootp
45
Manual Configuration
46
With Telnet
47
With Handheld Controller (G1323B)
51
PC and Agilent Chemstation Setup
54
PC Setup for Local Configuration
54
Agilent Chemstation Setup
55
Using the Detector
58
Setting up an Analysis
58
Before Using the System
58
Requirements and Conditions
60
Optimization of the System
62
Preparing the HPLC System
63
Running the Sample and Verifying the Results
72
Special Settings of the Detector
73
Control Settings
73
Configuration Settings
74
Online Spectra
75
Run Recovery Settings
76
Analog Output Settings
79
Spectrum Settings
80
Peakwidth Settings
82
Slit Settings
83
Margin for Negative Absorbance Settings
84
Optimizing the Detector
84
Special Setups with Multiple Dad/Mwds
85
Two Detectors of same Type (E.g. G1315C and G1315C)
85
Two Detectors of Similar Type (E.g. G1315C and G1315A/B)
85
How to Optimize the Detector
88
Agilent Technologies 1100 Series User Manual (148 pages)
Handheld Control Module
Brand:
Agilent Technologies
| Category:
Control Unit
| Size: 1.6 MB
Table of Contents
Table of Contents
9
1 The Agilent 1100 Series Control Module
17
Overview over the Agilent 1100 Series Control Module
18
Control Module Features
19
Control Module Keys
20
Control Module Software
24
Control Module Versions
31
2 Working with the Control Module
33
How to Use the Agilent 1100 Series Control Module
33
Installing the Control Module
34
General Functions
35
Troubleshooting
36
Inserting and Removing PC Cards
37
Working with Methods
38
Time Programming
43
Automating Analyses
44
Displaying Data Graphically
46
Logbooks
48
Printing Screens
49
Connecting External Devices
51
Firmware
53
Updating Firmware in the Control Module
53
Updating Firmware in the LC Modules
54
Coexecution with Agilent Chemstation
58
3 Using the Pump
63
Operational Details for the Agilent 1100 Series Pumping Systems
63
Turning the Pump on and off
64
Entering Settings
64
Purging the Pump
64
Purging Procedure
65
Adjusting Compressibility
66
Adjusting Stroke Volume
67
Automatic Shut-Down
67
Troubleshooting the Pump
68
Tracking Pump History / Pump EMF Limits
68
Resetting the Pump
69
Resetting the Pump Settings
69
4 Using the Degasser
71
Operational Details for the Agilent 1100 Series Vacuum Degasser
71
Starting the Degasser
72
Removing Gas Bubbles
72
Changing Solvents
73
5 Using the Autosampler
75
Operational Details for the Agilent 1100 Series Autosampler
75
Configuring the Autosampler
76
Entering Settings
76
Aligning Transport Arm/Gripper
79
Tracking Autosampler History / EMF Limits
79
Resetting the Autosampler
80
Troubleshooting the Autosampler
80
Agilent Technologies 1100 Series Reference Manual (108 pages)
Sample Capacity Extension
Brand:
Agilent Technologies
| Category:
Laboratory Equipment
| Size: 2.84 MB
Table of Contents
Table of Contents
5
Overview
9
Description
10
Specifications
11
General Instrument
11
Robotic Arm
12
Physical Performance
12
Environmental
12
Physical
13
Electrical
14
Barcodes
14
Installation
15
Site Preparation
16
Bench Space Requirements
16
Contents of the G2257A Shipping Kit
17
Installation
19
Installing the Automation Interface
19
Setting up the Well-Plate Handler
25
Installing the Optional Rack Extension
33
Installing the Optional Fixed Barcode Reader
35
Installing the Optional Hand-Held Barcode Reader
38
Barcode Requirements
39
Making the Electrical Connections
41
Adjusting the Barcode Reader Position
42
Adjusting the Lateral Position of the Well-Plate Handler
44
Preliminary Adjustment of the Well-Plate Handler Position
45
Well-Plate Handler Teaching
47
Teaching Using the Chemstation
47
Teaching Using the Hand-Held Controller
51
Fine Adjustment of the Well-Plate Handler Position
53
Adjusting the Radius
53
Adjusting for the Gripper Fingers
54
Adjusting the Centering Spring
55
De-Installation of the Automation Interface
56
G2257A Software Navigation
57
Using the Sample Capacity Extension with the Chemstation
58
Well-Plate Handler Configuration
58
Working with the Sample Capacity Extension
63
What Is a Hypersequence
64
Creating a Hypersequence
65
Hypersequence Parameters
65
Barcode Settings
69
The Hypersequence Table
70
Importing an Import File
72
Making an Import File
76
Troubleshooting and Error Handling
82
Well-Plate Handler Test
82
Testing with the Chemstation
82
Testing with the Hand-Held Controller
85
Automation Interface Test
87
Agilent Technologies 1100 Series Reference Manual (98 pages)
Autosampler Thermostat
Brand:
Agilent Technologies
| Category:
Thermostat
| Size: 2.76 MB
Table of Contents
Table of Contents
5
1 Theory of Operation
10
Introduction to the Thermostatted Autosampler
10
ALS Thermostat Operation
12
ALS Thermostat Control and Electronics
14
Temperature Controlled Autosampler Board (TCA)
15
Electrical Connections
17
2 Installing the G1330B Thermostat
20
Site Requirements
20
Unpacking the Autosampler
23
Optimizing the Stack Configuration
25
Controller Requirements
27
Installing the G1330B Thermostat
28
Stage 1: Preparing the als Thermostat and Autosampler
29
Stage 2: Power Cable and Interface Cable Connection
32
Stage 3: Flow Connections
35
Stage 4: Installing the Sample Tray
36
Stage 5: Installing Tray Cover and Front Cover
39
Stage 6: Turning on the Thermostatted Autosampler
40
Stage 7: Update of Control Module Firmware
40
Stage 8: Update of the Agilent Chemstation Software
41
Transporting the Thermostatted Autosampler
43
3 Troubleshooting and Test Functions
46
Overview of the Thermostat's Indicators and Test Functions
46
Status Indicators
47
Power Supply Indicator
48
Instrument Status Indicator
48
ALS Thermostat Error Messages
49
Fan Failed
50
Temperature Control Failed (1 - 4)
51
Temperature Sensor Failed (1 - 4)
52
Lost Contact to als Thermostat
53
Power Fail for als Thermostat Module
54
Temperature out of Range
55
Bad Cooling / Heating Performance
56
4 Repairing the als Thermostat Module
58
Introduction into Repairing the Thermostat
58
Using the ESD Strap
59
Overview of the Repairing the Thermostat
60
Exchanging the Power Supply Fuses
61
Exchanging Internal Parts
62
Removing the Top Cover and Foam
63
Exchanging Heat Exchanger Fan
65
Exchanging the Heatsink Fans
67
Exchanging the Sensors
69
Exchanging the TCA Board
72
Assembling the Main Cover
75
5 ALS Thermostat Parts and Materials
78
Main Assemblies
78
Accessory Kit G1330-68705
79
Main Assemblies
80
Foam Parts
81
Plastic Parts
82
Heat Exchanger Fan Parts
83
Agilent Technologies 1100 Series Reference Manual (94 pages)
Micro Vacuum Degasser
Brand:
Agilent Technologies
| Category:
Laboratory Equipment
| Size: 2.45 MB
Table of Contents
Table of Contents
5
1 Installing the Micro Vacuum Degasser
9
How to Install the Micro Vacuum Degasser
9
Site Requirements
10
Unpacking the Micro Vacuum Degasser
12
Optimizing the Stack Configuration
14
Installing the Micro Vacuum Degasser
16
Flow Connections to the Micro Vacuum Degasser
18
Transporting the Micro Vacuum Degasser
21
2 Optimizing Performance
23
How to Optimize the Micro Vacuum Degasser to Achieve Best Chromatographic Results
23
Introduction to the Micro Vacuum Degasser
24
When to Use a Micro Vacuum Degasser
25
Operation Modes of the Micro Vacuum Degasser
26
Operational Hints for the Micro Vacuum Degasser
29
Solvent Information
31
Prevent Blocking of Solvent Filters
32
3 Troubleshooting
33
Errors, Their Probable Cause, and the Action Required to Correct Them
33
Status Indicators
34
Power Supply Lamp
35
Instrument Status Indicator
35
Hardware Symptoms
36
All Lamps Are off
37
If the Status Indicator Is Red
39
If the Status Indicator Is Yellow and the Vacuum Pump Is Not Running
40
If the Status Lamp Is Yellow and the Vacuum Pump Runs Continuously
41
4 Repairing the Micro Vacuum Degasser
45
Instructions on How to Repair the Micro Vacuum Degasser
45
Cleaning the Instrument
48
Using the ESD Strap
49
Removing and Refitting the Top Cover
50
Assembling the Main Cover
52
Exchanging the Status Light Pipe
53
Overview of Internal Parts
54
Exchanging a Vacuum Chamber
55
Exchanging the Vacuum Pump
57
Exchanging the Solenoid Valve
59
Exchanging the Degasser Control Assembly and the Sensor Assembly
60
5 Parts and Materials
63
Detailed Illustrations and Listings for Parts and Materials Identification
63
Micro Vacuum Degasser Parts
64
Cover Parts
66
Sheet Metal Kit
67
Power and Status Light Pipes
68
Accessory Kit
69
Cable Overview
70
Remote Cables
71
Auxiliary Cable
72
Agilent Technologies 1100 Series User Manual (68 pages)
Nano Pump
Brand:
Agilent Technologies
| Category:
Water Pump
| Size: 1.58 MB
Table of Contents
Table of Contents
5
1 Introduction - Around Your Nano Pump
10
Introduction to the Nano Pump
10
Nano Pump Main Overview
11
Pumphead Overview
12
Flow Connections
13
Fittings and Ferrules
14
Electrical Connections
15
2 Getting Started
17
Road Maps to Start an Analysis with the Nano Pump
18
Road Map to Configure the Nano Pump
18
Road Map to Prepare the Nano Pump for an Analysis
18
Road Map to Start an Analysis
19
Using the Chemstation to Configure Your Pump
20
Pump Configuration Screen
20
Pump Auxiliary Screen
21
Setup Pump Parameter Screen
23
Priming the Pump for Best Results
28
Manually Priming the Solvent Channels
28
Purging the Pump
29
3 Become an Expert
34
Hints for Successful Use of the Capillaries
34
Hints for Successful Use of the Micro Vacuum Degasser
36
Hints for Successful Use of the Nano Pump
37
Hints for Using the Fast Composition Change/Reconditioning
38
Purpose
38
How the Function Works
38
Hints for Successful Use of the Micro Well Plate Sampler
40
Hints for Successful Use of the Column and Switching Valve Compartment
41
Best Practices for Filters
42
The Solvent Inlet Filters
42
Inline Filter
43
Hints for Successful Use of Solvents and Mobile Phase
44
Hints for Choosing the Primary Flow
45
Hints to Optimize the Compressibility Compensation Setting
47
Diagnosis Screens
49
Test Screens
52
EMF Screen
53
A Safety Information
56
Safety Information
56
General
56
Operation
56
Safety Symbols
57
Lithium Batteries Information
59
Danish Information
59
Radio Interference
60
Test and Measurement
60
Sound Emission
61
Manufacturer's Declaration
61
Solvent Information
62
Agilent Technologies on Internet
63
Agilent Technologies 1100 Series Quick Start Manual (49 pages)
LC/MSD Trap System
Brand:
Agilent Technologies
| Category:
Laboratory Equipment
| Size: 0.44 MB
Table of Contents
What Is the Agilent 1100 Series LC/MSD Trap System
2
Where to Find Additional System Information
3
What Is New in Version 5.2 Software
4
New for Overall Software Package
4
New for Individual Programs with Compliance Software
4
New for Individual Programs with or Without Compliance Software
4
Data Analysis
5
Instructional Overview
6
Start here
6
Step 1-Start the Software
7
Start the Trap Software on an LC/MSD Trap Control PC
7
Start the Trap Software for an Offline Installation
9
Open the Libraryeditor or Reportdesigner Programs
9
Chemstation Window
10
Step 1A-Become Familiar with the Software
10
MSD Trap Control Window
11
Status Modes
18
Dataanalysis Window
19
Quantanalysis Window
20
Step 2-Prepare the Instrument
21
Step 3-Set up and Run an Acquisition Method
22
Set up an Acquisition Method
23
Acquire MS/MS Spectral Data Only
26
Acquire Chromatographic and Spectral Data
27
Step 4-Review Data and Identify Compounds
28
Start the Dataanalysis Software
29
Review Chromatograms and Spectra
29
Find Compound MS Spectra
30
Find Compound MS/MS Spectra and Generate a Results Report
31
Create and Use a Library to Identify Unknowns
32
Optional Steps
34
Deconvolute and Search Protein Spectra
34
Quantify Compounds
35
Shut down or Place the Instrument in Standby
36
Power off the Instrument
37
Agilent Methods, Data Files and Report Layouts
38
Dataanalysis Methods (VB Scripts and Commands) and Data
38
Comma Separated Value (CSV) Methods for MSD Trap Control
44
Report Layouts for Dataanalysis and Quantanalysis
45
In this Book
48
Agilent Technologies
48
Agilent Technologies 1100 Series User Manual (28 pages)
LC Devices Connecting the Hardware and Triggering Data Acquisition
Brand:
Agilent Technologies
| Category:
Test Equipment
| Size: 0.78 MB
Table of Contents
Table of Contents
3
Preface
5
About this Guide
5
Related Documentation
5
Safety and Special Notices
5
Safety Precautions
6
Contacting Us
6
Chapter 1 Agilent Modules Supported by LC Devices Versions 2.0.2 and 2.1.0
9
Chapter 2 Connecting the Hardware
11
Ethernet Communication Kit
11
Installing a Network Card in an Agilent Module
12
Connecting the Ethernet Communication Cables
15
Installing the External Contact Interface Board
16
Connecting the Trigger Cable
17
Chapter 3 Configuring the Autosampler for Contact Closure
19
Chapter 4 Triggering Data Acquisition with the Autosampler
21
Chapter 5 Turning off the Solvent Tracking Feature
23
Appendix A Upgrading an HP 1100 Series LC
25
Index
27
Agilent Technologies 1100 Series Manual (4 pages)
Exchanging the Multi-Channel Gradient Valve on the Quaternary Pump
Brand:
Agilent Technologies
| Category:
Water Pump
| Size: 0.14 MB
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